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Book Chapter
Finishing and Coating
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 November 2013
DOI: 10.31399/asm.tb.mfub.t53740325
EISBN: 978-1-62708-308-9
... Occasional or intermittent Solvent wipe Emulsion dip or spray Vapor degrease Cold solvent dip Alkaline dip, rinse, dry or dip in rust preventative Solvent wipe Vapor degrease Phosphoric acid etch Solvent wipe Emulsion dip or spray, rinse Vapor degrease Alkaline spray Solvent wipe Emulsion soak, barrel...
Abstract
This chapter covers a wide range of finishing and coating operations, including cleaning, honing, polishing and buffing, and lapping. It discusses the use of rust-preventative compounds, conversion coatings, and plating metals as well as weld overlay, thermal spray, and ceramic coatings and various pack cementation and deposition processes. It also discusses the selection and use of industrial paints and paint application methods.
Book Chapter
Etchants for Revealing Macrostructure
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 December 1984
DOI: 10.31399/asm.tb.mpp.t67850509
EISBN: 978-1-62708-260-0
... N 0 3 24 mL HCI 39 mL H 2 0 15 mL HF 45 mL HCI 15 mL H N 0 3 25 mL H 2 0 10-20 g NaOH 100 mL H 2 0 1 mLHF 1.5 mL HCI 2.5 mL HNO3 95 mL H 2 0 12 mL HCI 12 mL HNO3 6 mLHF 90 mL H 2 0 Flick's etch. Immerse for 10-20 s, dip in HNO3, rinse, and dry. 180-grit ground surface is best. Etch by immersion...
Abstract
This appendix provides a list of etch compositions and procedures that reveal the macrostructure of aluminum, beryllium, bismuth, antimony, cobalt, copper, lead, magnesium, nickel, tin, titanium, zinc, and their respective alloys as well as iron, steel, noble metals, refractory metals, silicon, zirconium, and hafnium.
Book Chapter
Glossary of Terms
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 March 2001
DOI: 10.31399/asm.tb.secwr.t68350231
EISBN: 978-1-62708-315-7
... from alkali hydroxides and such al- kaline salts as borates, carbonates, phosphates, or silicates. The clean- ing action may be enhanced by the addition of surface-active agents and special solvents. aluminizing. Forming of an aluminum or aluminum alloy coating on a metal by hot dipping, hot spraying...
Abstract
This chapter is a compilation of terms and definitions related to surface engineering for corrosion and wear resistance.
Book
Series: ASM Technical Books
Publisher: ASM International
Published: 01 March 2001
DOI: 10.31399/asm.tb.secwr.9781627083157
EISBN: 978-1-62708-315-7
Book Chapter
Metallography of Beryllium and Beryllium Alloys
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 July 2009
DOI: 10.31399/asm.tb.bcp.t52230199
EISBN: 978-1-62708-298-3
... etchants recommended in the literature were tried, and although most produced heavy pitting at the oxide inclusions, an oxalic acid etch has been modified to give very satisfactory grain-boundary definition. The etch involves dipping the specimen in 3 vol% oxalic acid at 100 °C (212 °F) for 1 min...
Abstract
This chapter explains how to safely prepare beryllium alloy samples for metallographic analysis. It describes grinding, polishing, and etching procedures in detail. It also discusses the identification of major and minor constituents and the general appearance of beryllium microstructure.
Book Chapter
Corrosion Control by Protective Coatings and Inhibitors
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 January 2000
DOI: 10.31399/asm.tb.cub.t66910363
EISBN: 978-1-62708-250-1
..., and inspection and quality assurance. The next section discusses the methods by which metals, and in some cases their alloys, can be applied to almost all other metals and alloys: electroplating, electroless plating, hot dipping, thermal spraying, cladding, pack cementation, vapor deposition, ion implantation...
Abstract
Organic coatings (paints and plastic or rubber linings), metallic coatings, and nonmetallic inorganic coatings (conversion coatings, cements, ceramics, and glasses) are used in applications requiring corrosion protection. These coatings and linings may protect substrates by three basic mechanisms: barrier protection, chemical inhibition, and galvanic (sacrificial) protection. This chapter begins with a section on organic coating and linings, providing a detailed account of the steps involved in the coating process, namely, design and selection, surface preparation, application, and inspection and quality assurance. The next section discusses the methods by which metals, and in some cases their alloys, can be applied to almost all other metals and alloys: electroplating, electroless plating, hot dipping, thermal spraying, cladding, pack cementation, vapor deposition, ion implantation, and laser processing. The last section focuses on nonmetallic inorganic coatings including ceramic coating materials, conversion coatings, and anodized coatings.
Book Chapter
Introduction—Composite Materials and Optical Microscopy
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 November 2010
DOI: 10.31399/asm.tb.omfrc.t53030001
EISBN: 978-1-62708-349-2
...-filled epoxy resin and chopped glass fiber. Bright-field illumination, 65 mm macrophotograph montage. (b) Quasi-isotropic unidirectional prepreg laminate. Slightly uncrossed polarized light, 5× objective, montage. (c) 3k-70 woven carbon fabric laminate. Bright-field illumination, 5× objective, montage...
Abstract
This chapter provides a general description of materials and methods for manufacturing high-performance composites. The materials covered are polymer matrices and prepreg materials and the methods include infusion processes, composite-toughening methods, matrix-toughening methods, and dispersed-phase toughening. In addition, the chapter provides information on interlayer-toughened composites and honeycomb or foam structure composite materials. It also discusses the processes in optical microscopy of composite materials.
Series: ASM Technical Books
Publisher: ASM International
Published: 01 November 2010
DOI: 10.31399/asm.tb.omfrc.9781627083492
EISBN: 978-1-62708-349-2
Book Chapter
Introduction to Surface Engineering for Corrosion and Wear Resistance
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 March 2001
DOI: 10.31399/asm.tb.secwr.t68350001
EISBN: 978-1-62708-315-7
... resistance and heat resistance Hot-dip galvanizing (zinc coatings) Improved corrosion resistance via sacrificial protection of steel substrate Hot-dip aluminizing Improved corrosion and oxidation resistance of steel substrate Hot-dip lead-tin alloy-coatings (terne coatings) Improved corrosion...
Abstract
This chapter begins with a brief review of the different types of surface treatments and coatings used in industry and their effect on properties and performance. It then discusses the importance of corrosion and wear treatments and the consequences of failing to properly implement them in critical industries such as mining, energy production, transportation, and mineral and chemical processing. The chapter also describes basic approaches to dealing with corrosion and wear in steel.
Book Chapter
Metallography
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 April 2013
DOI: 10.31399/asm.tb.imub.t53720161
EISBN: 978-1-62708-305-8
... immersion of a metal specimen into a suitable solution to obtain a metallographic polish. The results of chemical polishing are similar to those of electropolishing. They vary from an etched specimen surface that has been macrosmoothed but not brightened to a bright dipped surface that has been brightened...
Abstract
This chapter describes the methods and equipment applicable to metallographic studies and discusses the preparation of specimens for examination by light optical microscopy. Five major operations for preparation of metallographic specimens are discussed: sectioning, mounting, grinding, polishing, and etching. The discussion covers their basic principles, advantages, types, and applications, as well as the equipment setup. The chapter includes tables that list etchants used for microscopic examination. It also provides information on microscopic examination, microphotography, and the effects of grain size on the structural properties of the material.
Book Chapter
Cross-Sectioning: Mechanical Polishing, Ion Milling, and Focused Ion Beam (FIB)
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 November 2019
DOI: 10.31399/asm.tb.mfadr7.t91110391
EISBN: 978-1-62708-247-1
... needs to aware. Etches can be applied by dipping the sample face into the etchant or by swabbing the etchant on the sample face with a cotton swab. Dipping is the preferred method of many as it is easier to control and leaves a cleaner surface. Note: HF-containing etches should be stored and used...
Abstract
Cross-sectioning is a technique used for process development and reverse engineering. This article introduces novice analysts to the methods of cross-sectioning semiconductor devices and provides a refresher for the more experienced analysts. Topics covered include encapsulated (potted) device sectioning techniques, non-encapsulated device techniques, utilization of the focused ion beam (FIB) making a cross-section and/or enhancing a physically polished one. Delineation methods for revealing structures are also discussed. These can be chemical etchants, chemo-mechanical polishing, and ion milling, either in the FIB or in a dedicated ion mill.
Book Chapter
Customer Manufacturing Processes
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 30 June 2023
DOI: 10.31399/asm.tb.atia.t59340211
EISBN: 978-1-62708-427-7
... equipment manufacturer Tanker trucks use numerous aluminum parts, including the tank from welded polished sheet; formed parts for bumper, grill, fenders, and steps; formed and welded extrusions and tubes in the chassis; and bright anodized wheels machined from forgings THE ATTRIBUTES...
Abstract
This chapter provides basic concepts and background for customer-related manufacturing processes applied to aluminum products including forming, joining and welding, surface treatments, and machinability. It reviews the selection criteria, key testing regimes, and original equipment manufacturer (OEM) requirements. The chapter also presents examples that demonstrate the importance of choosing the correct alloy and temper to successfully meet the OEM fabrication criteria.
Book Chapter
Properties of Titanium-Alloy Welds
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 July 1997
DOI: 10.31399/asm.tb.wip.t65930311
EISBN: 978-1-62708-359-1
... Certain alloy compositions and microstructures have been found to be susceptible to a severe ductility loss (ductility dip) in a temperature range from about 750 to 850 °C (1380 to 1560 °F) on cooling from temperatures above the beta transus. In particular, alpha-beta alloys that contain niobium rather...
Abstract
This article discusses the fusion welding processes that are most widely used for joining titanium, namely, gas-tungsten arc welding, gas-metal arc welding, plasma arc welding, laser-beam welding, and electron-beam welding. It describes several important and interrelated aspects of welding phenomena that contribute to the overall understanding of titanium alloy welding metallurgy. These factors include alloy types, weldability, melting and solidification effects on weld microstructure, postweld heat treatment effects, structure/mechanical property/fracture relationships, and welding process application.
Book Chapter
Etchants for Revealing Microstructure
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 December 1984
DOI: 10.31399/asm.tb.mpp.t67850610
EISBN: 978-1-62708-260-0
.... Grain contrast usually poor. The 0.5% concentration of HF is very popular. Keller's reagent, very popular general-purpose reagent for Al and Al alloys, except high-Si alloys. Immerse sample 10-20 s, wash in warm water. Can follow with a dip in cone. HNO,. Outlines all common constituents, reveals grain...
Abstract
This appendix contains tables that list the composition and capabilities of etchants that reveal the microstructure of metals and alloys, including aluminum, chromium, cobalt, copper, lead, magnesium, molybdenum, nickel, niobium, palladium, platinum, radioactive metals, rare earth metals, rhenium, rhodium, selenium, tellurium, silicon, silver, tantalum, tin, titanium, tungsten, vanadium, and zinc, as well as carbides, oxides, and nitrides.
Book Chapter
Diffusion in Solids
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 September 2022
DOI: 10.31399/asm.tb.dsktmse.t56050001
EISBN: 978-1-62708-432-1
... for precise gas control, safety concerns Vacuum carburizing 815–1050 1500–1920 75 μm–1.5 mm 50–63 Excellent process control, bright parts, faster than gas process, high capital cost Plasma carburizing 815–1050 1500–1920 75 μm–1.5 mm 50–65 Excellent process control, faster than gas and vacuum...
Abstract
A working knowledge of diffusion is necessary to understand and predict the behavior of metals and alloys during manufacturing and in certain types of service. This chapter covers the fundamentals of diffusion in solids and some of the applications in which diffusion plays a role. It discusses the mechanisms behind interstitial, substitutional, grain boundary, and surface diffusion, the derivation and use of Fick’s laws, and the basic principles of diffusion coating processes, including carburizing, nitriding, nitrocarburizing, cyaniding, carbonitriding, boriding, aluminizing, siliconizing, chromizing, vanadizing, and titanizing. It also discusses diffusion bonding and presents several approaches for dealing with oxide barrier problems.
Book Chapter
Glossary
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 March 2002
DOI: 10.31399/asm.tb.mgppis.t60400245
EISBN: 978-1-62708-258-7
... in air or other gaseous media from a temperature above its transformation range. This term should be restricted to steels that are capable of being hardened by cooling in air in fairly large sections, about 50 mm (2 in.) or more in diameter. Same as self-hardening steel. Airy disk. The image of a bright...
Abstract
This chapter presents definitions of terms related to the metallurgy and metallographic study of irons and steels.
Book Chapter
Package Failure Analysis: Flow and Technique
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 November 2019
DOI: 10.31399/asm.tb.mfadr7.t91110010
EISBN: 978-1-62708-247-1
... As semiconductor feature sizes have shrunk, the technology needed to encapsulate modern ICs (integrated circuits) has expanded. Although DIP (dual in-line package) and QFN (quad-flat no-leads) packages are still widely used; they are being replaced in most high-volume applications with WLPs (wafer level packages...
Abstract
As semiconductor feature sizes have shrunk, the technology needed to encapsulate modern integrated circuits has expanded. Due to the various industry changes, package failure analyses are becoming much more challenging; a systematic approach is therefore critical. This article proposes a package failure analysis flow for analyzing open and short failures. The flow begins with a review of data on how the device failed and how it was processed. Next, non-destructive techniques are performed to document the condition of the as-received units. The techniques discussed are external optical inspection, X-ray inspection, scanning acoustic microscopy, infrared (IR) microscopy, and electrical verification. The article discusses various fault isolation techniques to tackle the wide array of failure signatures, namely IR lock-in thermography, magnetic current imaging, time domain reflectometry, and electro-optical terahertz pulse reflectometry. The final step is the step-by-step inspection and deprocessing stage that begins once the defect has been imaged.
Book Chapter
Thin-Section Preparation and Transmitted-Light Microscopy
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 November 2010
DOI: 10.31399/asm.tb.omfrc.t53030115
EISBN: 978-1-62708-349-2
.... The morphology of the interlayer area is shown with the use of transmitted-light Hoffman modulation contrast and differential interference contrast (DIC). Reflected-light bright-field micrographs are shown of the planar and side view of the composite for comparison. When preparing ultrathin sections...
Abstract
Transmitted-light methods reveal more details of the morphology of fiber-reinforced polymeric composites than are observable using any other available microscopy techniques. This chapter describes the various aspects relating to the selection and preparation of ultrathin-section specimens of fiber-reinforced polymeric composites for examination by transmitted-light microscopy techniques. The preparation steps covered are a selection of the rough section, preparation of the rough section for preliminary mounting, grinding and polishing the primary-mount first surface, mounting the first surface on a glass slide, and preparing the second surface (top surface). The optimization of microscope conditions and analysis of specimens by microscopy techniques are also covered. In addition, examples of composite ultrathin sections that are analyzed using transmitted-light microscopy contrast methods are shown throughout.
Book Chapter
The Joining Environment
Available to PurchaseBook: Principles of Brazing
Series: ASM Technical Books
Publisher: ASM International
Published: 01 August 2005
DOI: 10.31399/asm.tb.pb.t51230105
EISBN: 978-1-62708-351-5
.... If the flux is liquid at the joining temperature, it has to wet the joint surfaces in order to be effective. A flux that is liquid can beneficially help suppress the volatilization of high vapor-pressure constituents of filler metals and thereby improve joint quality. This is particularly true in dip brazing...
Abstract
This chapter discusses joining atmospheres that are used for brazing, along with their advantages and disadvantages. It discusses the processes, advantages, and disadvantages of chemical fluxing, self-fluxing, and fluxless brazing. Information on stop-off compounds that are considered as the antithesis of fluxes is also provided.
Book Chapter
Principles of Alloying
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 December 2001
DOI: 10.31399/asm.tb.aub.t61170003
EISBN: 978-1-62708-297-6
... changing the chemical composition of the surface of a part by such processes as plating, cladding, nitriding, ion implantation, carburizing, and hot dip galvanizing, this book is limited to only those alloying processes that affect the bulk of the material, while surface modification is discussed in other...
Abstract
This article discusses the general purpose of alloying and identifies some of the material properties and behaviors that can be improved by adding various elements to the base metal. It explains how alloying can make metals stronger and more resistant to corrosion and wear as well as easier to cast, weld, form, and machine. It also discusses some of the alloying techniques that have been developed to address problems stemming from dissimilarities between the base metal and alloying or inoculate material.
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