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optical emission spectroscopy

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Series: ASM Technical Books
Publisher: ASM International
Published: 01 December 2018
DOI: 10.31399/asm.tb.fibtca.t52430107
EISBN: 978-1-62708-253-2
... Abstract This chapter describes some of the most effective tools for investigating boiler tube failures, including scanning electron microscopy, optical emission spectroscopy, atomic absorption spectroscopy, x-ray fluorescence spectroscopy, x-ray diffraction, and x-ray photoelectron...
Book Chapter

Series: ASM Technical Books
Publisher: ASM International
Published: 01 April 2013
DOI: 10.31399/asm.tb.imub.t53720139
EISBN: 978-1-62708-305-8
... Abstract The overall chemical composition of metals and alloys is most commonly determined by x-ray fluorescence (XRF) and optical emission spectroscopy (OES). High-temperature combustion and inert gas fusion methods are typically used to analyze dissolved gases (oxygen, nitrogen, and hydrogen...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 November 2019
DOI: 10.31399/asm.tb.mfadr7.t91110180
EISBN: 978-1-62708-247-1
... Abstract Photon emission (PE) is one of the major optical techniques for contactless isolation of functional faults in integrated circuits (ICs) in full electrical operation. This article describes the fundamental mechanisms of PE in silicon based ICs. It presents the opportunities...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 November 2007
DOI: 10.31399/asm.tb.smnm.t52140201
EISBN: 978-1-62708-264-8
... color bands, it appears white to the human eye. Also, human eyes can only see light having wavelengths over a relatively narrow range, generally referred to as the optical range. Light with wavelengths slightly larger than this range is called infrared light, while light with wavelengths shorter...
Book Chapter

Series: ASM Technical Books
Publisher: ASM International
Published: 01 December 2003
DOI: 10.31399/asm.tb.cfap.t69780383
EISBN: 978-1-62708-281-5
... (the Auger parameter) has been used for refined chemical-state identification. Fig. 7 Low-resolution x-ray photoelectron spectroscopy spectrum of an ethylene-chlorotrifluoroethylene copolymer Fig. 8 Orbital energy level diagrams. (a) Photoelectron emission. (b) Auger relaxation High...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 January 2000
DOI: 10.31399/asm.tb.cub.t66910475
EISBN: 978-1-62708-250-1
... with an eyedropper. Bulk Material Analysis Various analytical techniques can be used to determine elemental concentrations and to identify compounds in alloys, bulky deposits, and samples of environmental fluids, lubricants, and suspensions. Techniques such as emission spectroscopy, atomic absorption...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 December 2018
DOI: 10.31399/asm.tb.fibtca.t52430149
EISBN: 978-1-62708-253-2
... nature of the failure, as indicated in Fig. 6.33(a) and (b) . Fig. 6.33 Enlarged views of the fracture surface indicating brittle nature of failure, (a) 8×, and (b) 13× Chemical analysis of the tube material by optical emission spectroscopy revealed that it did not meet the requirements...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 November 2019
DOI: 10.31399/asm.tb.mfadr7.t91110010
EISBN: 978-1-62708-247-1
... if the material is not commonly found in integrated circuits. Figure 10 and Figure 11 respectively show the Scanning Electron image and material composition identified using Energy Dispersive Spectroscopy of the contaminant observed during optical inspection in Figure 1 . Contaminant material...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 November 2019
DOI: 10.31399/asm.tb.mfadr7.t91110563
EISBN: 978-1-62708-247-1
... Emission Spectroscopy) is also useful. A number of things to consider on EDS of particles on MEMS: Particles can charge up and jump away. Coating the sample can help reduce this. Doing EDS mapping can also help: in mapping, the electron beam does not sit on the particle all the time, allowing...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 November 2019
DOI: 10.31399/asm.tb.mfadr7.t91110673
EISBN: 978-1-62708-247-1
..., and an optical microscope. More subtle problems required a scanning electron microscope (SEM) and possibly energy dispersive spectroscopy (EDS). The investment in failure analysis tools was modest. $250,000 bought all of the tools that were necessary to do most any analysis job. More importantly, the investment...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 June 2016
DOI: 10.31399/asm.tb.hpcspa.t54460121
EISBN: 978-1-62708-285-3
... coatings. The techniques covered are optical microscopy, X-Ray diffraction, scanning electron microscopy, focused ion beam machining, electron probe microanalysis, transmission electron microscopy, and electron backscattered diffraction. The techniques also include electron channeling contrast imaging, X...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 October 2005
DOI: 10.31399/asm.tb.faesmch.t51270019
EISBN: 978-1-62708-301-0
... elements and organic functional groups; accessible range, 0.001 to 50%; accuracy, 2 to 5% Atomic absorption spectrometry: Applicable to practically all elements; accessible range, 0.001 to 10%; accuracy, 2 to 5% Emission spectroscopy: Applicable to all elements; accessible range, 0.005 to 10...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 November 2019
DOI: 10.31399/asm.tb.mfadr7.t91110413
EISBN: 978-1-62708-247-1
..., electron beam testing, and charge-induced voltage alternation (CIVA) are covered in a separate chapters. Principles of Operation SEM/Optical Comparison It is always a good idea to inspect a new sample in an optical microscope before putting it into a SEM. The SEM has much higher resolution...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 November 2019
DOI: 10.31399/asm.tb.mfadr7.t91110447
EISBN: 978-1-62708-247-1
... six methods used in semiconductor industry are: Auger spectroscopy, dynamic secondary ion mass spectroscopy, time of flight static secondary ion mass spectroscopy (ToF-SIMS), X-ray photoelectron spectroscopy, scanning electron microscope-energy dispersive X-ray spectroscopy (SEM-EDX), and transmission...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 November 2019
DOI: 10.31399/asm.tb.mfadr7.t91110001
EISBN: 978-1-62708-247-1
... to further pinpoint the exact fail location or characterize the defect. The final step involves inspecting the defect using high-resolution scanning electron microscopes and spectroscopy to determine the failure root cause. Although this FA process flow works well in general, it does not differentiate...
Series: ASM Technical Books
Publisher: ASM International
Published: 23 January 2020
DOI: 10.31399/asm.tb.stemsem.t56000020
EISBN: 978-1-62708-292-1
.../S1431927616001100 16. N. Brodusch, et al., Electron Energy-Loss Spectroscopy (EELS) with a Cold-Field Emission Scanning Electron Microscope at Low Accelerating Voltage in Transmission Mode, Ultramicroscopy, Vol 203, 2019, p 21 36. httpsdoi.org/10.1016/j.ultramic.2018.12.015 ...
Series: ASM Technical Books
Publisher: ASM International
Published: 23 January 2020
DOI: 10.31399/asm.tb.stemsem.9781627082921
EISBN: 978-1-62708-292-1
Series: ASM Technical Books
Publisher: ASM International
Published: 01 November 2019
DOI: 10.31399/asm.tb.mfadr7.t91110461
EISBN: 978-1-62708-247-1
... information about the defect. Various elemental analysis techniques, namely energy dispersive spectroscopy, electron energy loss spectroscopy, and energy-filtered TEM, are described using examples encountered in failure analysis. The origin of different image contrast mechanisms, their interpretation...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 November 2019
DOI: 10.31399/asm.tb.mfadr7.t91110524
EISBN: 978-1-62708-247-1
..., where the diffusion length is typically on the order of 1-2 µm. Inside this area, DLDs grow extremely quickly, typically about 1 µm every few minutes. Outside this area, DLD growth is believed to progress by an entirely different mechanism. Spontaneous emission from the emitting area optically excites...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 November 2019
DOI: 10.31399/asm.tb.mfadr7.t91110219
EISBN: 978-1-62708-247-1
... distribution in relation to the focus position. In order to correlate the measured thermal emissions to a spot size, Gaussian fitting functions in combination with the pixel size and an optical magnification factor was conducted. Figure 14 shows the estimated lateral extents of the hot spot...