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energy dispersive x-ray analysis

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Series: ASM Technical Books
Publisher: ASM International
Published: 01 November 2019
DOI: 10.31399/asm.tb.mfadr7.t91110434
EISBN: 978-1-62708-247-1
... Abstract This article provides an overview of the most common micro-analytical technique in the failure analysis laboratory: energy dispersive X-ray spectroscopy (EDS). It discusses the general characteristics, advantages, and disadvantages of some of the X-ray detectors attached to the...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 October 2005
DOI: 10.31399/asm.tb.faesmch.t51270197
EISBN: 978-1-62708-301-0
... metal particles near the craters, and energy-dispersive x-ray analysis showed that slivers recovered from the grease had the same composition as the bearing raceway and balls. Based on these observations, it was concluded that the bearing failed due to electrostatic discharge, which would have led to...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 November 2019
DOI: 10.31399/asm.tb.mfadr7.t91110447
EISBN: 978-1-62708-247-1
... six methods used in semiconductor industry are: Auger spectroscopy, dynamic secondary ion mass spectroscopy, time of flight static secondary ion mass spectroscopy (ToF-SIMS), X-ray photoelectron spectroscopy, scanning electron microscope-energy dispersive X-ray spectroscopy (SEM-EDX), and transmission...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 November 2007
DOI: 10.31399/asm.tb.htcma.t52080335
EISBN: 978-1-62708-304-1
.... Chemical compositions at different locations were analyzed by energy-dispersive x-ray spectroscopy (EDX) analysis (trace elements not reported here): 1: 31% Ca, 29% Si, 14% Mg, 15% Fe, 9% S, and 2% Zn 2: 63% Fe, 16% Cl, 9% Zn, 4% Pb, and 2% S 3: 20% Fe, 13% Cl, 3% Zn, 41% Pb, 11% S, 4% Na, 3% K...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 August 2018
DOI: 10.31399/asm.tb.msisep.t59220085
EISBN: 978-1-62708-259-4
... the chemical elements present in the sample and even perform chemical analysis of points or regions of the sample. Two methods are widely used to analyze the energy spectrum of the x-rays. The first one is a method called wavelength dispersion spectroscopy (WDS), in which the spectrum of emitted x...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 November 2019
DOI: 10.31399/asm.tb.mfadr7.t91110461
EISBN: 978-1-62708-247-1
... electrons, back-scattered electrons, Auger electrons and X-ray photons. Most of the transmitted and elastically scattered electrons and some of the inelastically scattered electrons are used to form an image. TEM based elemental analysis techniques utilize X-ray photons in energy dispersive spectroscopy...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 June 2016
DOI: 10.31399/asm.tb.hpcspa.t54460121
EISBN: 978-1-62708-285-3
...-dispersive spectroscopy (WDS). The equipment possesses a lateral resolution of 1 to 50 nm in the secondary electron mode. Energy-dispersive x-ray spectroscopy can provide a rapid multielement analysis for Z > 11, with a detection limit of approximately 200 ppm. Wavelength-dispersive spectroscopy is...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 November 2019
DOI: 10.31399/asm.tb.mfadr7.t91110010
EISBN: 978-1-62708-247-1
... Reference , Sixth edition , 477 – 496 ( 2011 ) [11] Vanderlinde W. “ Energy Dispersive X-Ray analysis ” Microelectronics Failure Analysis Desk Reference , Sixth edition , 549 – 560 ( 2011 ) As semiconductor feature sizes have shrunk, the technology needed to encapsulate modern ICs...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 December 2018
DOI: 10.31399/asm.tb.fibtca.t52430107
EISBN: 978-1-62708-253-2
... 2400 191 2600 199 2800 200 Energy dispersive x-ray spectroscopy, also known as energy dispersive analysis by x-rays (EDAX), is a chemical and microanalysis technique used in conjunction with SEM. This technique detects x-rays emitted from the sample to determine the elemental...
Book Chapter

Series: ASM Technical Books
Publisher: ASM International
Published: 01 December 2003
DOI: 10.31399/asm.tb.cfap.t69780383
EISBN: 978-1-62708-281-5
... scanning electron microscope (SEM), which typically includes x-ray instrumentation for chemical characterization by energy-dispersive spectroscopy (EDS). In addition, other analytical techniques are available, either through an in-house laboratory or from an outside service laboratory. The most common...
Book Chapter

Series: ASM Technical Books
Publisher: ASM International
Published: 01 December 2003
DOI: 10.31399/asm.tb.cfap.t69780343
EISBN: 978-1-62708-281-5
...) Elemental concentrations Chemical compositions of surfaces Wavelength dispersive x-ray analysis Elements present on polymer surfaces Identification of contaminants on polymer surfaces References 1. Mark J.E. , Eisenberg A. , Graessley W. , Mandelkern...
Book Chapter

Series: ASM Technical Books
Publisher: ASM International
Published: 01 April 2013
DOI: 10.31399/asm.tb.imub.t53720139
EISBN: 978-1-62708-305-8
... are: Qualitative and quantitative chemical analysis for major and minor elements in metals and alloys Determination of composition and thickness of thin film deposits X-ray fluorescence with energy dispersive detectors have a threshold sensitivity of ~0.02% and a precision for...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 March 2002
DOI: 10.31399/asm.tb.mgppis.t60400149
EISBN: 978-1-62708-258-7
... in the sample. The importance of collecting these x-rays is that compositional information can be thus obtained. Generally, in a SEM, only the x-ray energy is analyzed. The technique is called energy dispersive spectroscopy, or EDS. An example of an EDS analysis is shown in Fig. 6.22 where a...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 November 2019
DOI: 10.31399/asm.tb.mfadr7.t91110413
EISBN: 978-1-62708-247-1
... before purchasing. Energy dispersive x-ray (EDS) analysis is problematic in the ESEM because electron beam scattering into the beam skirt greatly degrades the lateral spatial resolution of the technique. Specimen current methods like EBIC (electron beam induced conductivity), RCI (resistive contrast...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 December 2009
DOI: 10.31399/asm.tb.sfa.t52780193
EISBN: 978-1-62708-268-6
... inspection Missing component Visual examination, x-ray or n-ray (if device cannot be disassembled and depending on materials) Incorrect material Visual examination, along with energy-dispersive analysis of x-rays (EDAX), spectrometry, chromatography (depending on material type) Incorrect assembly...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 November 2019
DOI: 10.31399/asm.tb.mfadr7.t91110603
EISBN: 978-1-62708-247-1
... create counterfeits. These include relabeling, refurbishing, and repackaging. The article presents a systematic inspection methodology that can be applied for detecting signs of possible part modifications. The methodology consists of external visual inspection, marking permanency tests, and X-ray...
Book Chapter

Series: ASM Technical Books
Publisher: ASM International
Published: 01 October 2012
DOI: 10.31399/asm.tb.lmub.t53550193
EISBN: 978-1-62708-307-2
... used in energy-dispersive analysis of x-ray equipment. Powder metallurgy is required for a number of reasons, the primary one being that beryllium castings contain too much porosity and other casting defects to allow their use in critical applications. In addition to the casting defects, the grain...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 September 2008
DOI: 10.31399/asm.tb.fahtsc.t51130111
EISBN: 978-1-62708-284-6
... accentuates height or elevation differences on a fracture surface. The characteristic x-rays can be detected and analyzed according to their energy. This is called energy-dispersive x-ray analysis. The x-ray wavelength corresponds to the presence of a specific element, and its amplitude corresponds to the...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 January 2017
DOI: 10.31399/asm.tb.sccmpe2.t55090419
EISBN: 978-1-62708-266-2
... used for microanalysis, using an electron microprobe or a scanning electron microscope (SEM) with an energy-dispersive x-ray analysis system (EDS) or other suitable analytical equipment. After stripping, the fracture surface should be ultrasonically cleaned in acetone. Additional information on...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 December 2003
DOI: 10.31399/asm.tb.cfap.9781627082815
EISBN: 978-1-62708-281-5