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Swaminathan Subramanian, Raghaw Rai
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Book Chapter
Transmission Electron Microscopy
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 November 2019
DOI: 10.31399/asm.tb.mfadr7.t91110461
EISBN: 978-1-62708-247-1
... Abstract The ultimate goal of the failure analysis process is to find physical evidence that can identify the root cause of the failure. Transmission electron microscopy (TEM) has emerged as a powerful tool to characterize subtle defects. This article discusses the sample preparation procedures...
Abstract
The ultimate goal of the failure analysis process is to find physical evidence that can identify the root cause of the failure. Transmission electron microscopy (TEM) has emerged as a powerful tool to characterize subtle defects. This article discusses the sample preparation procedures based on focused ion beam milling used for TEM sample preparation. It describes the principles behind commonly used imaging modes in semiconductor failure analysis and how these operation modes can be utilized to selectively maximize signal from specific beam-specimen interactions to generate useful information about the defect. Various elemental analysis techniques, namely energy dispersive spectroscopy, electron energy loss spectroscopy, and energy-filtered TEM, are described using examples encountered in failure analysis. The origin of different image contrast mechanisms, their interpretation, and analytical techniques for composition analysis are discussed. The article also provides information on the use of off-axis electron holography technique in failure analysis.
Book Chapter
Imaging and Diffraction with Commercially Available Transmission Detectors
Available to PurchaseBook: STEM in SEM Introduction to Scanning Transmission Electron Microscopy for Microelectronics Failure
Series: ASM Technical Books
Publisher: ASM International
Published: 23 January 2020
DOI: 10.31399/asm.tb.stemsem.t56000001
EISBN: 978-1-62708-292-1
... Abstract This chapter discusses the principles of scanning transmission electron microscopy (STEM) as implemented using conventional scanning electron microscopes (SEMs). It describes the pros and cons of low-energy imaging and diffraction, addresses basic hardware requirements, and provides...
Abstract
This chapter discusses the principles of scanning transmission electron microscopy (STEM) as implemented using conventional scanning electron microscopes (SEMs). It describes the pros and cons of low-energy imaging and diffraction, addresses basic hardware requirements, and provides information on imaging modes, detector positioning and alignment, and the effect of contrast reversal. It also discusses beam convergence and angular selectivity, the use of application-specific masks, and how to generate grain orientation maps for different material systems.
Book
STEM in SEM: Introduction to Scanning Transmission Electron Microscopy for Microelectronics Failure
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 23 January 2020
DOI: 10.31399/asm.tb.stemsem.9781627082921
EISBN: 978-1-62708-292-1
Image
Transmission of Si improves with wafer thinning Note that transmission for ...
Available to PurchasePublished: 01 November 2019
Figure 28 Transmission of Si improves with wafer thinning Note that transmission for 10 20 cm −3 material through 100 microns is less than a percent. Calculated from empirical formulas given by A. Falk in [7] .
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Image
Dislocation network in undeformed single crystal (transmission electron mic...
Available to PurchasePublished: 01 December 2006
Fig. 4.29 Dislocation network in undeformed single crystal (transmission electron micrograph of aluminum M = 10,000:1) [ Alt 94 ]
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Image
Formation of dislocation image in wafer-thin specimen by transmission elect...
Available to PurchasePublished: 01 March 2006
Fig. 10.7 Formation of dislocation image in wafer-thin specimen by transmission electron microscope. Source: Ref 10.11
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Image
Use of transmission electron microscopy to observe formation of substructur...
Available to PurchasePublished: 01 March 2006
Fig. 10.9 Use of transmission electron microscopy to observe formation of substructure in aluminum; total strain range = 0.004, life ≈ 500,000 cycles. Source: Ref 10.12
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Image
Comparison of fatigue life of induction surface-hardened transmission shaft...
Available to PurchasePublished: 01 August 2015
Fig. 10.3 Comparison of fatigue life of induction surface-hardened transmission shafts with that of through-hardened and carburized shafts. Arrow in lower bar (induction-hardened shafts) indicates that one shaft had not failed after testing for the maximum number of cycles shown. Source: Ref
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Image
Powder forged internal ring gear used in automatic transmission for trucks ...
Available to PurchasePublished: 01 September 2005
Fig. 17 Powder forged internal ring gear used in automatic transmission for trucks of up to 22,700 kg (50,000 lb) gross vehicle weight. Courtesy of Precision Forged Products Division, Borg Warner Corp.
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Image
Transmission electron micrographs showing retained austenite stringers betw...
Available to PurchasePublished: 01 December 1996
Fig. 5-54 Transmission electron micrographs showing retained austenite stringers between the martensite laths. (From J.P Materkowski and G. Krauss, Met. Trans ., Vol 10A, p 1643 (1979), Ref 25 )
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Image
Transmission electron micrograph (dark field) showing fine Nb carbonitrides...
Available to PurchasePublished: 01 December 1996
Fig. 8-41 Transmission electron micrograph (dark field) showing fine Nb carbonitrides (white) in a 0.15% Nb steel. (From G. Gauthier and A.B. LeBon, MicroAlloying 75 , Union Carbide Corporation, New York, p 73 (1975), Ref 18 )
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Image
Moduli of reflectance and transmission vs. the angle of incidence at a flui...
Available to Purchase
in Acoustic Microscopy of Semiconductor Packages
> Microelectronics Failure Analysis: Desk Reference
Published: 01 November 2019
Figure 15 Moduli of reflectance and transmission vs. the angle of incidence at a fluid - solid interface. Fluid: water @ 21°C. Solid: fused silica.
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Image
in Acoustic Microscopy of Semiconductor Packages
> Microelectronics Failure Analysis: Desk Reference
Published: 01 November 2019
Figure 25 The corresponding through-transmission image for the package in Fig. 24 . The 16 solder balls beneath the die are evident, as is the weave pattern in the substrate. Three small delaminations are shown in this image (arrows).
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Image
Representation of the current standing-wave (red) formed in a transmission ...
Available to Purchase
in Magnetic Field Imaging for Electrical Fault Isolation[1]
> Microelectronics Failure Analysis: Desk Reference
Published: 01 November 2019
Figure 6 Representation of the current standing-wave (red) formed in a transmission line due to the superposition of the signals incident onto (blue), and reflected from (green) the open boundary. N and AN indicate the nodes and antinodes, respectively.
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Image
Signal path loss over transmission length (plotted from path loss equation ...
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in Fault Isolation Using Time Domain Reflectometry, Electro Optical Terahertz Pulse Reflectometry and Time Domain Transmissometry
> Microelectronics Failure Analysis: Desk Reference
Published: 01 November 2019
Figure 9 Signal path loss over transmission length (plotted from path loss equation ( L = 10 * log 10 (4π d /λ)) [11] .
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Image
Published: 01 November 2019
Figure 1 Transmission of light as a function of varying Si thickness [5] .
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Image
IR transmission of 625 μm of p-doped Si with doping concentration x 1016 cm...
Available to PurchasePublished: 01 November 2019
Figure 3 IR transmission of 625 μm of p-doped Si with doping concentration x 1016 cm -3 of (a) 1.5, (b) 33, (c) 120, (d) 730.
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Image
Spectral sensitivity of PEM detectors and silicon transmission for 10μm and...
Available to Purchase
in Photon Emission in Silicon Based Integrated Circuits
> Microelectronics Failure Analysis: Desk Reference
Published: 01 November 2019
Figure 12 Spectral sensitivity of PEM detectors and silicon transmission for 10μm and 100μm thickness; after [8] .
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