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Image
Principle of autoclave curing. The autoclave vessel is pressurized with gas...
Available to PurchasePublished: 01 October 2012
Fig. 8.38 Principle of autoclave curing. The autoclave vessel is pressurized with gas, usually nitrogen or carbon dioxide, at some pressure (e.g., 690 kPa, or 100 psi). Because the laminate inside the vacuum bag is either at atmospheric pressure or has an applied vacuum, there exists
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Image
Published: 01 November 2010
Fig. 4.8 Tools used for autoclave heat-up tests. NC, numerical control. Source: Ref 5
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Published: 01 November 2010
Fig. 4.9 First autoclave heat-up rate test. NC, numerical control. Source: Ref 5
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Published: 01 November 2010
Fig. 4.10 Second autoclave heat-up rate test. NC, numerical control. Source: Ref 5
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Published: 01 November 2010
Fig. 4.11 Third autoclave heat-up rate test. NC, numerical control. Source: Ref 5
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Book Chapter
Fabrication Tooling
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 November 2010
DOI: 10.31399/asm.tb.scm.t52870101
EISBN: 978-1-62708-314-0
... Abstract This chapter discusses the tooling used for autoclave curing, one of the most common composite fabrication processes. The discussion covers curing practices, material selection factors, and design challenges associated with thermal expansion, tool shrinkage, part complexity...
Abstract
This chapter discusses the tooling used for autoclave curing, one of the most common composite fabrication processes. The discussion covers curing practices, material selection factors, and design challenges associated with thermal expansion, tool shrinkage, part complexity, and heating and cooling rates. The chapter also includes best practices and recommendations for toolmaking and assembly.
Book Chapter
Processing Science of Polymer Matrix Composites
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 November 2010
DOI: 10.31399/asm.tb.scm.t52870201
EISBN: 978-1-62708-314-0
... heat and the reaction is exothermic. The concern when curing a composite laminate in an autoclave is that the heat-up rate can be too fast, resulting in a significant rise in temperature in a thick laminate, as shown in Fig. 7.6 . This could result in degradation of the laminate by overheating...
Abstract
This chapter provides an overview of the tools and techniques, as well as some of the underlying theory, that have proven useful for process modeling and simulation. It begins by presenting the framework of a thermoset cure model that accounts for kinetics, viscosity, heat transfer, flow, voids, and residual stress. It then discusses each variable in detail, explaining how it affects the cure process, how it is measured, and how it can be expressed mathematically in the form of a simple model. The discussions throughout the chapter are supported by numerous images, diagrams, and data plots.
Image
A JEDEC tray pattern is outlined by residue that accumulated during autocla...
Available to Purchase
in Acoustic Microscopy of Semiconductor Packages
> Microelectronics Failure Analysis: Desk Reference
Published: 01 November 2019
Figure 43 A JEDEC tray pattern is outlined by residue that accumulated during autoclave testing and observable optically when the part is tilted at an angle (A). The pattern affects the TT-SAM image (B). After removing accumulated residue with an eraser, the TT-SAM image in (C) is obtained.
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Image
Metallographic cross sections of the corroded surface of weld deposits on H...
Available to PurchasePublished: 01 July 1997
Fig. 4 Metallographic cross sections of the corroded surface of weld deposits on Hastelloy B-2 (UNS N10665) after testing in an autoclave at 150 °C (300 °F) for 96 h in a 20% HCI environment. (a) Ni-28Mo (UNS N10665) alloy filler metal. 375x. (b) Ni-42Mo filler metal. 375x. Both samples were
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Image
Metallographic cross sections of the corroded surface of weld deposits on a...
Available to PurchasePublished: 01 December 2006
Fig. 4 Metallographic cross sections of the corroded surface of weld deposits on alloy B-2 (UNS N10665) after testing in an autoclave at 150 °C (300 °F) for 96 h in a 20% HCl environment. (a) Ni-28Mo (UNS N10665) alloy filler metal. 375× (b) Ni-42Mo filler metal. 375×. Both samples were etched
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Book Chapter
Thermoset Composite Fabrication Processes
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 November 2010
DOI: 10.31399/asm.tb.scm.t52870119
EISBN: 978-1-62708-314-0
... processes are discussed: wet lay-up, prepreg lay-up, and low-temperature/vacuum bag curing prepreg. Wet lay-up is used extensively in commercial industries to fabricate fiberglass/polyester parts. Prepreg lay-up and autoclave curing is the predominant fabrication method used in the aerospace industry...
Abstract
This chapter familiarizes readers with the many and varied thermoset composite fabrication processes and the types of applications for which they were developed. It describes wet lay-up, prepreg lay-up, and low-temperature vacuum bag curing prepreg processes, which are best suited for low-volume, medium-sized and larger parts. It also discusses filament winding and preforming processes (including weaving, knitting, stitching, and braiding) in addition to resin-transfer molding, resin film infusion, and pultrusion.
Book Chapter
Thermoplastic Composite Fabrication Processes
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 November 2010
DOI: 10.31399/asm.tb.scm.t52870183
EISBN: 978-1-62708-314-0
... ovens, heated platen presses, or autoclaves. Since time for chemical reactions is not requisite, the time required to reach consolidation temperature is a function of the heating method and the mass of the tooling. The consolidation temperature depends on the specific thermoplastic resin, but it should...
Abstract
This chapter discusses thermoplastic composite fabrication processes and related equipment and procedures. The discussion covers consolidation and thermoforming operations as well as joining methods.
Book Chapter
Repair
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 November 2010
DOI: 10.31399/asm.tb.scm.t52870517
EISBN: 978-1-62708-314-0
... made of prepreg, wet lay-ups, precured composites, or thin titanium sheets adhesively bonded together. Since field repairs are conducted with only vacuum bag pressure (≤14.7 psia or less), the quality of the repair is not as high as that of the original laminate, which was cured in an autoclave at 100...
Abstract
This chapter discusses the primary methods used to repair composites, including fill repairs, injection repairs, bolted repairs, and bonded repairs. It also discusses issues associated with field repairs.
Book Chapter
Sandwich and Integral Cocured Structure
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 November 2010
DOI: 10.31399/asm.tb.scm.t52870255
EISBN: 978-1-62708-314-0
... to 350 kPa) for honeycomb assemblies. The positive pressure of an autoclave, with a vented bag, usually gives quality superior to that of a bond produced in an oven under vacuum bag pressure. The amount of pressure and the adhesive selected are important in forming fillets at the core-to-skin bondlines...
Abstract
This chapter discusses the advantages and disadvantages of sandwich and integral cocured structures, and the methods by which they are made. It begins by explaining where and how sandwich construction is used and why it is so efficient. It then describes the design and fabrication of honeycomb panels and foam cores along with their respective applications and unique attributes. The chapter also discusses the cocuring process and its use in fabricating unitized structures.
Book Chapter
Polymer-Matrix Composites
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 October 2012
DOI: 10.31399/asm.tb.lmub.t53550385
EISBN: 978-1-62708-307-2
... strength, wet = 1 week immersion in 70 °C (160 °F) water. Source: Ref 8.1 To date, most high-performance carbon/epoxy structures have been fabricated using prepreg that is autoclave cured at either 121 or 177 °C (250 or 350 °F). In the early 1990s, work began in developing lower-temperature-curing...
Abstract
Polymer-matrix composites are among the lightest structural materials in use today. They are also highly resistant to corrosion and fatigue and their load-carrying capabilities, such as strength and stiffness, can be tailored for specific applications. This chapter discusses the primary advantages and disadvantages of polymer-matrix composites, how they are produced, and how they perform in different applications. It describes the construction of laminates, the fibers and resins used, and the methods by which they are combined. It explains how strength, modulus, toughness, and high-temperature and corrosion behaviors are determined by the orientation, shape, and spacing of fibers, the number of plies, resin properties, and consolidation and forming methods. The chapter also covers secondary fabrication processes, such as thermoforming, machining, and joining, as well as production equipment and product forms, and include guidelines for optimizing tradeoffs when selecting fibers, resins, and production techniques.
Book Chapter
Void Analysis of Composite Materials
Available to PurchaseSeries: ASM Technical Books
Publisher: ASM International
Published: 01 November 2010
DOI: 10.31399/asm.tb.omfrc.t53030147
EISBN: 978-1-62708-349-2
... void contents. Voids may be located throughout the composite or near the bottom of the part, due to lower pressure near the tool surface ( Ref 6 , 14 , 15 ). Figure 8.2 shows an autoclave-cured composite part made with plies of woven carbon fabric prepreg and unidirectional carbon fiber prepreg...
Abstract
Achieving the best-performing composite part requires that the processing method and cure cycle create high-quality, low-void-content structures. If voids are present, the performance of the composite will be significantly reduced. There are multiple causes of voids in composite materials; they are generally categorized as voids that are due to volatiles (such as solvents, water) or voids that result from entrapped air. This chapter describes the analysis of various types of voids. It reviews techniques for analysis of voids at ply-drops, voids due to high fiber packing, and voids that occur in honeycomb core composites. The final section of the chapter discusses void documentation through the use of nondestructive inspection techniques and density/specific gravity measurement methods.
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