Search Results for high-temperature dynamic recovery test

This chapter discusses the development and use of microstructure models for optimizing superalloy forging operations. It describes how the processes that control grain structure evolution during hot working were used in model formulation and compares predicted microstructures with experimental results.

This article addresses some established protocols in characterizing thermoplastics, whether they are homogeneous resins, alloyed or blended compositions, or highly modified thermoplastic composites. It begins with a description of various approaches used for the determination of molecular weight (MW) by viscosity measurements. This is followed by a discussion of the use of cone and plate and parallel plate geometries in determining the viscoelastic properties of a polymer melt. Details on some of the chromatographic techniques that allow determination of MW and MW distribution of polymers are then provided. The article concludes with information on three distinctive, but complementary operations of thermoanalytical techniques, namely differential scanning calorimetry, thermogravimetric analysis, and thermomechanical testing.

Steels with martensitic and tempered martensitic microstructures, though sometimes perceived as brittle, exhibit plasticity and ductile fracture behavior under certain conditions. This chapter describes the alloying and tempering conditions that produce a ductile form of martensite in low-carbon steels. It also discusses the effect of tempering temperature on the mechanical behavior and deformation properties of medium-carbon steels.

This article briefly introduces some commonly used methods of mechanical testing of plastics for determining mechanical properties, also describing the test methods and providing comparative data for the mechanical property tests. In addition, creep testing and dynamic mechanical analyses of viscoelastic plastics are briefly described. The discussion covers the most commonly used tests for impact performance, various types of hardness test for plastics, the fatigue strength of viscoelastic materials, and the tension testing of elastomers and fibers.

This chapter explains the basic terminology and principles of metallurgy as they apply to extrusion. It begins with an overview of crystal structure in metals and alloys, including crystal defects and orientation. This is followed by sections discussing the development of the continuous cast microstructure of aluminum and copper alloys. The discussion provides information on billet and grain segregation and defects in continuous casting. The chapter then discusses the processes involved in the deformation of pure metals and alloys at room temperature. Next, it describes the characteristics of pure metals and alloys at higher temperatures. The processes involved in extrusion are then covered. The chapter provides details on how the toughness and fracture characteristics of metals and alloys affect the extrusion process. The weld seams in hollow profiles, the production of composite profiles, and the processing of composite materials, as well as the extrusion of metal powders, are discussed. The chapter ends with a discussion on the factors that define the extrudability of metallic materials and how these attributes are characterized.

Creep occurs in any metal or alloy at a temperature where atoms become sufficiently mobile to allow the time-dependent rearrangement of structure. This chapter begins with a section on creep curves, covering the three distinct stages: primary, secondary, and tertiary. It then provides information on the stress-rupture test used to measure the time it takes for a metal to fail at a given stress at elevated temperature. The major classes of creep mechanism, namely Nabarro-Herring creep and Coble creep, are then covered. The chapter also provides information on three primary modes of elevated fracture, namely, rupture, transgranular fracture, and intergranular fracture. The next section focuses on some of the metallurgical instabilities caused by overaging, intermetallic phase precipitation, and carbide reactions. Subsequent sections address creep life prediction and creep-fatigue interaction and the approaches to design against creep.

This chapter focuses on short-term tensile testing at high temperatures. It emphasizes one of the most important reasons for conducting hot tensile tests: the determination of the hot working characteristics of metallic materials. Two types of hot tensile tests are discussed in this chapter, namely, the Gleeble test and the conventional isothermal hot-tensile test. The discussion covers equipment used and testing procedures for the Gleeble test along with information on hot ductility and strength data from this test. The chapter describes the stress-strain curves, material coefficients, and flow behavior determined in the isothermal hot tensile test. It also describes three often-overlapping stages of cavitation during tensile deformation, namely, cavity nucleation, growth of individual cavities, and cavity coalescence.

This chapter compares and contrasts the high-temperature behaviors of metals and composites. It describes the use of creep curves and stress-rupture testing along with the underlying mechanisms in creep deformation and elevated-temperature fracture. It also discusses creep-life prediction and related design methods and some of the factors involved in high-temperature fatigue, including creep-fatigue interaction and thermomechanical damage.

This chapter elucidates the indispensable role of characterization in the development of cold-sprayed coatings and illustrates some of the common processes used during coatings development. Emphasis is placed on the advanced microstructural characterization techniques that are used in high-pressure cold spray coating characterization, including residual-stress characterization. The chapter includes some preliminary screening of tool hardness and bond adhesion strength, as well as a distinction between surface and bulk characterization techniques and their importance for cold spray coatings. The techniques covered are optical microscopy, X-Ray diffraction, scanning electron microscopy, focused ion beam machining, electron probe microanalysis, transmission electron microscopy, and electron backscattered diffraction. The techniques also include electron channeling contrast imaging, X-Ray photoelectron spectroscopy, X-ray fluorescence, Auger electron spectroscopy, Raman spectroscopy, oxygen analysis, and nanoindentation.

This chapter describes the general characteristics of major types of steel annealing, including the process of normalization, which is a process that refines or normalizes the microstructure of steel. The first part of the chapter begins with an overview of the three-stage process of recovery, recrystallization, and grain growth. This is followed by discussions on annealing processes, namely subcritical annealing, critical-range annealing, full annealing, isothermal annealing, annealing for microstructure, and solution or quench annealing. Next, the chapter describes two undesirable reactions that occur during annealing: decarburization and scaling. Information on the gases and gas mixtures used for controlled atmospheres is then provided. The second part of the chapter focuses on the processes involved in normalizing, along with information on furnace equipment for normalizing. In addition, the chapter includes information on processes involved in induction heating of steel.

This article reviews various analytical techniques most commonly used in plastic component failure analysis. The description of the techniques is intended to make the reader familiar with the general principles and benefits of the methodologies. The descriptions of the analytical techniques are supplemented by a series of case studies that include pertinent visual examination results and the corresponding images that aided in the characterization of the failures. The techniques covered include Fourier transform infrared spectroscopy, differential scanning calorimetry, thermogravimetric analysis, thermomechanical analysis, and dynamic mechanical analysis. The article also discusses various analytical methods used to characterize the molecular weight distribution of a polymeric material. It provides information on a wide range of mechanical tests that are available to evaluate plastics and polymers, covering the various considerations in the selection and use of test methods.

This article describes the weldability tests that are used to evaluate the effects of welding on such properties and characteristics as base-metal and weld-metal cracking; base-metal and weld-metal ductility; weld penetration; and weld pool shape and fluid flow. It also describes several weldability tests for evaluating cracking susceptibility, classified as self-restraint or externally loaded tests. The article discusses the processes, advantages, and disadvantages of the weld pool shape tests, the weld penetration tests, and the Gleeble test.

This article introduces procedures an engineer or materials scientist can use to investigate failures. It provides a brief survey of polymer systems and key properties that need to be measured during failure analysis. The article begins with an overview of the problem-solving approach pertinent to structure analysis. This is followed by a review of the characterization of plastics by infrared and nuclear magnetic resonance spectroscopy. The article then provides information on the distribution of molecular weight of an engineering plastic. It further discusses the methods used in thermal analysis, namely differential thermal analysis, thermogravimetric analysis, thermal-mechanical analysis, and dynamic mechanical analysis. The following sections provide details on X-ray diffraction for analyzing crystalline phases and on a minimal scheme for polymer analysis and characterization to assist the design engineer. The article ends with a discussion on the thermal-analytical scheme for analyzing the milligram quantities of polymer samples.

Most of the counterfeit parts detected in the electronics industry are either novel or surplus parts or salvaged scrap parts. This article begins by discussing the type of parts used to create counterfeits. It discusses the three most commonly used methods used by counterfeiters to create counterfeits. These include relabeling, refurbishing, and repackaging. The article presents a systematic inspection methodology that can be applied for detecting signs of possible part modifications. The methodology consists of external visual inspection, marking permanency tests, and X-ray inspection followed by material evaluation and characterization. These processes are typically followed by evaluation of the packages to identify defects, degradations, and failure mechanisms that are caused by the processes (e.g., cleaning, solder dipping of leads, reballing) used in creating counterfeit parts.

In dynamic hardness tests, the test force is applied to the defined indenter in an accelerated way (with a high application rate). Dynamic test methods relate hardness to the elastic response of a material, whereas the classical static indentation tests determine hardness in terms of plastic behavior. This chapter describes the most important and widespread dynamic hardness testing methods. These tests fall into two categories: methods in which the deformation is measured and methods in which the energy is measured. Methods that measure deformation include the Poldi hammer method, the shearing force method, the Baumann hammer method, and the Dynatest method. Methods that measure energy include the Shore method, the Leeb method, and the Nitronic method. The chapter concludes with a discussion of applications of dynamic hardness testing.

Hardness tests provide valuable information about the quality of materials and how they are likely to perform in different types of service. This chapter covers some of the most widely used hardness testing methods, including Vickers, Rockwell, and Brinell tests, Shore scleroscope and Equotip hardness tests, and microindentation tests. It describes the equipment and procedures used, discusses the factors that influence accuracy, and provides hardness conversion equations for different types of materials. It also explains how hardness testing sheds light on anisotropy, machinability, wear, fracture toughness, and tensile strength as well as temperature effects, residual stress, and quality control.

This chapter describes the general characteristics of two commonly classified metalworking processes, namely hot working and cold working. Primary metalworking processes, such as the bulk deformation processes used to conduct the initial breakdown of cast ingots, are always conducted hot. Secondary processes, which are used to produce the final product shape, are conducted either hot or cold. The chapter discusses the primary objectives, principal types, advantages, and disadvantages of both primary and secondary metalworking processes. They are rolling, forging, extrusion, sheet metal forming processes, blanking and piercing, bending, stretch forming, drawing, rubber pad forming, and superplastic forming.

Structural and fracture mechanics-based tools for metals are believed to be applicable to nonmetals, as long as they are homogeneous and isotropic. This chapter discusses the essential aspects of the fatigue and fracture behaviors of nonmetallic materials with an emphasis on how they compare with metals. It begins by describing the fracture characteristics of ceramics and glasses along with typical properties and subcritical crack growth mechanisms. It then discusses the properties of engineering plastics and the factors affecting crack formation and growth, fracture toughness, fatigue life, and stress rupture failures.

This chapter provides a detailed account of corrosion inhibitors for oil and gas production. It begins by discussing some of the demands of competitive industry on inhibitor formulations. It then describes the varying characteristics of oil wells, gas wells, water injection systems, and pipelines. The following sections provide information on the factors influencing corrosivity of produced fluids and the methods of inhibitor application. The chapter discusses the primary causes of corrosion problems and inhibition in waterfloods and provides an overview of bacteria-induced corrosion. Various laboratory testing methods of corrosion inhibitors and the methods used to monitor corrosion rates and inhibitor effectiveness are also presented. The chapter ends by providing information on quality control of inhibitors and computerization of inhibitor treating programs.