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Series: ASM Technical Books
Publisher: ASM International
Published: 30 September 2024
DOI: 10.31399/asm.tb.pmamfa.t59400073
EISBN: 978-1-62708-479-6
... Abstract This chapter provides an overview of sintering techniques and the microstructures and properties that can be achieved in different material systems. It covers conventional furnace sintering, microwave and laser sintering, hot and hot-isostatic pressing, and spark plasma sintering...
Abstract
This chapter provides an overview of sintering techniques and the microstructures and properties that can be achieved in different material systems. It covers conventional furnace sintering, microwave and laser sintering, hot and hot-isostatic pressing, and spark plasma sintering. It describes the advantages and disadvantages of each method, the mechanisms involved, and the effect of sintering parameters on the density, grain size, and mechanical properties of titanium and tungsten heavy alloys, stainless steel, cemented carbides, ceramics, composites, and rare earth magnets.
Series: ASM Technical Books
Publisher: ASM International
Published: 30 September 2024
DOI: 10.31399/asm.tb.pmamfa.t59400115
EISBN: 978-1-62708-479-6
... Abstract This chapter describes how forces and temperatures generated during sintering influence particle bonding, grain growth, shrinkage, and densification as well as bulk material properties. It explains how density, a good predictor of mechanical and electrical properties, can be controlled...
Abstract
This chapter describes how forces and temperatures generated during sintering influence particle bonding, grain growth, shrinkage, and densification as well as bulk material properties. It explains how density, a good predictor of mechanical and electrical properties, can be controlled by proper selection of sintering time, temperature, and particle size for various steels, ceramics, and tungsten and titanium alloys.
Book Chapter
Series: ASM Technical Books
Publisher: ASM International
Published: 30 April 2020
DOI: 10.31399/asm.tb.bpapp.t59290169
EISBN: 978-1-62708-319-5
... Abstract After shaping and first-stage binder removal, the component (with remaining backbone binder) is heated to the sintering temperature. Further heating induces densification, evident as dimensional shrinkage, pore rounding, and improved strength. This chapter begins with a discussion...
Abstract
After shaping and first-stage binder removal, the component (with remaining backbone binder) is heated to the sintering temperature. Further heating induces densification, evident as dimensional shrinkage, pore rounding, and improved strength. This chapter begins with a discussion on the events that are contributing to sintering densification, followed by a discussion on the driving forces, such as surface energy, and high-temperature atomic motion as well as the factors affecting these processes. The process of microstructure evolution in sintering is then described, followed by a discussion on the tools used for measuring bulk properties to monitor sintering and density. The effects of key parameters, such as particle size, oxygen content, sintering atmosphere, and peak temperature, on the sintered properties are discussed. Further, the chapter covers sintering cycles and sintering practices adopted as well as provides information on dimensional control and related concerns of sintering. Cost issues associated with sintering are finally covered.
Book Chapter
Series: ASM Technical Books
Publisher: ASM International
Published: 01 June 2007
DOI: 10.31399/asm.tb.pmsspmp.t52000059
EISBN: 978-1-62708-312-6
... Abstract This chapter discusses the sintering process for stainless steel powders and its influence on corrosion resistance. It begins with a review of sintering furnaces and atmospheres and the effect of temperature and density on compact properties such as conductivity, ductility...
Abstract
This chapter discusses the sintering process for stainless steel powders and its influence on corrosion resistance. It begins with a review of sintering furnaces and atmospheres and the effect of temperature and density on compact properties such as conductivity, ductility, and strength. It then describes the relationship between sintered density and corrosion resistance and how it varies for different types of powders and operating environments. The chapter also explains how stainless steel powders respond to different sintering atmospheres, including hydrogen, hydrogen-nitrogen, and vacuum, and liquid-phase sintering processes.
Series: ASM Technical Books
Publisher: ASM International
Published: 01 June 2007
DOI: 10.31399/asm.tb.pmsspmp.t52000101
EISBN: 978-1-62708-312-6
... Abstract This chapter describes the most effective ways to improve the corrosion resistance of sintered stainless steels, including increasing alloy content, optimizing the sintering process, and the use of surface treatments and modifications. alloying element corrosion resistance...
Abstract
This chapter describes the most effective ways to improve the corrosion resistance of sintered stainless steels, including increasing alloy content, optimizing the sintering process, and the use of surface treatments and modifications.
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Published: 01 November 2013
Fig. 25 Sintering process. (a) Schematic of sintering. (b) Scanning electron micrographs of the neck formation due to sintering. The spheres (33 μm diam) were sintered at 1030 °C for 30 min in vacuum. Courtesy of Randall M. German, The Pennsylvania State University. Source: Ref 11
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Published: 30 April 2020
Fig. 8.27 Micrographs of tungsten during sintering. (a) Initial-stage sintering, with considerable residual porosity and small bonds between the particles. (b) Intermediate-stage sintering, where the pores are rounded and highly connected. (c) and (d) Final-stage sintering, with residual pores
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Published: 01 December 1995
Fig. 2-115 Sintering pallet with grate bars for sintering ore and fluxes for the blast furnace. Width of pallet, 6 ft (1.8 m). The grate bars of heat resistant cast steel are cast separately.
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Published: 01 October 2012
Fig. 10.8 Diagram of a section through a free surface at (a) the sintering temperature. On cooling, particles of ZrO 2 near the surface (b) transform due to reduced constraint, developing a compressive stress in the matrix. The thickness of this compressively stressed layer can be increased
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Published: 01 October 2012
Fig. 10.20 Progressive densification and grain growth at several stages of sintering. (a) Initial stage. (b) Intermediate stage. (c) Final stage. (d) Fracture surface. The fracture surface micrograph shows the desirable placement of spherical pores on grain boundaries in the final stage
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Published: 01 April 2013
Fig. 4 Poor degree of sintering in P/M compact, unetched. Source: Ref 2
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Published: 01 July 2009
Fig. 19.16 Effects of time and temperature during pressureless sintering on the ultimate tensile strengths of +200-mesh beryllium powder (powder lot Y.9833, 1B). Source: Reeves and Keeley 1961
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Published: 01 July 2009
Fig. 22.31 Effect of sintering temperature on electrical conductivity of plasma-sprayed beryllium. Source: Dunmur 1979
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in Compacting and Shaping
> Powder Metallurgy Stainless Steels: Processing, Microstructures, and Properties
Published: 01 June 2007
Fig. 4.13 Schematic representation of the effects of green density, sintering temperature, and sintering time on sintered density. Source: Ref 15 . Reprinted with permission from MPIF, Metal Powder Industries Federation, Princeton, NJ
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in Sintering and Corrosion Resistance
> Powder Metallurgy Stainless Steels: Processing, Microstructures, and Properties
Published: 01 June 2007
Fig. 5.2 Variation in compact properties with degree of sintering, as represented by sintering temperature. Source: Ref 2 . Reprinted with permission from MPIF, Metal Powder Industries Federation, Princeton, NJ
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in Sintering and Corrosion Resistance
> Powder Metallurgy Stainless Steels: Processing, Microstructures, and Properties
Published: 01 June 2007
Fig. 5.30 Redox curves and sintering scenarios for 316L in H 2 at atmospheric pressure (schematic). Source: Ref 19 . Reprinted with permission from MPIF, Metal Powder Industries Federation, Princeton, NJ
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in Sintering and Corrosion Resistance
> Powder Metallurgy Stainless Steels: Processing, Microstructures, and Properties
Published: 01 June 2007
Fig. 5.54 Effect of sintering temperature and graphite addition on (a) corrosion resistance and (b) carbon and oxygen content of vacuum-sintered 316L (green densities: 6.6 g/cm 3 ; cooling rate: 30 °C/min, or 54 °F/min). Reprinted with permission from MPIF, Metal Powder Industries Federation
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Published: 30 April 2020
Fig. 1.3 Cylinder showing distortion after sintering. Initially, the top and bottom diameters were the same, but substrate friction retarded sintering shrinkage at the bottom.
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Published: 30 April 2020
Fig. 8.7 Sintered density for a 40 μm prealloyed tool steel powder versus sintering temperature, showing how supersolidus liquid-phase sintering acts over a narrow temperature range. Source: German et al. ( Ref 2 )
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