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differential scanning calorimetry
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Published: 30 April 2020
Fig. 3.16 Differential scanning calorimetry data taken during heating of polyethylene, showing onset of melting at 112 °C (234 °F) and termination of melting at 138 °C (280 °F). Source: Barbosa et al. ( Ref 3 )
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Published: 30 April 2020
Fig. 3.19 Differential scanning calorimetry data used to measure heat capacity, in this case for a wax blend, showing a broad melting event. The integral of the curve is the basis for calculating the melting enthalpy. Source: Gebelin et al. ( Ref 4 )
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Published: 30 April 2020
Fig. 3.29 Differential scanning calorimetry curves for polypropylene and polypropylene mixed with added stearic acid up to 40 wt%. The heating rate was 5 °C/min (9 °F/min). The results show that stearic acid is soluble in polypropylene at low concentrations, but at 20%, the stearic acid forms
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Published: 01 November 2010
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in Physical, Chemical, and Thermal Analysis of Thermoplastic Resins[1]
> Characterization and Failure Analysis of Plastics
Published: 01 December 2003
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in Physical, Chemical, and Thermal Analysis of Thermoplastic Resins[1]
> Characterization and Failure Analysis of Plastics
Published: 01 December 2003
Fig. 27 Differential scanning calorimetry (DSC) of polyethylene/polypropylene blend 10 mcal/s range; 20 °C/min (36 °F/min). PE, polyethylene; PP, polypropylene. Source: Ref 29
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Published: 01 December 2003
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Published: 01 December 2003
Fig. 6 Differential scanning calorimetry thermogram of polyethylene/polypropylene blend, 10 mcal/s range, 20 °C/min (36 °F/min) heating rate. PE, polyethylene; PP, polypropylene. Source: Ref 56
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Published: 01 December 2003
Fig. 7 Differential scanning calorimetry determination of the effect of a plasticizer on T m of nylon 11. Range, 0.0024 W (10 mcal/s); heating rate, 20 °C/min (36 °F/min); weight, 6.8 mg (0.105 gr), both samples. Source: Ref 51
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Published: 01 December 2003
Fig. 8 Differential scanning calorimetry determination of polyethylene in impact polycarbonate. Range, 0.00048 W (2 mcal/s); heating rate, 20 °C/min (36 °F/min); weight, 23 mg (0.355 gr). Source: Ref 51
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Published: 01 December 2003
Fig. 10 Differential scanning calorimetry thermogram of Fiberite 934 epoxy, 4.89 mg (0.075 gr), 10 °C/min (18 °F/min) heating rate
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Published: 01 December 2003
Fig. 2 Annealing time effects on differential scanning calorimetry traces of epoxy 828-0-0. Annealed at 23 °C (73 °F). H , convective heat-transfer coefficient. Source: Ref 39
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Published: 01 December 2003
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Published: 01 December 2003
Fig. 18 Differential scanning calorimetry of nylon gears. MW, molecular weight; T g , glass transition temperature; T m , melt temperature
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Published: 01 December 2003
Fig. 19 Differential scanning calorimetry determination of the effect of a plasticizer on melting temperature ( T m ) of nylon 11. Range, 0.0024 W (10 mcal/s); heating rate, 20 °C/min (36 °F/min); weight, 6.8 mg (0.105 gr), both samples. Source: Ref 19
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Published: 01 December 2003
Fig. 20 Differential scanning calorimetry determination of polyethylene in impact polycarbonate. Range, 0.00048 W (2 mcal/s); heating rate, 20 °C/min (36 °F/min); weight, 23 mg (0.355 gr). T m , melting temperature; T g , glass transition temperature. Source: Ref 19
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in Characterization of Plastics in Failure Analysis[1]
> Characterization and Failure Analysis of Plastics
Published: 01 December 2003
Fig. 5 Differential scanning calorimetry thermogram showing various transitions associated with polymeric materials. The (I) indicates that the numerical temperature was determined as the inflection point on the curve.
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in Characterization of Plastics in Failure Analysis[1]
> Characterization and Failure Analysis of Plastics
Published: 01 December 2003
Fig. 6 Differential scanning calorimetry used to identify polymeric materials by determination of their melting point
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in Characterization of Plastics in Failure Analysis[1]
> Characterization and Failure Analysis of Plastics
Published: 01 December 2003
Fig. 7 Differential scanning calorimetry used to detect glass transitions within amorphous thermoplastic resins. The (I) indicates that the numerical temperature was determined as the inflection point on the curve.
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in Characterization of Plastics in Failure Analysis[1]
> Characterization and Failure Analysis of Plastics
Published: 01 December 2003
Fig. 19 The differential scanning calorimetry thermogram representing the reference clip material, exhibiting an endothermic transition characteristic of the melting of a nylon 6/6 resin. The results also showed a second melting transition attributed to a hydrocarbon-based impact modifier.
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