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metallographic examination
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in Case Studies of Steel Component Failures in Aerospace Applications
> Failure Analysis of Heat Treated Steel Components
Published: 01 September 2008
Fig. 14 Metallographic examination of cracks evident in the flange of the main landing gear lever attach pin, showing loss of chromium at cracks (20 μm)
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in Case Studies of Steel Component Failures in Aerospace Applications
> Failure Analysis of Heat Treated Steel Components
Published: 01 September 2008
Fig. 27 Metallographic examination of primary crack. Fracture path followed prior-austenite grain boundaries. No precipitates in grain boundaries (50 μm) were observed.
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Published: 01 July 1997
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in Mechanical Work of Steels—Cold Working
> Metallography of Steels: Interpretation of Structure and the Effects of Processing
Published: 01 August 2018
Fig. 12.52 (a) Metallographic assembly for the examination of a nail. (b) Longitudinal cross section of the nail, showing the edge of the nail head where the “fibers” have been deformed by the forming operation. (c) Transverse cross section of the body of the nail: the fiber orientation gives
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Series: ASM Technical Books
Publisher: ASM International
Published: 01 September 2008
DOI: 10.31399/asm.tb.fahtsc.t51130043
EISBN: 978-1-62708-284-6
... of specimens, mechanical testing, macroexamination, microexamination, metallographic examination, determination of the fracture mechanism, chemical analysis, exemplar testing, and analysis and writing the report. The chapter ends with a discussion on various processes involved in the determination...
Abstract
This chapter provides an overview of the possible mechanisms of failure for heat treated steel components and discusses the techniques for examining fractures, ductile and brittle failures, intergranular failure mechanisms, and fatigue. It begins with a description of the general sources of component failure. This is followed by a section on the stages of a failure analysis, which can proceed one after the other or occur at the same time. These stages of analysis are collection of background data, preliminary visual examination, nondestructive testing, selection and preservation of specimens, mechanical testing, macroexamination, microexamination, metallographic examination, determination of the fracture mechanism, chemical analysis, exemplar testing, and analysis and writing the report. The chapter ends with a discussion on various processes involved in the determination of the fracture mechanism.
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in Overview of the Mechanisms of Failure in Heat Treated Steel Components
> Failure Analysis of Heat Treated Steel Components
Published: 01 September 2008
Fig. 7 Typical metallographic specimen. This specimen was used to examine microstructures in a failed weldment.
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Published: 01 October 2011
Fig. 7.2 Jose Ramon Vilella (1897–1971), distinguished metallographer who understood the need to faithfully prepare representative surfaces in metallographic examinations. Source: Ref 7.1
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Book Chapter
Series: ASM Technical Books
Publisher: ASM International
Published: 01 December 1984
DOI: 10.31399/asm.tb.mpp.t67850541
EISBN: 978-1-62708-260-0
... Abstract This appendix contains recipes of the electrolytic solutions in which various metals are polished in preparation for metallographic examination. electrolyte electromechanical polishing Metallography Principles and Practice George F. Vander Voort, p 541-542 DOI: 10.31399...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 October 2005
DOI: 10.31399/asm.tb.faesmch.t51270130
EISBN: 978-1-62708-301-0
.... The bolts were removed and analyzed to determine the mode and cause of failure. Based on the results of macroscopy, scanning electron fractography, metallographic examination, and chemical analysis, the failures were caused by stress corrosion cracking, and in one case, overtightening. microstructural...
Abstract
An aircraft crashed following the loss of yaw control in full airborne flight. The subsequent discovery of broken shutter bolts in the rear pitch reaction control valve led to an inspection campaign that found bolt failures of a similar nature in valves on several other aircraft. The bolts were removed and analyzed to determine the mode and cause of failure. Based on the results of macroscopy, scanning electron fractography, metallographic examination, and chemical analysis, the failures were caused by stress corrosion cracking, and in one case, overtightening.
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in Mechanical Work of Steels—Cold Working
> Metallography of Steels: Interpretation of Structure and the Effects of Processing
Published: 01 August 2018
Fig. 12.10 Cold working polycrystalline materials will generate anisotropy of the grain shape: their elongation in the deformation direction is evident. Anisotropy increases with cold work. For small deformations (< approx. 10%), this anisotropy may not be observable in the metallographic
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Published: 01 November 2007
Fig. 5.60 Oxide scale and no evidence of metal dusting on the surface of a Multimet alloy fan box exposed to flowing carburizing gas (same fan box as that shown in Fig. 5.59 ). The sample was plated with nickel before mounting for metallographic examination.
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Published: 01 November 2007
Fig. 7.41 Sulfidation resistance of alloy HR160 compared to those of alloys 556, 800H, and 600 after 215 h at 870 °C (1600 °F) in Ar-5H 2 -5CO-1CO 2 -0.15H 2 S ( p O 2 = 3×10 –19 atm, p S 2 = 0.9 × 10 –6 atm). Samples were cathodically descaled before being mounted for metallographic
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Book Chapter
Series: ASM Technical Books
Publisher: ASM International
Published: 01 October 2005
DOI: 10.31399/asm.tb.faesmch.t51270084
EISBN: 978-1-62708-301-0
... that the rim had exerted a very heavy force on this tie-rod before the nut had been sheared off. Fig. CH10.3 Fracture surface of the hub Testing Procedure and Results Metallography and Scanning Electron Fractography To check the quality of the hub material, metallographic examination...
Abstract
An aircraft tire burst while inflating, causing one of the flanges on the wheel hub to fracture. This chapter provides a summary of the investigation along with key findings. It includes images of the damaged hub and describes how various parts failed as the pressure in the tire increased. It explains that the hub material was of good quality under uniform load and that it fractured quickly by cleavage due to the force exerted by the overinflated tire.
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in Conventional Heat Treatment—Basic Concepts
> Metallography of Steels: Interpretation of Structure and the Effects of Processing
Published: 01 August 2018
Fig. 10.95 Steel nitrocarburized at 550 °C (1020 °F) for 5 h. The surface was coated with a chemically deposited layer of hard nickel to preserve it for metallographic examination (indicated as Ni in the figure). The “white layer” is where the formation of high hardness nitrides occur
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Book Chapter
Series: ASM Technical Books
Publisher: ASM International
Published: 01 October 2005
DOI: 10.31399/asm.tb.faesmch.t51270150
EISBN: 978-1-62708-301-0
.... Fig. CH36.5 SEM fractograph of region close to the origin showing inclusions that were analyzed to be rich in silicon Metallography A section from the root was cut and prepared for metallographic examination. It was found to contain a few large silicon-rich inclusions. Discussion...
Abstract
This chapter discusses the failure of a compressor blade in an aircraft engine and explains how investigators determined the cause. Based on visual examination and the results of SEM fractography and chemical analysis, it was concluded that blade failed due to fatigue fracture originating from nonmetallic inclusions in the blade root.
Book Chapter
Series: ASM Technical Books
Publisher: ASM International
Published: 01 October 2005
DOI: 10.31399/asm.tb.faesmch.t51270087
EISBN: 978-1-62708-301-0
..., chromium, titanium, aluminum, iron, and molybdenum ( Fig. CH11.6 ). Metallographic examination of the adjacent blade and a good blade indicated that the microstructures in all of them were similar. Fig. CH11.5 Microstructure of the failed blade Fig. CH11.6 Energy-dispersive spectrum...
Abstract
A turbine blade in an aircraft engine failed, fracturing at the root above the fir tree region. Fractography indicated that a fatigue crack initiated at the trailing edge of the blade and the final fracture occurred when the crack reached critical length. Although the exact cause of crack initiation could not be established, material defects, improper root loading, and high operating temperatures were ruled out. This chapter describes how investigators came to their conclusions and what they learned through visual and SEM examination and qualitative elemental analysis. It includes images of the microstructure and fracture surfaces and explains what some of the details reveal about the failure.
Series: ASM Technical Books
Publisher: ASM International
Published: 01 August 2018
DOI: 10.31399/asm.tb.msisep.t59220667
EISBN: 978-1-62708-259-4
... originating from various sources, as discussed at length in the previous chapters in this book. Metallographic examination must thus carefully consider the position and orientation of the portion of the material to be sampled. Depending on the technique used, the region that will be observed and analyzed may...
Abstract
This chapter provides guidelines for conducting metallographic evaluations and offers suggestions on how to effectively report the results. It explains how the approach depends on the objective of the evaluation, which is usually to measure a structural feature, test a hypothesis, or investigate structure-related effects. The chapter addresses each case, tailoring its guidelines and suggestions accordingly.
Series: ASM Technical Books
Publisher: ASM International
Published: 01 October 2005
DOI: 10.31399/asm.tb.faesmch.t51270133
EISBN: 978-1-62708-301-0
... due to stress-corrosion cracking combined with the effects of inadequate tempering. compressor blades fractography metallographic examination stress corrosion cracking visual examination Summary A blade of the second-stage compressor in an engine fractured in service. The fracture...
Abstract
A second-stage compressor blade in an aircraft engine fractured after 21 h of service. The remaining portion of the blade was removed and examined as were several adjacent blades. Based on the results of SEM fractography, microstructural analysis, and hardness testing, the blade failed due to stress-corrosion cracking combined with the effects of inadequate tempering.
Series: ASM Technical Books
Publisher: ASM International
Published: 01 January 2015
DOI: 10.31399/asm.tb.spsp2.t54410197
EISBN: 978-1-62708-265-5
... curves. The IT diagrams have been produced by metallographic examination of series of specimens held for various times at various temperatures between Ae 3 or A cm and M s . More than a hundred specimens are often required to determine a complete IT diagram for a given steel ( Ref 10.2...
Abstract
Isothermal and continuous cooling transformation (CT) diagrams help users map out diffusion-controlled phase transformations of austenite to various mixtures of ferrite and cementite. This chapter discusses the application as well as limitations of these engineering tools in the context of heat treating eutectoid, hypoeutectoid, and proeutectoid steels. It also provides references to large collections of transformation diagrams and includes several diagrams that plot quenching and hardening transformations as a function of bar diameter.
Series: ASM Technical Books
Publisher: ASM International
Published: 01 September 2008
DOI: 10.31399/asm.tb.fahtsc.t51130351
EISBN: 978-1-62708-284-6
... micrographs of a typical crack. This crack extended through the chromium plating and into the base metal to a depth of approximately 0.25 mm (0.010 in.). There was no visual indication of untempered or over-tempered martensite. Fig. 14 Metallographic examination of cracks evident in the flange...
Abstract
This chapter presents various case histories that illustrate a variety of failure mechanisms experienced by the high-strength steel components in aerospace applications. The components covered are catapult holdback bar, AISI 420 stainless steel roll pin, main landing gear (MLG) lever, inboard flap hinge bolt, nose landing gear piston axle, multiple-leg aircraft-handling sling, aircraft hoist sling, internal spur gear, and MLG axle. In addition, the chapter provides information on full-scale fatigue testing, nondestructive testing, and failure analysis of fin attach bolts.
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