In this paper, three productive polishing transmission electron microscopy (TEM) sample preparation methods are reported. The methods are studied to improve the efficiency and expand the application fields. Method 1 and 2 address expanding conventional polishing method application on same or similar pattern samples. Method 1 used a laser mark to identify one of the sample; and method 2 used a Pt coated glass inserted between samples or a direct deposition of Pt on one of the samples. Method 3 was developed facilitate stacking three or more samples into a single, batch process block and improved the efficiency greatly.

This paper reports optimized Transmission Electron Microscopy (TEM) sample preparation methods with Focus Ion Beam (FIB), which are used to reduce or avoid the overlapping of TEM images. Several examples of optimized cross-section sample preparation on 38nm and 45nm pitch are provided with general and novel FIB methods. And its application to plan view TEM sample preparation is also shown. The results establish that the proposed method is useful to reduce or remove pattern overlapping effects in dense structures and can produce higher quality TEM images than can be obtained using conventional top-down FIB-based TEM preparation methods.

This paper reports a novel method for site specific plan view transmission electron microscopy (TEM) sample preparation. The detailed procedure is introduced step by step. To demonstrate the practicality of this technique in failure analysis, case studies on 45nm and below technology nodes using the novel method are reported. The results showed that the method is very useful for the analysis of the specified failure location and is helpful to improve the success rate of failure analysis.

The MEMS structure has its particular character like hollow areas inside, and “floating” structures. Traditional TEM sample preparation method usually leads to distortion and dissociation defects of the floating structure. This paper introduces two innovative practical methods of TEM sample preparation using focused ion beam (FIB) for MEMS floating structure analysis. Method 1 used glass needle to lift out the separated film onto glue coated blank wafer; method 2 used in situ pick up system to lift out L- or C-shaped cut film onto TEM half-grid. And then the sample can be applied to normal TEM membrane preparation procedure.

The corrosion phenomenon was found at the edge area of bond pad under OM images after dicing saw. Experiment showed that the corrosion was related with the feed speed of dicing saw. From SEM and OM results, there were some abnormal contaminations around the corrosive area. Auger and TEM with EDX system were used to characterize the corrosive region and the related Al pad corrosion mechanism was discussed. In this paper, Cu rich and O rich layers were identified by TEM and EDX, which could be induced by galvanic cell reaction.