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in Introduction—Composite Materials and Optical Microscopy
> Optical Microscopy of Fiber-Reinforced Composites
Published: 01 November 2010
Fig. 1.2 Composite materials made from different types of fibers. (a) Woven glass fiber fabric composite revealing a multiphase-matrix morphology. Ultrathin section, transmitted-light phase contrast, 20× objective. (b) Kevlar (E.I. du Pont de Nemours and Company) fabric composite cross section
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Series: ASM Technical Books
Publisher: ASM International
Published: 01 September 2011
DOI: 10.31399/asm.tb.cfw.t52860035
EISBN: 978-1-62708-338-6
... of programming various geometries using advanced software tools and discusses how various materials, such as rovings, tow-preg, prepreg tape, and woven materials, affect winding program generation. computer numerical controlled winding machines computer-aided manufacturing filament winding prepreg tape...
Abstract
This chapter discusses the ways in which the evolution of filament winding software systems has capitalized on the inherent flexibility of computer numerical controlled winding machines and enhanced their productivity. It provides a detailed discussion on different types of geometries that can be wound, from the simple to the highly complex, with insight into the limitations, advantages, and challenges of each. Components covered include classic axisymmetric parts (rings, pipes, driveshafts, pipe reducers, tapered shafts, closed-end pressure vessels, and storage tanks), nonround sections (aeromasts, airfoils, box sections, and fuselage sections), curved-axis parts (elbows, ducts), and special applications (tees). Basic winding concepts, such as band pattern, are discussed and explained, and some simple predictive formulae are introduced. The chapter also provides examples of programming various geometries using advanced software tools and discusses how various materials, such as rovings, tow-preg, prepreg tape, and woven materials, affect winding program generation.
Book Chapter
Series: ASM Technical Books
Publisher: ASM International
Published: 01 November 2010
DOI: 10.31399/asm.tb.omfrc.t53030237
EISBN: 978-1-62708-349-2
... and constituents of the matrix and composite material. Figure 14.1(a) shows a micrograph of an as-processed epoxy woven glass fabric composite with an epoxy surfacing film. In this image, there is no surface degradation. When the composite was subjected to a temperature of 204 °C (400 °F) for a period of time...
Abstract
Polymer composite materials are subject to degradation if not appropriately protected from the environment. Composite materials having polymeric matrices are susceptible to degradation from heat, sunlight, ozone, atomic oxygen (in space), moisture, solvents (chemicals), fatigue, excessive loading, and combinations of these environmental conditions. This chapter discusses the effects of heat, ultraviolet-light, and atomic oxygen on composite materials.
Book Chapter
Series: ASM Technical Books
Publisher: ASM International
Published: 01 November 2010
DOI: 10.31399/asm.tb.scm.t52870489
EISBN: 978-1-62708-314-0
... sizes help reduce labor costs because more material is deposited with each ply. However, large tow sizes in woven cloth can increase the chances of voids and matrix microcracking caused by larger resin pockets. 18.3 Product Form Selection A multitude of material product forms are used...
Book Chapter
Series: ASM Technical Books
Publisher: ASM International
Published: 01 November 2010
DOI: 10.31399/asm.tb.scm.t52870031
EISBN: 978-1-62708-314-0
... as well as physical and mechanical property data for commercially important high-strength fibers. aramid fibers carbon fibers composite reinforcement glass fibers graphite fibers prepreg ultra-high molecular weight polyethylene fibers woven fabrics REINFORCEMENTS for composite materials...
Abstract
This chapter discusses the properties and processing characteristics of glass, aramid, carbon, and ultra-high molecular weight polyethylene fibers and related product forms, including woven fabrics, prepreg, and reinforced mats. It also includes a review of fiber terminology as well as physical and mechanical property data for commercially important high-strength fibers.
Book Chapter
Series: ASM Technical Books
Publisher: ASM International
Published: 01 October 2012
DOI: 10.31399/asm.tb.lmub.t53550385
EISBN: 978-1-62708-307-2
... and given a freestanding postcure at 177 °C (350 °F) for 2 h. The properties of both materials in both unidirectional and woven cloth form are essentially equivalent. However, two points must be made concerning these materials. First, because there is no autoclave pressure to suppress void formation...
Abstract
Polymer-matrix composites are among the lightest structural materials in use today. They are also highly resistant to corrosion and fatigue and their load-carrying capabilities, such as strength and stiffness, can be tailored for specific applications. This chapter discusses the primary advantages and disadvantages of polymer-matrix composites, how they are produced, and how they perform in different applications. It describes the construction of laminates, the fibers and resins used, and the methods by which they are combined. It explains how strength, modulus, toughness, and high-temperature and corrosion behaviors are determined by the orientation, shape, and spacing of fibers, the number of plies, resin properties, and consolidation and forming methods. The chapter also covers secondary fabrication processes, such as thermoforming, machining, and joining, as well as production equipment and product forms, and include guidelines for optimizing tradeoffs when selecting fibers, resins, and production techniques.
Book Chapter
Series: ASM Technical Books
Publisher: ASM International
Published: 01 November 2010
DOI: 10.31399/asm.tb.omfrc.t53030147
EISBN: 978-1-62708-349-2
... and unidirectional carbon fiber prepreg. Voids were found mainly at the bottom of the lay-up and in the woven fabric prepreg, most likely due to lower resin pressure. Although most composite materials are cross sectioned through the thickness to determine the void content, more insight may be gained...
Abstract
Achieving the best-performing composite part requires that the processing method and cure cycle create high-quality, low-void-content structures. If voids are present, the performance of the composite will be significantly reduced. There are multiple causes of voids in composite materials; they are generally categorized as voids that are due to volatiles (such as solvents, water) or voids that result from entrapped air. This chapter describes the analysis of various types of voids. It reviews techniques for analysis of voids at ply-drops, voids due to high fiber packing, and voids that occur in honeycomb core composites. The final section of the chapter discusses void documentation through the use of nondestructive inspection techniques and density/specific gravity measurement methods.
Book Chapter
Series: ASM Technical Books
Publisher: ASM International
Published: 01 November 2010
DOI: 10.31399/asm.tb.omfrc.t53030137
EISBN: 978-1-62708-349-2
..., or environmental resistance. The addition of woven fabric or different fiber materials may be combined to achieve the desired performance. Figure 7.6 shows a cross section of a composite part made with woven glass fabric prepreg and two different unidirectional carbon fiber prepreg materials. Using...
Abstract
Analyzing the structure of composite materials is essential for understanding how the part will perform in service. Assessing fiber volume variations, void content, ply orientation variability, and foreign object inclusions helps in preventing degradation of composite performance. This chapter describes the optical microscopy and bright-field illumination techniques involved in analyzing ply terminations, prepreg plies, splices, and fiber orientation to provide the insight necessary for optimizing composite structure and performance.
Series: ASM Technical Books
Publisher: ASM International
Published: 01 November 2010
DOI: 10.31399/asm.tb.omfrc.9781627083492
EISBN: 978-1-62708-349-2
Series: ASM Technical Books
Publisher: ASM International
Published: 01 November 2010
DOI: 10.31399/asm.tb.omfrc.t53030001
EISBN: 978-1-62708-349-2
... thermoplastic or thermoset resins combined with either discontinuous or continuous unidirectional fibers or woven fabrics ( Fig. 1.1a to 1.1c ). Typical reinforcements consist of glass, carbon, or aramid fibers, but other materials, such as boron, ceramic, and thermoplastic fibers, may also be used...
Abstract
This chapter provides a general description of materials and methods for manufacturing high-performance composites. The materials covered are polymer matrices and prepreg materials and the methods include infusion processes, composite-toughening methods, matrix-toughening methods, and dispersed-phase toughening. In addition, the chapter provides information on interlayer-toughened composites and honeycomb or foam structure composite materials. It also discusses the processes in optical microscopy of composite materials.
Series: ASM Technical Books
Publisher: ASM International
Published: 01 June 2022
DOI: 10.31399/asm.tb.tstap.t56040069
EISBN: 978-1-62708-428-4
... improvement in the viscosity of the epoxy. As with the preparation for all thermal spray coatings, sufficient material must be removed during the planar grinding stage to ensure that all sectioning damage has been removed. While all laboratories indicated a planar grinding step, one laboratory went as far...
Abstract
Abradable coatings (such as Ni-4Cr-4Al/bentonite) are used throughout jet engines, primarily as sacrificial coatings into which moving components wear. This article presents the Accepted Practice for sample preparation of abradable coatings for metallographic analysis, based on round robin testing by several laboratories.
Book Chapter
Series: ASM Technical Books
Publisher: ASM International
Published: 01 November 2010
DOI: 10.31399/asm.tb.scm.t52870119
EISBN: 978-1-62708-314-0
... with the resin and removing excess resin and entrapped air. The laminate is built up layer by layer until the required thickness is obtained. E-glass is the most prevalent material, but S-2 glass, carbon, or aramid can be used where the improved properties justify the higher costs. Heavy glass woven rovings (500...
Abstract
This chapter familiarizes readers with the many and varied thermoset composite fabrication processes and the types of applications for which they were developed. It describes wet lay-up, prepreg lay-up, and low-temperature vacuum bag curing prepreg processes, which are best suited for low-volume, medium-sized and larger parts. It also discusses filament winding and preforming processes (including weaving, knitting, stitching, and braiding) in addition to resin-transfer molding, resin film infusion, and pultrusion.
Book Chapter
Series: ASM Technical Books
Publisher: ASM International
Published: 01 November 2010
DOI: 10.31399/asm.tb.scm.t52870373
EISBN: 978-1-62708-314-0
... a freestanding postcure at 350 °F (175 °C) for two hours. The properties of both materials in unidirectional and woven cloth form are essentially equivalent. However, two points need to be made concerning these materials. First, since there is no autoclave pressure to suppress void formation and since...
Book Chapter
Series: ASM Technical Books
Publisher: ASM International
Published: 01 August 2013
DOI: 10.31399/asm.tb.ems.t53730115
EISBN: 978-1-62708-283-9
...Abstract Abstract This chapter discusses the properties and uses of fiber-reinforced composites. It also describes the effect of volume fraction and fiber length. fiber length fiber-reinforced composites WITH COMPOSITE MATERIALS, combinations of properties can be achieved that could...
Book Chapter
Series: ASM Technical Books
Publisher: ASM International
Published: 01 November 2010
DOI: 10.31399/asm.tb.omfrc.t53030067
EISBN: 978-1-62708-349-2
... for the first step of the polishing process. These surfaces have included woven, nonnap cloths as well as diamond lapping films. The use of a 9 μm diamond lapping film provides good results but is quite costly due to the ease with which these substrates tear during polishing of hybrid materials. Although...
Abstract
The most common methods for preparing polymeric composites for microscopic analysis can be used for most fiber-reinforced composite materials. There are, however, a few composite materials that require special preparation techniques. This chapter discusses the processes involved in the preparation of titanium honeycomb composites, boron fiber composites, titanium/polymeric composite hybrids, and uncured prepreg materials.
Series: ASM Technical Books
Publisher: ASM International
Published: 01 June 2022
DOI: 10.31399/asm.tb.tstap.t56040030
EISBN: 978-1-62708-428-4
...) Medium resilience woven acetate cloth. Courtesy of Metcut Research Figure 13(c) High nap cloth. Courtesy of Metcut Research The disc rotation speed, process time and specimen loading required for the respective grinding and polishing steps for various classes of material are summarized...
Abstract
This article presents best practices for the metallographic preparation of specimens produced via thermal spray coating methods. It outlines typical metallographic preparation process flow, highlighting important considerations for obtaining a clear and representative specimen suitable for characterization via examination techniques, such as optical or electron microscopy. The process flow includes preliminary resin infiltration, sectioning, mounting, grinding, and polishing. To aid in the identification and resolution of common issues during subsequent specimen analysis, the article presents common issues, along with causes and mitigation strategies. It describes the processes involved in the interpretation of the thermal spray coating microstructure.
Series: ASM Technical Books
Publisher: ASM International
Published: 01 November 2019
DOI: 10.31399/asm.tb.mfadr7.t91110391
EISBN: 978-1-62708-247-1
... adequate for those early devices but as device geometries, densities, and materials have evolved these techniques have also had to evolve. This guide will introduce new analysts to the methods of cross-sectioning semiconductor devices and provide a refresher for the more experienced analysts. Topics...
Abstract
Cross-sectioning is a technique used for process development and reverse engineering. This article introduces novice analysts to the methods of cross-sectioning semiconductor devices and provides a refresher for the more experienced analysts. Topics covered include encapsulated (potted) device sectioning techniques, non-encapsulated device techniques, utilization of the focused ion beam (FIB) making a cross-section and/or enhancing a physically polished one. Delineation methods for revealing structures are also discussed. These can be chemical etchants, chemo-mechanical polishing, and ion milling, either in the FIB or in a dedicated ion mill.
Book Chapter
Series: ASM Technical Books
Publisher: ASM International
Published: 01 December 2003
DOI: 10.31399/asm.tb.cfap.t69780417
EISBN: 978-1-62708-281-5
...Abstract Abstract This article depicts typical fractographic features for a number of different composite materials, covering interlaminar and translaminar fracture characteristics in composite materials. fractography composites interlaminar fracture translaminar fracture FRACTURE...
Book Chapter
Series: ASM Technical Books
Publisher: ASM International
Published: 01 October 2012
DOI: 10.31399/asm.tb.lmub.t53550569
EISBN: 978-1-62708-307-2
...-matrix composites chemical vapor infiltration directed metal oxidation hot pressing liquid silicon infiltration polymer infiltration reaction bonding sol-gel techniques MONOLITHIC CERAMIC MATERIALS contain many desirable properties, such as high moduli, high compression strengths, high...
Abstract
Ceramic-matrix composites possess many of the desirable qualities of monolithic ceramics, but are much tougher because of the reinforcements. This chapter explains how reinforcements are used in ceramic-matrix composites and how they alter energy-dissipating mechanisms and load-carrying behaviors. It compares the stress-strain curves for monolithic ceramics and ceramic-matrix composites, noting improvements afforded by the addition of reinforcements. It then goes on to discuss the key attributes, properties, and applications of discontinuously reinforced ceramic composites, continuous fiber ceramic composites, and carbon-carbon composites. It also describes a number of ceramic-matrix composite processing methods, including cold pressing and sintering, hot pressing, reaction bonding, directed metal oxidation, and liquid, vapor, and polymer infiltration.
Book Chapter
Series: ASM Technical Books
Publisher: ASM International
Published: 01 November 2010
DOI: 10.31399/asm.tb.scm.t52870183
EISBN: 978-1-62708-314-0
... thermoplastic composites THERMOPLASTIC COMPOSITE FABRICATION PROCESSES are discussed in this chapter. The three main areas covered are consolidation, thermoforming, and joining. The basics of thermoplastic composite materials were discussed in Chapter 3, “Matrix Resin Systems.” 6.1 Thermoplastic...