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R. Taylor
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Proceedings Papers
ITSC1998, Thermal Spray 1998: Proceedings from the International Thermal Spray Conference, 623-628, May 25–29, 1998,
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Within a Brite Euram project thick thermal barrier coatings for combustor applications were produced by plasma spraying of yttria partially stabilised zirconia (ZrO2 + 8 wt.% Y2O3). The material properties of such coatings strongly depend on their microstructure which can be altered by manipulating the parameters controlling the plasma spraying process. Covering a variation of possible microstructures, the coatings considered had a thickness of about 2 mm and were six to eight times thicker than the coatings currently in service. This investigation was concerned with an evaluation of the thermophysical and mechanical properties of these coatings and their correlation with the microstructure and the plasma spray parameters. Particular attention was paid to the influence of coating segmentation, microcracking and porosity. The experimental work included the measurement of the thermal diffusivity using the laser flash technique, thermal expansion measurements, and the determination of flexural strength and Young's modulus by means of a specially constructed four-point bend rig. Since some of the samples considered were sprayed according to a partially factorial test plan a statistical evaluation of the material data was possible yielding the correlation between process parameters and material properties.
Proceedings Papers
ITSC1997, Thermal Spray 1997: Proceedings from the United Thermal Spray Conference, 291-298, September 15–18, 1997,
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Thermal conductivity is an important design parameter for thermal barrier coatings. Accurate thermal conductivity data is therefore required to ensure proper design and reliability of gas turbine blades. In the present research, thermal conductivities of Al 2 O 3 and 8wt.% Y 2 O 3 stabilized ZrO 2 (8YSZ) coatings, made by air plasma spray, were determined from the measurements of thermal diffusivity and specific heat as a function of temperature. Thermal diffusivity was determined by the laser flash technique. Specific heat was determined by a Differential Scanning Calorimeter (DSC). Detailed analyses of the results indicate that the thermal conductivity is sensitive to coating density (porosity), interfaces between splats as well as the interface between the coating and the substrate. Additionally, thermal conductivity evaluations of these coatings were also influenced by the accuracy and relevance of the data on bulk monolithic materials. Further, analyses of sensitivity of the laser flash technique to variations in the coating and the substrate parameters, for the coatings evaluated in this study, were also performed. The results are discussed in the context of coating characteristics, reference conductivity data for dense materials and the sensitivity of the measurement method to coating parameters.
Proceedings Papers
ITSC1997, Thermal Spray 1997: Proceedings from the United Thermal Spray Conference, 305-313, September 15–18, 1997,
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In order to increase the efficiency of heavy duty gas turbines for power generation and to reduce their emissions, higher combustion chamber temperature is required; a considerable improvement of the insulation properties of the thermal barrier coatings is therefore required. 1.5 mm thick thermal barrier coatings have been deposited by air plasma spraying a mixed polyester-zirconia powder; by this process high porosity, up to 22%, has been achieved together with a good deposition efficiency (about 50%); the coating microstructure has been thoroughly examined by quantitative image analysis, determining the pores size distribution and the vertical segmentation cracks density. Thermal shock tests showed a life improvement with respect to the state-of-art by a factor > 100; relationships among thermal shock life, deposition rate, segmentation cracks density and porosity were determined. Thermal expansion and thermal diffusivity were measured up to 1200 °C; failure strength, failure strain and Young's modulus were determined by a four-point bending technique.