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chemical analysis

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Published: 01 August 1999
Fig. 12.20 (Part 4) (j) Comparison among two microscopical methods and the chemical-analysis method (full line) of estimating case depth. More
Series: ASM Technical Books
Publisher: ASM International
Published: 01 December 2003
DOI: 10.31399/asm.tb.cfap.t69780105
EISBN: 978-1-62708-281-5
... thermogravimetric analysis thermomechanical testing molecular weight molecular weight distribution thermoplastic resins chemical analysis physical test DURING THE PROCESSING OF THERMOPLASTICS, polymer chains are sheared, twisted, distorted, stretched, and subjected to a vast array of flow histories...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 December 2003
DOI: 10.31399/asm.tb.cfap.t69780089
EISBN: 978-1-62708-281-5
... to improve since the first inception of this control concept through an Air Force contract ( Ref 1 ). Numerous procedures and methods of physical, chemical, and thermal analysis for thermosetting polymer systems have evolved from this work and subsequent efforts. Most important among...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 January 2000
DOI: 10.31399/asm.tb.cub.t66910475
EISBN: 978-1-62708-250-1
... Abstract This chapter discusses the techniques applicable to the diagnosis of corrosion failures, including visual and microscopic examination of corroded surfaces and microstructure; chemical analysis of the metal, corrosion products, and bulk environment; nondestructive evaluation methods...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 October 2005
DOI: 10.31399/asm.tb.faesmch.t51270113
EISBN: 978-1-62708-301-0
.... Based on visual examination, SEM fractography, and chemical analysis, investigators concluded that the hinge pins were not made from the specified steel and were not properly treated after cadmium plating. The pins failed due to hydrogen embrittlement, which may have been aggravated by welding...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 October 2005
DOI: 10.31399/asm.tb.faesmch.t51270019
EISBN: 978-1-62708-301-0
... and collect test specimens for subsequent examination and chemical analysis. It also discusses the role of mechanical property testing, the use of nondestructive evaluation, and the final step of generating a report. failure analysis nondestructive evaluation FAILURE ANALYSIS...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 October 2005
DOI: 10.31399/asm.tb.faesmch.t51270074
EISBN: 978-1-62708-301-0
... of the springs along with photographs of the damaged slipper pads and cam plate. It also includes an image of a copper flake found in one of the pistons and discusses the results of qualitative x-ray chemical analysis. adhesive wear scanning electron microscopy slipper pads visual examination Summary...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 November 2012
DOI: 10.31399/asm.tb.ffub.t53610549
EISBN: 978-1-62708-303-4
... Abstract This chapters discusses the basic steps in the failure analysis process. It covers examination procedures, selection and preservation of fracture surfaces, macro and microfractography, metallographic analysis, mechanical testing, chemical analysis, and simulated service testing...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 October 2005
DOI: 10.31399/asm.tb.faesmch.t51270130
EISBN: 978-1-62708-301-0
.... The bolts were removed and analyzed to determine the mode and cause of failure. Based on the results of macroscopy, scanning electron fractography, metallographic examination, and chemical analysis, the failures were caused by stress corrosion cracking, and in one case, overtightening. microstructural...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 September 2008
DOI: 10.31399/asm.tb.fahtsc.t51130043
EISBN: 978-1-62708-284-6
... of specimens, mechanical testing, macroexamination, microexamination, metallographic examination, determination of the fracture mechanism, chemical analysis, exemplar testing, and analysis and writing the report. The chapter ends with a discussion on various processes involved in the determination...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 December 2016
DOI: 10.31399/asm.tb.ascaam.t59190147
EISBN: 978-1-62708-296-9
... Abstract Intermetallic phase precipitates in aluminum alloys can often be identified without resorting to chemical analysis. Very often the determination can be made based on the shape, color, and refractive properties of the particular phase. This chapter explains how these visual attributes...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 October 2005
DOI: 10.31399/asm.tb.faesmch.t51270102
EISBN: 978-1-62708-301-0
... and subjected to chemical analysis and low-cycle fatigue tests. Based on their findings, investigators concluded that the bolts failed due to fatigue compounded by excessive clearances and poor surface finishes. The chapter provides a number of recommendations addressing these issues and related concerns...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 April 2013
DOI: 10.31399/asm.tb.imub.t53720001
EISBN: 978-1-62708-305-8
... Abstract This chapter provides an overview of the various inspection methods used with metals and alloys, namely visual inspection, coordinate measuring machines, machine vision, hardness testing, tensile testing, chemical analysis, metallography, and nondestructive testing. The nondestructive...
Book Chapter

Series: ASM Technical Books
Publisher: ASM International
Published: 30 April 2020
DOI: 10.31399/asm.tb.bpapp.t59290009
EISBN: 978-1-62708-319-5
..., powder flow and rheology, and chemical analysis. The chapter then describes the general categories of powder fabrication methods, namely mechanical comminution, electrochemical precipitation, thermochemical reaction, and phase change and atomization. It provides information on the two largest...
Book Chapter

Series: ASM Technical Books
Publisher: ASM International
Published: 01 December 1995
DOI: 10.31399/asm.tb.sch6.t68200187
EISBN: 978-1-62708-354-6
..., and the recovery of elements from slag. It then presents an overview of argon-oxygen-decarburization (AOD) refining and types of ladles. The chapter describes chemical analysis that is performed using either optical emission or x-ray spectrographs. chemical analysis melting melting furnaces refractories...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 October 2005
DOI: 10.31399/asm.tb.faesmch.t51270115
EISBN: 978-1-62708-301-0
.... Most of the blades in the first four stages had sheared off and many lifted from the dovetail region, particularly in the first two stages where several mounting dovetails had also fractured. Based on visual examination and the results of SEM fractography, metallography, and chemical analysis...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 October 2005
DOI: 10.31399/asm.tb.faesmch.t51270146
EISBN: 978-1-62708-301-0
... Abstract During a major servicing of an aircraft, cracks were found in the bottom wing root fitting. Based on dye penetrant inspection and the results of SEM fractography and chemical analysis, investigators concluded that the cracks were due to stress corrosion. They also recommended...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 October 2005
DOI: 10.31399/asm.tb.faesmch.t51270150
EISBN: 978-1-62708-301-0
... Abstract This chapter discusses the failure of a compressor blade in an aircraft engine and explains how investigators determined the cause. Based on visual examination and the results of SEM fractography and chemical analysis, it was concluded that blade failed due to fatigue fracture...
Series: ASM Technical Books
Publisher: ASM International
Published: 01 October 2005
DOI: 10.31399/asm.tb.faesmch.t51270177
EISBN: 978-1-62708-301-0
... Abstract A driven gear in the gear box of an aircraft engine fractured after a 40 h test run. The driving gear and gear shaft were also damaged. Based on the results of fractography, chemical analysis, metallography, and hardness testing, the fracture was caused by a fatigue crack initiating...
Image
Published: 01 August 2018
Fig. 11.49 Cross section of the plane identified as LS in the HY-100 steel plate shown in Fig. 11.48 , slow cooled. The hardness prints indicate the location where the microprobe (WDS) analysis started and ended. Chemical analysis (WDS), shown in (b). Heat analysis: C = 0.16%, Mn = 0.26%, P More