Stress Corrosion Cracking in a Mild Steel Autoclave Used in the Manufacture of Dyestuffs' Intermediates
A steam jacketed autoclave of orthodox design was fabricated from mild steel for a working pressure of 320 psi. The only unusual feature in its construction was a protective layer of weld metal, which was deposited on the internal surface of the upper half of the 1 in. thick shell. The first indication of latent trouble was provided by the bolts which attached the stirring paddles to the shaft and the stationary scraper blades to the shell, either failing in service or breaking off when an attempt was made to remove them. It was the practice to renew them...
Stress Corrosion Cracking in a Mild Steel Autoclave Used in the Manufacture of Dyestuffs' Intermediates, ASM Failure Analysis Case Histories: Chemical Processing Equipment, ASM International, 2019, https://doi.org/10.31399/asm.fach.chem.c9001437
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