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epi-fluorescence
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Image
Published: 01 November 2010
Fig. 9.12 Intraply microcracks in a carbon fiber composite material. Epi-fluorescence, 390–440 nm excitation, 25× objective
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Book Chapter
Series: ASM Technical Books
Publisher: ASM International
Published: 01 November 2010
DOI: 10.31399/asm.tb.omfrc.t53030159
EISBN: 978-1-62708-349-2
... in a carbon fiber composite that is difficult to observe using bright-field illumination but easily identified after the application of a fluorescing dye (Magnaflux Zylgo, Magnaflux Corp.) and epi-fluorescence. (a) Bright-field illumination, 10× objective, with an inset showing the crack using epi...
Abstract
The formation of microcracks in composite materials may arise from static-, dynamic-, impact-, or fatigue-loading situations and also by temperature changes or thermal cycles. This chapter discusses the processes involved in the various methods for the microcrack analysis of composite materials, namely bright-field analysis, polarized-light analysis, contrast dyes analysis, and dark-field analysis. The analysis of microcracked composites using epi-fluorescence is also covered. In addition, the chapter describes the procedures for the determination and recording of microcracks in composite materials.
Image
Published: 01 November 2010
Fig. 11.3 Impact damage of a carbon fiber composite material that has a brittle matrix. (a) Montage of the impact area. Epi-fluorescence, 390–440 nm excitation, 5× objective. (b) Fiber fracture area in the composite. Epi-fluorescence, 390–440 nm excitation, 25× objective. (c) Fracture shown
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Image
Published: 01 November 2010
Fig. 9.11 Intraply microcrack in a carbon fiber composite that is difficult to observe using bright-field illumination but easily identified after the application of a fluorescing dye (Magnaflux Zylgo, Magnaflux Corp.) and epi-fluorescence. (a) Bright-field illumination, 10× objective
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Image
Published: 01 November 2010
Fig. 11.4 Impact damage of a carbon fiber composite material that has a toughened matrix. (a) Montage of the impact area. Epi-fluorescence, 390–440 nm excitation, 5× objective. (b) Multiple intraply fractures. Epi-fluorescence, 390–440 nm excitation, 25× objective. (c) Adhesive failure
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Image
Published: 01 November 2010
Fig. 11.5 Impact damage of a carbon fiber composite material that has a toughened matrix. (a) Montage of the impact area. Epi-fluorescence, 390–440 nm excitation, 5× objective. (b) Wide crack formation in the 45° plies and mainly cohesive failure in the interlayer. Epi-fluorescence, 390–440 nm
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Image
Published: 01 November 2010
Fig. 9.14 Comparison of the same area in a carbon fiber composite using epi-bright-field illumination and epi-fluorescence. The microcracked area of the composite material was sectioned and polished at an oblique angle through the thickness to emphasize the interlayer region. (a) Bright-field
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Image
in Viewing the Specimen Using Reflected-Light Microscopy
> Optical Microscopy of Fiber-Reinforced Composites
Published: 01 November 2010
Fig. 5.10 Microcracks in a composite material that are difficult to observe using epi-bright-field illumination. (a) Bright-field illumination, 25× objective. (b) Same location viewed after applying a fluorescent penetrant dye (Magnaflux Zyglo) to the surface and back-polishing. Epi
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Book Chapter
Series: ASM Technical Books
Publisher: ASM International
Published: 01 November 2010
DOI: 10.31399/asm.tb.omfrc.t53030193
EISBN: 978-1-62708-349-2
...-dyed epoxy casting resin. The use of epi-bright-field illumination does not allow the dye to fluoresce, and therefore, the cracks are hard to distinguish. Bright-field montage, 5× objective Fig. 11.4 Impact damage of a carbon fiber composite material that has a toughened matrix. (a) Montage...
Abstract
As fiber-reinforced polymeric composites continue to be used in more damage-prone environments, it is necessary to understand the response of these materials when subjected to impact from foreign objects. This chapter provides an overview of the analysis methods for impact-damaged composites. It discusses the causes and effects of various failure mechanisms in composite materials. The failure mechanisms covered are brittle-matrix composite failure, tough-matrix composite failure, thermoplastic-matrix composite failure mechanisms, untoughened thermoset-matrix composite failure mechanisms, toughened thermoset-matrix composite failure mechanisms, particle interlayer-toughened composite failure mechanisms, and dispersed-phase, rubber-toughened thermoset-matrix composite failure mechanisms.
Image
in Toughening Methods for Thermoset-Matrix Composites
> Optical Microscopy of Fiber-Reinforced Composites
Published: 01 November 2010
of the polished specimen, wiped off after 2 min, and cleaned with water. The solvent/dye preferentially absorbed into the particles and phases and not the thermoset matrix. Epi-fluorescence, 390–440 nm excitation, 25× objective
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Image
in Toughening Methods for Thermoset-Matrix Composites
> Optical Microscopy of Fiber-Reinforced Composites
Published: 01 November 2010
present is a very small dispersed phase that fluoresces yellow. Epi-fluorescence, 390–440 nm excitation, 25× objective
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Image
Published: 01 November 2010
Fig. 2.5 Composite material that was cut using a waterjet. Very little damage is observed at the cut edge of the specimen. A fluorescing dye was applied to the cut edge to determine if cracks were present. Epi-fluorescence, 390–440 nm excitation, 25× objective
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Image
in Viewing the Specimen Using Reflected-Light Microscopy
> Optical Microscopy of Fiber-Reinforced Composites
Published: 01 November 2010
of the specimen to enhance the contrast of the microcracks. Epi-fluorescence, 390–440 nm excitation, 10× objective
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Image
in Viewing the Specimen Using Reflected-Light Microscopy
> Optical Microscopy of Fiber-Reinforced Composites
Published: 01 November 2010
× objective. (b) Dark-field illumination, 25× objective. (c) Polarized light, 25× objective. (d) Slightly uncrossed polarized light, 25× objective. (e) Epi-fluorescence, 390–440 nm, 25× objective. (f) Transmitted light, Hoffman modulation contrast, 20× objective
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Image
Published: 01 November 2010
Fig. 9.13 Large-scale microcracking in a carbon fiber composite material. Epi-fluorescence, 390–440 nm excitation, 10× objective
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Image
in Introduction—Composite Materials and Optical Microscopy
> Optical Microscopy of Fiber-Reinforced Composites
Published: 01 November 2010
Fig. 1.9 Thermoplastic stitch in carbon fiber composite material. Note the microcracks in the center of the stitch. Epi-fluorescence, 390–440 nm excitation, 25× objective
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Image
in The Effects of Lightning Strikes on Polymeric Composites
> Optical Microscopy of Fiber-Reinforced Composites
Published: 01 November 2010
Fig. 15.5 Micrograph taken under the strike zone showing damage induced by the lightning strike. Epi-fluorescence, 390–440 nm excitation, 25× objective
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Series: ASM Technical Books
Publisher: ASM International
Published: 01 November 2010
DOI: 10.31399/asm.tb.omfrc.t53030245
EISBN: 978-1-62708-349-2
... zone corresponding to section plane A in Fig. 15.1 . The micrographs are taken away from the main damage area to show the effects of interply arcing. A Kevlar stitch is shown between the carbon fibers. (a) Slightly uncrossed polarized light, 25× objective. (b) Epi-fluorescence, 390–440 nm excitation...
Abstract
Lightning damage in polymer composites, as in metal structures, is manifested by damage at both the macroscopic or visual level and within the material microstructure. In addition to visual damage assessment, non-destructive inspection techniques are employed to detect damage within the composite part. This chapter describes the macroeffects of a lightning strike on composites and discusses the methods involved in the assessment of microstructural damage in composites.
Image
in The Effects of Lightning Strikes on Polymeric Composites
> Optical Microscopy of Fiber-Reinforced Composites
Published: 01 November 2010
Fig. 15.4 Micrograph taken at an area under the lightning strike zone showing delamination and microcracking in the composite. Epi-fluorescence, 390–440 nm excitation, 10× objective
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Image
Published: 01 November 2010
, and then subjected to the last stage of polishing to remove additional dye from the surface. Epi-fluorescence, 390–440 nm excitation, 50× objective
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