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Book Chapter
Finishing, Heat Treatment and Inspection
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 December 1995
DOI: 10.31399/asm.tb.sch6.t68200197
EISBN: 978-1-62708-354-6
..., abrasive blast cleaning, removal of risers, ingates, and discontinuities, rough inspection, removal of discontinuities, finishing welding, heat treatment, and final visual, dimensional, and NDT inspection. This chapter provides a detailed discussion on these activities. finishing heat treatment...
Abstract
After pouring, castings are allowed to solidify and cool. They are later removed from the molds in the shakeout operation. A series of activities then follow, which are generally referred to as finishing and heat treatment. These activities can be broadly categorized as shakeout, abrasive blast cleaning, removal of risers, ingates, and discontinuities, rough inspection, removal of discontinuities, finishing welding, heat treatment, and final visual, dimensional, and NDT inspection. This chapter provides a detailed discussion on these activities.
Book Chapter
Cross-Sectioning: Scribing and Cleaving
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 November 2019
DOI: 10.31399/asm.tb.mfadr7.t91110402
EISBN: 978-1-62708-247-1
... of microns to millimeters long, mechanical polishing is generally the optimal method for sample preparation. However, if the stack is primarily of non-metals, cleaving is the fastest option for viewing large regions of more than approximately 50-60 μm in length. Samples coated with photoresist, however...
Abstract
Cross-sectioning refers to the process of exposing the internal layers and printed devices below the surface by cleaving through the wafer. This article discusses in detail the steps involved in common cross-sectioning methods. These include sample preparation, scribing, indenting, and cleaving. The article also provides information on options for mounting, handling, and cleaning of samples during and after the cleaving process. The general procedures, tools required, and considerations that need to be taken into account to perform these techniques are considered.
Book Chapter
Cross-Sectioning: Mechanical Polishing, Ion Milling, and Focused Ion Beam (FIB)
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 November 2019
DOI: 10.31399/asm.tb.mfadr7.t91110391
EISBN: 978-1-62708-247-1
...) device sectioning techniques, non-encapsulated device techniques, utilization of the focused ion beam (FIB) making a cross-section and/or enhancing a physically polished one. Delineation methods for revealing structures are also discussed. These can be chemical etchants, chemo-mechanical polishing...
Abstract
Cross-sectioning is a technique used for process development and reverse engineering. This article introduces novice analysts to the methods of cross-sectioning semiconductor devices and provides a refresher for the more experienced analysts. Topics covered include encapsulated (potted) device sectioning techniques, non-encapsulated device techniques, utilization of the focused ion beam (FIB) making a cross-section and/or enhancing a physically polished one. Delineation methods for revealing structures are also discussed. These can be chemical etchants, chemo-mechanical polishing, and ion milling, either in the FIB or in a dedicated ion mill.
Book Chapter
Extrusion of Hard Alloys
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 March 2000
DOI: 10.31399/asm.tb.aet.t68260187
EISBN: 978-1-62708-336-2
... the outer surface of the billet from sliding, and the undesirable skin of the billet is left in the container as the dummy pad shears metal during its forward stroke. The oxide layer separation and cleaning mechanism are shown schematically in Fig. 1 to 3 . Figure 1 shows that the container has...
Abstract
This chapter discusses the extrusion characteristics of hard aluminum alloys, particularly those in the 5000 and 7000 series. It begins with a review of two studies, one showing how the extrudability of 7 xxx alloys varies with the presence and amount of different alloying elements, the other relating minimum wall thickness with circumscribing circle diameter. It then explains how oxides on either the billet or container complicate the control of extrusion as well as auxiliary processes and how material flow and the movement of trapped gasses in different regions of the extrusion can lead to defects and variations in strength. It also discusses the extrusion of aluminum matrix composites and explains how composite billets are made.
Book Chapter
Introduction to Steel Castings
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 December 1995
DOI: 10.31399/asm.tb.sch6.t68200001
EISBN: 978-1-62708-354-6
...? A steel casting is the product formed by pouring molten steel into a mold cavity. The liquid steel cools and solidifies in the mold cavity and is then removed for cleaning. Heat treating may be required to meet desired properties. This process provides the near net shape and mechanical properties...
Abstract
This chapter defines steel castings, explains when to use steel castings, gives an overview of casting processes, and gives examples of suitable applications for cast steel parts.
Book Chapter
Extrusion of Hard Alloys
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 30 April 2025
DOI: 10.31399/asm.tb.aet2.t59420291
EISBN: 978-1-62708-487-1
... diameter as the dummy/nose pad shears metal during its forward stroke. The oxide layer separation and cleaning mechanism are shown schematically in Fig. 7.3 . Figure 7.3(a) shows that the container has a residual built-up oxide layer before the next billet is loaded. Figure 7.3(b) shows that after...
Abstract
This chapter discusses the extrusion technology of hard alloys. The chapter provides an overview of hollow extrusion for aerospace application. It presents extrusion defects related to hard alloys. The chapter describes the extrusion quality requirements for aerospace applications. It also discusses extrusion of aluminum-matrix composites. The chapter outlines the powder metallurgy process for making billets for extrusion.
Book Chapter
Inspection, Data Collection, and Management
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 December 2015
DOI: 10.31399/asm.tb.cpi2.t55030360
EISBN: 978-1-62708-282-2
... for any signs of distress, corrosion, or cracking Debris found within the vessel prior to cleaning. This may include mechanical items from the vessel or upstream pipe work. Where appropriate, samples of deposit/sludge should be taken for analysis. Internal linings. Blisters in coatings should...
Abstract
This chapter concentrates almost exclusively on inspection techniques related to pressure vessels and pipework. The discussion covers the general aspects associated with inspection and the key factors relevant to it. In addition, the chapter addresses processes involved in data collection and management, namely data acquisition, reporting, trending, reviewing, and auditing. Capabilities and limitations of in-service inspection techniques are discussed in the Appendix to this chapter.
Book Chapter
Screening for Counterfeit Electronic Parts
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 November 2019
DOI: 10.31399/asm.tb.mfadr7.t91110603
EISBN: 978-1-62708-247-1
... inspection followed by material evaluation and characterization. These processes are typically followed by evaluation of the packages to identify defects, degradations, and failure mechanisms that are caused by the processes (e.g., cleaning, solder dipping of leads, reballing) used in creating counterfeit...
Abstract
Most of the counterfeit parts detected in the electronics industry are either novel or surplus parts or salvaged scrap parts. This article begins by discussing the type of parts used to create counterfeits. It discusses the three most commonly used methods used by counterfeiters to create counterfeits. These include relabeling, refurbishing, and repackaging. The article presents a systematic inspection methodology that can be applied for detecting signs of possible part modifications. The methodology consists of external visual inspection, marking permanency tests, and X-ray inspection followed by material evaluation and characterization. These processes are typically followed by evaluation of the packages to identify defects, degradations, and failure mechanisms that are caused by the processes (e.g., cleaning, solder dipping of leads, reballing) used in creating counterfeit parts.
Book Chapter
Commercial and Residential Applications
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 December 2008
DOI: 10.31399/asm.tb.ssde.t52310233
EISBN: 978-1-62708-286-0
... for products related to food, health care, and laundry because it combines strength and durability with an unexcelled ability to be cleaned, disinfected, and sterilized. These qualities have long been apparent to commercial food, laundry, and health care professionals and have increasingly carried over...
Abstract
The case for using stainless steel in appliances of all types, whether they are commercial or residential, relates to it being able to provide the best value over the intended service life. This chapter describes some of the qualities in any material considered for food contact, namely chemical neutrality, biological neutrality, and cleanliness. A vast majority of stainless steel applications in commercial and residential equipment are also discussed.
Book Chapter
2.5D and 3D Packaging Failure Analysis Techniques
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 November 2019
DOI: 10.31399/asm.tb.mfadr7.t91110550
EISBN: 978-1-62708-247-1
... speed milling machine (d) Package after remainder of lid removed and TIM cleaned off Mechanical Cross-Sectioning In order to observe large area defects or the interaction of multiple stacked levels, mechanical cross-sections are often performed. Due to the increased internal stresses present...
Abstract
The complexity of semiconductor chips and their packages has continuously challenged the known methods to analyze them. With larger laminates and the inclusion of multiple stacked die, methods to analyze modern semiconductor products are being pushed toward their limits to support these 2.5D and 3D packages. This article focuses on these methods of fault isolation, non-destructive imaging, and destructive techniques through an iterative process for failure analysis of complex packages.
Series: ASM Technical Books
Publisher: ASM International
Published: 01 June 2022
DOI: 10.31399/asm.tb.tstap.t56040030
EISBN: 978-1-62708-428-4
... stage and head for all stages bar the final oxide polish, for which counter-rotation is preferred. Generally, the polishing time and load are lower than the equivalent grinding parameters to minimize the possibility of any mechanical deformation of the surface. Samples should be cleaned after each step...
Abstract
This article presents best practices for the metallographic preparation of specimens produced via thermal spray coating methods. It outlines typical metallographic preparation process flow, highlighting important considerations for obtaining a clear and representative specimen suitable for characterization via examination techniques, such as optical or electron microscopy. The process flow includes preliminary resin infiltration, sectioning, mounting, grinding, and polishing. To aid in the identification and resolution of common issues during subsequent specimen analysis, the article presents common issues, along with causes and mitigation strategies. It describes the processes involved in the interpretation of the thermal spray coating microstructure.
Book Chapter
Thin Film Deposition Techniques—An Overview
Available to PurchaseBook: Introduction to Thin Film Deposition Techniques: Key Topics in Materials Science and Engineering
Series: ASM Technical Books
Publisher: ASM International
Published: 31 January 2023
DOI: 10.31399/asm.tb.itfdtktmse.t56060001
EISBN: 978-1-62708-440-6
... to solid by mechanical means rather than chemical, virtually any material can be deposited using this process (that said, to sputter a non-conducting material, a radiofrequency potential must be applied to the target; see Ref 3 ). Furthermore, since this technique maintains the target at relatively low...
Abstract
This chapter presents the theory and practice associated with the application of thin films. The first half of the chapter describes physical deposition processes in which functional coatings are deposited on component surfaces using mechanical, electromechanical, or thermodynamic techniques. Physical vapor deposition (PVD) techniques include sputtering, e-beam evaporation, arc-PVD, and ion plating and are best suited for elements and compounds with moderate melting points or when a high-purity film is required. The remainder of the chapter covers chemical vapor deposition (CVD) processes, including atomic layer deposition, plasma-enhanced and plasma-assisted CVD, and various forms of vapor-phase epitaxy, which are commonly used for compound films or when deposit purity is less critical. A brief application overview is also presented.
Book Chapter
Corrosion Prevention Methods
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 August 1999
DOI: 10.31399/asm.tb.caaa.t67870191
EISBN: 978-1-62708-299-0
... Two-phase fluids Temperature Oxidation, scales Heat-transfer effects Molten deposits Condensation and dewpoint Control Surface cleaning and preparation Coatings Cathodic protection Inhibitors Inspection Planned maintenance Source: Ref 1 Design Details...
Abstract
This chapter discusses corrosion prevention methods used with aluminum and its alloys. The methods range from relatively straightforward measures, such as proper handling and storage, to advanced early warning corrosion monitoring systems for military aircraft. The chapter summarizes the basic factors that influence design for corrosion resistance and discusses the use of conversion coatings, organic coatings, porcelain enameling, and electroplating. It also discusses corrosion monitoring methods used in chemical processing and refining industries.
Book Chapter
Basic Understanding of Environment
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 June 1985
DOI: 10.31399/asm.tb.sagf.t63420027
EISBN: 978-1-62708-452-9
... Abstract This chapter provides an overview of environmental factors when studying a gear failure. Environmental factors discussed are lubrication, temperature, and mechanical stability. failure analysis gears lubrication mechanical stability temperature Environment is a set...
Abstract
This chapter provides an overview of environmental factors when studying a gear failure. Environmental factors discussed are lubrication, temperature, and mechanical stability.
Book Chapter
The Joining Environment
Available to PurchaseBook: Principles of Brazing
Series: ASM Technical Books
Publisher: ASM International
Published: 01 August 2005
DOI: 10.31399/asm.tb.pb.t51230105
EISBN: 978-1-62708-351-5
... perfectly clean and remained so throughout the process cycle, enabling the constituents to interact freely so that the filler metal can wet and spread over the component surfaces. However, this situation represents the ideal case because oxides and other nonmetallic species are usually present on surfaces...
Abstract
This chapter discusses joining atmospheres that are used for brazing, along with their advantages and disadvantages. It discusses the processes, advantages, and disadvantages of chemical fluxing, self-fluxing, and fluxless brazing. Information on stop-off compounds that are considered as the antithesis of fluxes is also provided.
Book Chapter
Joining Technology and Practice
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 March 2002
DOI: 10.31399/asm.tb.stg2.t61280149
EISBN: 978-1-62708-267-9
...-(aluminum + titanium) content alloys. The procedures used in welding superalloys depend, to some extent, on the mechanism by which they are strengthened for high-temperature service, that is, whether primarily solid-solution strengthening or primarily precipitation strengthening is employed. Concepts...
Abstract
Superalloys, except those with high aluminum and titanium contents, are welded with little difficulty. They can also be successfully brazed. This chapter describes the welding and brazing processes most often used and the factors that must be considered when making application decisions. It discusses the basic concepts of fusion welding and the differences between solid-solution-hardened and precipitation-hardened wrought superalloys. It addresses joint integrity, design, weld-related cracking, and the effect of grain size, precipitates, and contaminants. It covers common fusion welding techniques, defect prevention, fixturing, heat treatments, and general practices, including the use of filler metals. It also discusses several solid-state welding methods, superplastic forming, and transient liquid phase bonding, a type of diffusion welding process. The chapter includes extensive information on brazing processes, atmospheres, filler metals, and surface preparation procedures. It also includes examples of nickel-base welded components for aerospace use.
Book Chapter
Influential Microstructural Features
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 December 1999
DOI: 10.31399/asm.tb.cmp.t66770099
EISBN: 978-1-62708-337-9
..., the likely cause of variations observed, and their effect on mechanical properties and behaviors. The discussions throughout the chapter are aided by the use of images, diagrams, data plots, and tables. carbon content case-hardened steels grain size metallography microcracking microsegregation...
Abstract
This chapter is a study of the microstructure of case-hardened steels. It explains what can be learned by examining grain size, microcracking, nonmetallic inclusions, and the effects of microsegregation. It identifies information-rich features, describing their ideal characteristics, the likely cause of variations observed, and their effect on mechanical properties and behaviors. The discussions throughout the chapter are aided by the use of images, diagrams, data plots, and tables.
Series: ASM Technical Books
Publisher: ASM International
Published: 01 November 2019
DOI: 10.31399/asm.tb.mfadr7.t91110144
EISBN: 978-1-62708-247-1
.... It also presents a case study illustrating the application of CNC milling to isolate MCM leakage failure. chemical etching CNC machining flat lapping frontside sample preparation laser decap method laser etching mechanical milling multi-chip module plasma reactive ion etching...
Abstract
The orientation of the devices within a package determine the best chosen approach for access to a select component embedded in epoxy both in package or System in Package and multi-chip module (MCM). This article assists the analyst in making decisions on frontside access using flat lapping, chemical decapsulation, laser ablation, plasma reactive ion etching (RIE), CNC based milling and polishing, or a combination of these coupled with optical or electrical endpoint means. This article discusses the general characteristics, advantages, and disadvantages of each of these techniques. It also presents a case study illustrating the application of CNC milling to isolate MCM leakage failure.
Book Chapter
Failures from the Casting Process
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 September 2008
DOI: 10.31399/asm.tb.fahtsc.t51130151
EISBN: 978-1-62708-284-6
... methods, such as casting and machining operations prior to the heat treatment Heat treatment Final finishing operations Mechanical solicitation of the component and the service environment However, it is not a simple task to identify which of these items is responsible for the early failure...
Abstract
This chapter describes cast steel features that may be identified or attributed to component failure during heat treatment or subsequent processing or service, namely porosity (generated by the presence of gas as well as by shrinkage pores), decarburization, cold joint, and inclusions.
Book
Introduction to Thin Film Deposition Techniques: Key Topics in Materials Science and Engineering
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 31 January 2023
DOI: 10.31399/asm.tb.itfdtktmse.9781627084406
EISBN: 978-1-62708-440-6
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