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metallic contaminant removal
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Book Chapter
Cleaning and Finishing
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 March 2002
DOI: 10.31399/asm.tb.stg2.t61280203
EISBN: 978-1-62708-267-9
... for superalloys and how they work. It discusses the effect of metallic contaminants, tarnish, oxide, and scale and how they can be detected and removed. It also discusses chemical and mechanical surface finishing techniques and where they are used, and presents several application examples. finishing...
Abstract
Superalloys are susceptible to damage from a variety of surface contaminants. They may also require special surface finishes for subsequent processing steps such as coating applications. This chapter describes some of the cleaning and finishing procedures that have been developed for superalloys and how they work. It discusses the effect of metallic contaminants, tarnish, oxide, and scale and how they can be detected and removed. It also discusses chemical and mechanical surface finishing techniques and where they are used, and presents several application examples.
Book Chapter
Cleaning and Rust Protection
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 August 2015
DOI: 10.31399/asm.tb.piht2.t55050173
EISBN: 978-1-62708-311-9
... Abstract The surface condition of metals can have a significant effect on the outcome of high-temperature processes and vice versa. This chapter discusses the general cleaning and surface treatment needs of work in-process both before and after induction hardening. It identifies contaminants...
Abstract
The surface condition of metals can have a significant effect on the outcome of high-temperature processes and vice versa. This chapter discusses the general cleaning and surface treatment needs of work in-process both before and after induction hardening. It identifies contaminants and defects associated with various quenchants and processing atmospheres and provides insights on how they can be removed and, in some cases, prevented. It also recommends the application of a rust preventative shortly after parts have cooled.
Book Chapter
Joining Titanium and Its Alloys
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 January 2015
DOI: 10.31399/asm.tb.tpmpa.t54480265
EISBN: 978-1-62708-318-8
... baths. After heavy scale removal, acid pickling is required to ensure removal of all scale and sub-surface contaminated metal. Rinsing and drying treatments also are included in cleaning operations. It is important to protect cleaned surfaces from airborne contamination prior to welding. Edges...
Abstract
This chapter discusses the various methods used to join titanium alloy assemblies, focusing on welding processes and procedures. It explains how welding alters the structure and properties of titanium and how it is influenced by composition, surface qualities, and other factors. It describes several welding processes, including arc welding, resistance welding, and friction stir welding, and addresses related issues such as welding defects, quality control, and stress relieving. The chapter also covers mechanical fastening techniques along with adhesive bonding and brazing.
Book Chapter
Cleaning and Finishing
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 December 2000
DOI: 10.31399/asm.tb.ttg2.t61120085
EISBN: 978-1-62708-269-3
... a liability and a contaminant in postworking cleaning operations. The coatings are soluble and removable if the proper techniques are used. Protective coatings are applied to titanium surfaces during manufacturing operations for several reasons: To lubricate and aid in metal flow, good die...
Abstract
Cleaning procedures serve to remove scale, tarnish films, and other contaminants that form or are otherwise deposited on the surface of titanium during processing operations such as hot working and heat treatment. This chapter explains what makes titanium susceptible to the formation of scale and how it can be removed via belt grinding, abrasive blasting, and molten salt descaling baths. It also discusses the role of acid pickling, barrel finishing, polishing, and buffing as well as the use of chemical conversion coatings and protective platings.
Book Chapter
Corrosion Inhibitors for Crude Oil Refineries
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 December 2015
DOI: 10.31399/asm.tb.cpi2.t55030209
EISBN: 978-1-62708-282-2
... into the crude oil to dissolve salts (primarily chloride salts) for removal by separation of the water in the desalting vessel. Salt is a common contaminant in crude oil due to production and transportation processes. Removal of chloride salts is critical because they hydrolyze to form hydrochloric acid when...
Abstract
This chapter describes various units and process streams that are often susceptible corrosion inhibitors in crude oil refineries, discusses the types and applications of corrosion inhibitors, and provides some information on corrosion monitoring techniques used at refineries.
Book Chapter
Basic Understanding of Environment
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 June 1985
DOI: 10.31399/asm.tb.sagf.t63420027
EISBN: 978-1-62708-452-9
... the most complex. Atmosphere contamination consisting of oxidizing vapors and water vapors tends to oxidize freshly worn surfaces, to break down the oil chemistry, or to set up cells of corrosion on metal surfaces. Liquid contamination may consist of water (which may also be contaminated with gases, acids...
Abstract
This chapter provides an overview of environmental factors when studying a gear failure. Environmental factors discussed are lubrication, temperature, and mechanical stability.
Book Chapter
Corrosion Resistance of Magnesium Alloys
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 December 2015
DOI: 10.31399/asm.tb.cpi2.t55030172
EISBN: 978-1-62708-282-2
...-metal contamination, blast residues, flux inclusions, and galvanic attack. corrosion resistance magnesium alloys chemical composition heat treatment grain size cold working heavy-metal contamination blast residues flux inclusions galvanic attack MAGNESIUM AND MAGNESIUM ALLOYS...
Abstract
This chapter discusses the effects of metallurgical factors on the corrosion resistance of magnesium alloys. The factors are chemical composition, heat treating, grain size, and cold-work effects. The chapter describes the causes of corrosion failures in magnesium alloys, namely heavy-metal contamination, blast residues, flux inclusions, and galvanic attack.
Book Chapter
Inspection of Forgings
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 April 2013
DOI: 10.31399/asm.tb.imub.t53720365
EISBN: 978-1-62708-305-8
... molds, or even the atmosphere itself if steps are not taken to prevent such contamination. The resulting hydrogen goes into solution at elevated temperatures; but as the metal solidifies after pouring, the solubility of hydrogen decreases, and it becomes entrapped in the metal lattice. Hydrogen...
Abstract
In forgings of both ferrous and nonferrous metals, the flaws that most often occur are caused by conditions that exist in the ingot, by subsequent hot working of the ingot or the billet, and by hot or cold working during forging. The inspection methods most commonly used to detect these flaws include visual, magnetic particle, liquid penetrant, ultrasonic, eddy current, and radiographic inspection. This chapter provides a detailed discussion on the characteristics, process steps, applications, advantages, and limitations of these methods. It also describes the flaws caused by the forging operation and the principal factors that influence the selection of a nondestructive inspection method for forgings.
Book Chapter
Surface Finishing
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 December 2008
DOI: 10.31399/asm.tb.ssde.t52310193
EISBN: 978-1-62708-286-0
... to a more soluble oxide without attacking the metal, making it more easily removed by subsequent pickling. Cleaning Stainless steel is very resistant to chemicals of many kinds, permitting it to be cleaned by many aggressive agents. Because contamination is on the surface of stainless rather than...
Abstract
This chapter discusses the functions of surface treatments important for stainless steel, namely the removal of oxide scale and cleaning, brightening, and coloring of the stainless surface. Details on the main methods of producing aesthetic surface finishes are also provided.
Book Chapter
Primary Working
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 January 2015
DOI: 10.31399/asm.tb.tpmpa.t54480207
EISBN: 978-1-62708-318-8
... temperatures practical. Titanium readily seizes and galls and requires thoroughly conditioned surfaces to remove any cracks or contamination that could propagate into the base metal on subsequent processing. In addition, anisotropy (the characteristic of exhibiting different values of a property in different...
Abstract
Most integrated titanium mills have primary working equipment designed specifically for titanium. This chapter describes the forging, rolling, and extruding equipment used to produce titanium mill products and sheds light on the corresponding process, structure, property relationships.
Book Chapter
Direct Chill Ingot and Continuous Casting Processes
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 30 June 2023
DOI: 10.31399/asm.tb.atia.t59340063
EISBN: 978-1-62708-427-7
... in the process are silicon (from dirt), iron (from banding), and titanium (from white pigment on beverage containers). There are no feasible methods to remove these elements from molten aluminum, meaning that the only way to recycle dirty, unsorted scrap is to dilute the contaminants with pure metal, raising...
Abstract
The manufacture of all aluminum wrought products begins with an ingot or a continuous strip solidified from the liquid state. During molten metal processing (MMP), aluminum undergoes a series of operations that are described in this chapter including melting and alloying, recycling, molten metal treatment, control of inclusions, ingot grain refinement, and direct chill (DC) or continuous casting.
Book Chapter
Properties of Refractory Metal Welds
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 July 1997
DOI: 10.31399/asm.tb.wip.t65930353
EISBN: 978-1-62708-359-1
..., and tungsten. Tantalum Alloys Tantalum and its alloys have good weldability, provided the welds and the heated base metal are free from contamination. Carbon, oxygen, nitrogen, and hydrogen all actively react with tantalum, typically forming intermetallics that lead to weld embrittlement. Tantalum also...
Abstract
This article discusses the weldability and fusion weld properties of refractory metal alloys. The alloys discussed include tantalum, niobium, rhenium, molybdenum, and tungsten.
Book Chapter
Maintenance
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 August 2015
DOI: 10.31399/asm.tb.piht2.t55050293
EISBN: 978-1-62708-311-9
... for testing at least once a year to make certain that there has been no deterioration. The five basic causes of contamination in water and polymer quench systems are: Solids contamination , comprising scale and metal particles that collect in the quench tank, should be removed on a continuous basis...
Abstract
This chapter discusses the maintenance needs of major components in induction heat-treating systems, including power supplies, heat stations, capacitors, high-frequency output stages, induction coils, water systems, quench systems, and fixturing.
Book Chapter
Manufacture and Characteristics of Stainless Steel Powders
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 June 2007
DOI: 10.31399/asm.tb.pmsspmp.t52000023
EISBN: 978-1-62708-312-6
... the melt from excessive oxidation. A low manganese content, essential for controlling oxidation during atomization, also keeps the slag from becoming too fluid. Just prior to pouring, the slag is removed and the liquid metal is poured, via a runner, into a preheated tundish. Care must be taken, especially...
Abstract
Stainless steel powders are usually made by water or gas atomization. This chapter describes both processes and the properties and characteristics of the powders they produce. It also discusses secondary processes, including drying, screening, annealing, and lubricating, and the effects of iron contamination on corrosion resistance.
Book Chapter
Role of Water Chemistry in Boiler Tube Failure
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 December 2018
DOI: 10.31399/asm.tb.fibtca.t52430379
EISBN: 978-1-62708-253-2
... pressure, the more critical becomes the removal of impurities from the water. The purity of potable water available for domestic use is far below that required for use in boilers as boiler feedwater (BFW). It is therefore essential to reduce the level of contaminants present in raw water and to add certain...
Abstract
Water chemistry is a factor in nearly all boiler tube failures. It contributes to the formation of scale, biofilms, and sludge, determines deposition rates, and drives the corrosion process. This chapter explains how water chemistry is managed in boilers and describes the effect of impurities and feedwater parameters on high-pressure boiler components. It discusses deposition and scaling, types of corrosion, and carryover, a condition that occurs when steam becomes contaminated with droplets of boiler water. The chapter also covers water treatment procedures, including filtration, chlorination, ion exchange, demineralization, reverse osmosis, caustic and chelant treatment, oxygen scavenging, and colloidal, carbonate, phosphate, and sodium aluminate conditioning.
Book Chapter
Joining Technology and Practice
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 December 2000
DOI: 10.31399/asm.tb.ttg2.t61120065
EISBN: 978-1-62708-269-3
.... An acetone-soaked, lint-free cloth serves to remove surface contamination caused by the die lubricant used in the wire drawing operation, in addition to cleaning the filler wire. Pickling in nitric-hydrofluoric acid solution is also used for cleaning. If the iron content of weld metal is above about 0.05...
Abstract
This chapter covers the welding characteristics of titanium along with the factors that determine which welding method is most appropriate for a given application. It discusses the joinability of titanium alloys, the effect of heat on microstructure, the cause of various defects, and the need for contaminant-free surfaces and atmospheres. It describes common forms of fusion, arc, and solid-state welding along with the use of filler metals, shielding gases, and stress-relief treatments. It also discusses the practice of titanium brazing and the role of filler metals.
Book Chapter
Failure of a Sealed Ball Bearing
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 October 2005
DOI: 10.31399/asm.tb.faesmch.t51270197
EISBN: 978-1-62708-301-0
... Abstract One of the rotor bearings in an electric motor failed, producing excessive vibrate. The bearing was removed and disassembled, revealing craters and bruises on the inner ring raceway and balls along with evidence of melting and burning of metal. Scanning electron microscopy revealed...
Abstract
One of the rotor bearings in an electric motor failed, producing excessive vibrate. The bearing was removed and disassembled, revealing craters and bruises on the inner ring raceway and balls along with evidence of melting and burning of metal. Scanning electron microscopy revealed metal particles near the craters, and energy-dispersive x-ray analysis showed that slivers recovered from the grease had the same composition as the bearing raceway and balls. Based on these observations, it was concluded that the bearing failed due to electrostatic discharge, which would have led to seizure if it continued. The report recommends the use of electrically conductive grease and proper grounding practices.
Book Chapter
The Influence and Control of Porosity and Inclusions in Aluminum Castings
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.tb.aacppa.t51140047
EISBN: 978-1-62708-335-5
... and, in the latter case, affects the efficiency of hydrogen removal. Moisture in any form: contamination on tools, flux tubes, ingot, scrap, metallurgical metals, grain refiners, and master alloys that may be added to the heat additively affect dissolved hydrogen content up to the applicable solubility limit...
Abstract
Porosity in aluminum is caused by the precipitation of hydrogen from liquid solution or by shrinkage during solidification, and more usually by a combination of these effects. Nonmetallic inclusions entrained before solidification influence porosity formation and mechanical properties. This chapter describes the causes and control of porosity and inclusions in aluminum castings as well as the combined effects of hydrogen, shrinkage, and inclusions on the properties of aluminum alloys. In addition, it discusses the applications of radiography to reveal internal discontinuities in aluminum.
Series: ASM Technical Books
Publisher: ASM International
Published: 01 June 2022
DOI: 10.31399/asm.tb.tstap.t56040030
EISBN: 978-1-62708-428-4
..., it is important not to induce too much stress during the sectioning and mounting steps. This may be achieved by use of appropriate cutting wheels, ideally a metal-bonded diamond wheel; these provide rapid and effective material removal with less force and heating generated in the surrounding material, which may...
Abstract
This article presents best practices for the metallographic preparation of specimens produced via thermal spray coating methods. It outlines typical metallographic preparation process flow, highlighting important considerations for obtaining a clear and representative specimen suitable for characterization via examination techniques, such as optical or electron microscopy. The process flow includes preliminary resin infiltration, sectioning, mounting, grinding, and polishing. To aid in the identification and resolution of common issues during subsequent specimen analysis, the article presents common issues, along with causes and mitigation strategies. It describes the processes involved in the interpretation of the thermal spray coating microstructure.
Book Chapter
Cross-Sectioning: Scribing and Cleaving
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 November 2019
DOI: 10.31399/asm.tb.mfadr7.t91110402
EISBN: 978-1-62708-247-1
... polishing generally involves mounting a sample on a polishing block using hot wax and grinding into the cross-section through the target area of interest, followed by use of polishing media to clean and remove scratches from the metal structures to be analyzed. This process is discussed in detail in [9...
Abstract
Cross-sectioning refers to the process of exposing the internal layers and printed devices below the surface by cleaving through the wafer. This article discusses in detail the steps involved in common cross-sectioning methods. These include sample preparation, scribing, indenting, and cleaving. The article also provides information on options for mounting, handling, and cleaning of samples during and after the cleaving process. The general procedures, tools required, and considerations that need to be taken into account to perform these techniques are considered.
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