Search Results for energy-dispersive X-ray spectrophotometry

Several hydraulic pumps that failed in service on a particular type of aircraft were received for analysis. Hydraulic testing was not an option, so the pumps were disassembled and their plungers and cylinders were cleaned and examined. Based on their observations, investigators concluded that cavitation erosion damaged the plungers, causing them to seize.

During a major servicing of an aircraft, cracks were found in the bottom wing root fitting. Based on dye penetrant inspection and the results of SEM fractography and chemical analysis, investigators concluded that the cracks were due to stress corrosion. They also recommended an inspection of all other aircraft with similar fittings and the consideration of alternate materials that are less prone to stress-corrosion cracking.

One of the rotor bearings in an electric motor failed, producing excessive vibrate. The bearing was removed and disassembled, revealing craters and bruises on the inner ring raceway and balls along with evidence of melting and burning of metal. Scanning electron microscopy revealed metal particles near the craters, and energy-dispersive x-ray analysis showed that slivers recovered from the grease had the same composition as the bearing raceway and balls. Based on these observations, it was concluded that the bearing failed due to electrostatic discharge, which would have led to seizure if it continued. The report recommends the use of electrically conductive grease and proper grounding practices.

This chapter discusses the failure of a compressor blade in an aircraft engine and explains how investigators determined the cause. Based on visual examination and the results of SEM fractography and chemical analysis, it was concluded that blade failed due to fatigue fracture originating from nonmetallic inclusions in the blade root.

A driven gear in the gear box of an aircraft engine fractured after a 40 h test run. The driving gear and gear shaft were also damaged. Based on the results of fractography, chemical analysis, metallography, and hardness testing, the fracture was caused by a fatigue crack initiating at the corner of the inner rim near an inclusion. The report recommends the use of a cleaner material and more carefully controlling case hardening process.

This chapter describes some of the most effective tools for investigating boiler tube failures, including scanning electron microscopy, optical emission spectroscopy, atomic absorption spectroscopy, x-ray fluorescence spectroscopy, x-ray diffraction, and x-ray photoelectron spectroscopy. It explains how the tools work and what they reveal. It also covers the topic of image analysis and its application in the measurement of grain size, phase/volume fraction, delta ferrite and retained austenite, inclusion rating, depth of carburization/decarburization, scale thickness, pearlite banding, microhardness, and hardness profiles. The chapter concludes with a brief discussion on the effect of scaling and deposition and how to measure it.

This chapters discusses the basic steps in the failure analysis process. It covers examination procedures, selection and preservation of fracture surfaces, macro and microfractography, metallographic analysis, mechanical testing, chemical analysis, and simulated service testing.

This chapter briefly outlines some of the basic aspects of failure analysis, describing some of the basic steps and major concerns in conducting a failure analysis. A brief review of failure types from fracture, distortion, wear-assisted failure, and environmentally assisted failure (corrosion) is also provided.

This appendix focuses on procedures, techniques, and precautions associated with the investigation and analysis of metallurgical failures that occur in service. It describes the steps of an orderly failure analysis from collecting and examining samples to performing mechanical and nondestructive tests, preparing and examining fractographs and micrographs, determining failure mode, writing the report, and developing follow-up recommendations. It also examines the fundamental mechanisms of failure, why they occur, and how to identify them by their characteristic features.

This appendix is a compilation of terms and definitions related to metallurgy.