There is a fairly wide variety of different tool steels for different applications. The American Iron and Steel Institute (AISI) classification of tool steels includes seven major categories: water-hardening tool steels, shock-resisting tool steels, cold work tool steels, hot work tool steels, low-alloy special-purpose tool steels, mold tool steels, high-speed tool steels, and powder metallurgy tool steels. This chapter provides discusses the manufacturing process, composition, properties, types, and applications of these tool steels and other cutting tool materials, such as cemented carbides. It also describes the methods of applying coatings to cutting tools to improve tool life.

This appendix contains tables listing the composition of austenitic, ferrite, martensitic, precipitation-hardenable, and duplex stainless steels and of Alloy Casting Institute heat- and corrosion-resisting casting alloys.

This chapter provides an overview of the microstructure-property relationships associated with aluminum-silicon alloys. It includes information on commercial designations and grades, phase compositions, solidification paths, alloying elements, and intermetallic phases. It also provides solubility data and maps out the topics covered in subsequent chapters in the book.

This chapter serves as a study and guide on the main phase constituents of cast aluminum-silicon alloys, alpha-Al solid solution and Si crystals. The first section focuses on the structure of Al-Si castings in the as-cast state, covering the morphology of the alpha-Al solid solution grains and the process by which they form. It describes how cooling rates, temperature gradients, and local concentrations influence the topology of the crystallization front, and how they play a role in determining the morphology and dispersion degree of the grains observed in cross sections of cast parts. It also describes the mechanism behind dendritic grain crystallization and how factors such as surface tension, capillary length, and lattice symmetry affect dendritic arm size and spacing. The section that follows examines the morphology of the silicon crystals that form in aluminum-silicon castings and its effect on properties and processing characteristics. It discusses the faceted nature of primary Si crystals and the modification techniques used to optimize their shape. It also describes the morphology of the (alpha-Al + Si) eutectic, which can be lamellar or rodlike in shape, and explains how it can be modified through temperature control or alloy additions to improve properties such as tensile strength and plasticity and reduce shrinkage.

Structurally differentiated intermetallic phases are important constituents in the microstructure of aluminum alloys, with the potential to influence properties, behaviors, and processing characteristics. These phases can form in aluminum-silicon alloys with transition metals (Fe, Mn, Ni, Cr, V, Ti) and with metals such as Mg and Cu. This chapter is a compilation of phase diagrams, microstructure images, and tables, providing information on more than 30 binary, ternary, and quaternary alloy systems associated with intermetallic phases in aluminum-silicon castings. Each section includes tabular information and data on the intermetallic phases in the aluminum corner of the equilibrium phase diagram, the characteristics of the crystal lattice of intermetallic phases, the chemical composition of the alloy intermetallic phases, and equilibrium reactions in the alloy system.

This chapter is an atlas of microstructures observed in AlSi7Mg, AlSi11, and Al21CuNiMg modified with either eutectic (strontium, sodium) or hypereutectic (phosphorus) silicon crystals. The microstructure images reveal the as-cast state of gravity castings made in sand and metal molds, before and after modification. The chapter also provides composition data and includes callouts identifying various phase constituents in the interdendritic eutectic microstructure.

Intermetallic phase precipitates in aluminum alloys can often be identified without resorting to chemical analysis. Very often the determination can be made based on the shape, color, and refractive properties of the particular phase. This chapter explains how these visual attributes can be observed using metallographic techniques. It describes, and in many cases illustrates, the characteristic shapes, colors, and optical properties associated with aluminum alloy intermetallic phases and how they can be enhanced through selective etching. It provides an atlas of microstructures comparing the effects of selective etching procedures on various phase constituents in cast aluminum-silicon alloys. The compilation of images demonstrates the use of two types of reagents: those that reveal discontinuities in crystal orientation and grain boundaries, and those that reveal differences in chemical composition.

The scanning acoustic microscope (SAM) is an important tool for development of improved molded and flip chip packages. The SAM used for integrated circuit inspection is a hybrid instrument with characteristics of both the Stanford SAM and the C-scan recorder. This chapter presents the historical development of SAM for integrated circuit package inspection, SAM theory, and analysis considerations. Case studies are presented to illustrate the practical applications of SAM. Other non-destructive imaging tools are briefly discussed, as well as SAM challenges and methods including spectral signature analysis and GHz-SAM.

This chapter describes three approaches for 3D hot-spot localization of thermally active defects by lock-in thermography (LIT). In the first section, phase-shift analysis for analyzing stacked die packages is performed. The second example employs defocusing sequences for the localization of resistive electrical shorts in 3D architectures, and the third operates in cross sectional LIT mode to investigate defects in the insulation liner of Through Silicon Vias. All three approaches allow for a precise localization of thermally active defects in all three spatial dimensions to guide subsequent high-resolution physical analyses.

This chapter provides a comprehensive overview over all phenomena related to Voltage Contrast (VC) mechanisms in SEM and FIB. The multiple advantages, possibilities, and limits of active and passive VC failure localization are systemized and discussed. The knowledge of all facts influencing the VC generation (capacitance, leakage, doping, and circuitry) is very helpful for successful failure localization.

This article presents six case studies of failures with steel forgings. The case studies covered are crankshaft underfill; tube bending; spade bit; trim tear; upset forging; and avoidance of flow through, lap, and crack. The case studies illustrate difficulties encountered in either cold forging or hot forging in terms of preforge factors and/or discontinuities generated by the forging process. Supporting topics that are discussed in the case studies include validity checks for buster and blocker design, lubrication and wear, mechanical surface phenomenon, forging process design, and forging tolerances. Wear, plastic deformation processes, and laws of friction are introduced as a group of subjects that have been considered in the case studies.

This chapter discusses the factors that must be considered when selecting a lubricant for sheet metal forming operations. It begins with a review of lubrication regimes and friction models. It then describes the selection and use of sheet metal forming lubricants, explaining how they are applied and removed and how their pressure and temperature ranges can be extended by performance enhancing additives. The chapter also explains how sheet metal forming lubricants are evaluated in the laboratory as well as on the production floor and how tribological tests are conducted to simulate stamping, deep drawing, ironing, and blanking operations.

This chapter begins with a review of the mechanics of bending and the primary elements of a bending system. It examines stress-strain distributions defined by elementary bending theory and explains how to predict stress, strain, bending moment, and springback under various bending conditions. It describes the basic principles of air bending, stretch bending, and U- and V-die bending as well as rotary, roll, and wipe die bending, also known as straight flanging. It also discusses the steps involved in contour (stretch or shrink) flanging, hole flanging, and hemming and describes the design and operation of press brakes and other bending machines.

This appendix provides information on organizations that issue specifications and standards related to titanium and its alloys.

This appendix includes selected references on topics related to the production and application of superalloys, including properties and microstructure; melting/ingot breakdown; forging/powder metallurgy; machining, heat treating, joining, refurbishment/repair; investment casting; coatings/corrosion; and modeling.

Stainless steels have a wide variety of applications for household products, food-handling equipment, major appliances, medical equipment, and industrial equipment. Stainless is also featured in many architectural designs and monuments. Many of the most important applications of stainless steel can be found in the transportation industry, where both the cutlery martensitic and the chromium-nickel austenitic stainless steels have been used. This chapter provides a detailed discussion on these applications.

This chapter covers the biographies and literary and research work of pioneers in metals research, namely Henry Marion Howe, Albert Sauveur, Isaiah (Zay) Jeffries, Paul Dyer Merica, Edgar C. Bain, Samuel Leslie Hoyt, and Francis L. VerSnyder.

This chapter presents the early classes of stainless steel. These include martensitic alloys, austenitic alloys, and ferritic alloys. It also presents stainless steel trade names. The chapter describes standardized designation for type 304 stainless steel by various specification organizations.

Corrosion can be defined as a chemical or electrochemical reaction between a material, usually a metal, and its environment that produces a deterioration of the material and its properties. This chapter describes the effects and economic impact of corrosion in major industrial plants. The emphasis in this chapter, as well as in other chapters in this book, is on aqueous corrosion, or corrosion in environments where water is present. The chapter describes the classification of various forms of corrosion based on the nature of the corrodent, mechanism of corrosion, and appearance of the corroded metal. It discusses five primary methods of corrosion control, namely, material selection, coatings, inhibitors, cathodic protection, and design. Examples of the opportunities in corrosion control and the means to implement a program to capitalize on those opportunities are presented in a table. The chapter concludes with varied sources of information pertaining to corrosion and corrosion prevention.

This chapter discusses the processes involved in the calculation of cooling and heating curves and the estimation of austenitizing time. The chapter discusses the transformation of austenite, describing nucleation and growth rates. The chapter examines the calculation of the amount of martensite and retained austenite, and hardenability calculations. It reviews models for tempering of steels, estimation of mechanical properties, the hardness of martensite, and factors to consider to be able to calculate the residual stresses. It provides information on Kirkaldy’s model used for calculating Jominy curves. Tables for calculating the temperature distribution in steels as a function of time during heating and cooling are also included.