This chapter discusses many aspects of extrusion die and tooling, including the terminology and function of extrusion die and tooling, the types of dies, the fundamentals of die design, manufacturing, correction, material, and the surface treatments of die bearings and tribology in extrusion dies. It then presents the fundamentals and function of finite-element modeling simulation. The chapter describes the role of tribology and thermodynamics in the die bearing to control the flow and dimensional stability of extrusion exiting the die.

This chapter discusses the extrusion technology of soft- and medium-strength aluminum alloys. The relative extrudability ratings of some soft- and medium-grade alloys are given. The chapter presents useful extrusion parameters and their relationships associated with day-to-day production practices in the aluminum extrusion industry. Useful parameters discussed include: extrusion runout; extrusion pressure; ram or extrusion speed control; and butt or extrusion discard thickness control. The chapter provides fundamental approaches to introducing and developing the design of experiments (DOE) for the aluminum extrusion plant to improve overall productivity. It also focuses on heat treatment of aluminum alloys.

This chapter discusses the critical soldering faults that lead to quality degradation and potential failure of a soldered connection. It then describes the types of nondestructive evaluations used to inspect soldered and brazed joints, including dimensional and visual inspection, ultrasonic testing, radiographic examination, dye penetrant inspection, and leak testing, including overpressure tests. The chapter also provides an overview of destructive physical analysis.

This chapter explains how to measure the shape, size, microstructure, and composition of powders as well as their flowability and crystallization behavior. It presents detailed workflows and calculations based on SEM, TEM, FESEM, and STEM imaging, x-ray diffraction, differential scanning calorimetry, EDS and EELS spectroscopy, and powder sieving. It also discusses the measurement of crystallite size, lattice mismatch, and crystallinity and the relationship between surface area and flowability.

This chapter reviews some of the differences between powder metallurgy and additive manufacturing and explains how they influence the microstructure and properties of various alloys and the formation of defects in manufactured parts.

Critical process variables must be controlled to ensure uniform and repeatable heat-treating results. This chapter covers the subject of controlling the heat-treating process. All heat-treating equipment utilizes various sensors, timers, and other components to monitor and control the process utilizing various control methods. The chapter focuses on temperature control and measurement, including a discussion about thermocouples and devices for measuring thermal and electrical conductivity.

Carbonitriding introduces and diffuses atomic nitrogen into the surface steel during carburization. This chapter focuses on case composition of a carbonitrided case, case depth, case hardenability, hardness gradients, void formation, and applications of carbonitriding. The chapter discusses furnaces suitable for carbonitriding, atmosphere constituents, batch furnace atmospheres, continuous furnace atmospheres, safety, temperature selection, quenching, tempering, and hardness testing of a carbonitrided case.

This chapter covers the steps and tests that are important to produce quality parts in heat treating. The quality tests discussed include hardness tests, such as Brinell, Rockwell, and microhardness tests. The chapter also examines tensile testing, toughness testing, optical metallography, and nondestructive testing. The chapter concludes by discussing in-process inspections and the final inspection.

To ensure consistency, quality of results, and documentation compliance, audits are required when heat treating. This chapter introduces basic parts of the ISO certification program.

This chapter focuses on the design of measuring devices. The devices used to measure vibration typically consist of an electronic transducer with an interconnecting cable and an alternating current voltmeter. The working principle of each type of transducer is described in this chapter along with their important characteristics and common applications. The chapter provides general guidelines for the selection of a measuring device, and discusses vibration severity levels.

Phase diagrams serve as a map to the phases present in an alloy at different temperatures and compositions. They also help in assessing mechanical properties, selecting heat treat temperatures, warning of possible solidification problems, and identifying routes for creating desired microstructures. This chapter familiarizes readers with the information contained in binary phase diagrams and the methods used to extract it. It explains how thermocouple measurements are used to determine liquidus, solidus, and eutectic reaction lines, how differential scanning calorimetry shows where phase reactions occur, and how x-ray diffraction identifies the actual phases present. It demonstrates the use of tie lines for determining phase composition at different temperatures and the application of the level rule to calculate phase fractions. It also discusses the CALPHAD method and presents computed binary phase diagrams that account for the presence of inclusions, oxygen content, and secondary phases.

This chapter covers the engineering aspects of corrosion inhibitors and their effect on corrosion reactions. It explains how different metallic salts and heterocyclic compounds influence chemical reactions on metal surfaces exposed to corrosive media or environments. It describes how to evaluate inhibition efficiency through weight loss measurements, linear polarization resistance tests, electrochemical impedance spectroscopy, electrochemical noise monitoring, and surface analysis. It demonstrates the use of potentiodynamic polarization curves, Tafel extrapolations, equivalent circuit models, and various methods for characterizing corrosion damage and protective surface films. It also discusses typical applications, industry trends, and the emerging role of high-throughput experimentation, quantitative modeling, and machine learning in the development of cleaner and more effective corrosion inhibitors.

This chapter contains sample problems with worked solutions pertaining to the application of corrosion inhibitors. Correct answers require an understanding of potentiodynamic polarization scan (PDS) curves, the determination of corrosion current and inhibitor efficiency, and the development of a test plan to evaluate the long-term corrosion protection of a potential inhibitor.