The result of applying normal xenon ion beam milling combined with patented DX chemistry to delayer state-of-theart commercial-grade 14nm finFETs has been demonstrated in a Helios Plasma FIB DualBeam™. AFM, Conductive-AFM and nano-probing with the Hyperion Atomic Force nanoProber™ were used to confirm the capability of the Helios PFIB DualBeam to delayer samples from metal-6 down to metal-0/local interconnect layer and in under two hours produce a sample that is compatible with the fault isolation, redetection, and characterization capabilities of the AFP. IV (current-voltage) curves were obtained from representative metal-0 contacts exposed by the PFIB+DX delayering process and no degradation to device parameters was uncovered in the experiments that were run. Compared to mechanically delayering samples, the many benefits of using the PFIB+DX process to delayer samples for nano-probing were conclusively demonstrated. Such benefits, include sitespecificity, precise control over the amount of material removed, >100μm square DUT (device under test) area, nm-scale flatness over the DUT area, nm-scale topography between contacts and the surrounding ILD, uniform conductivity across the DUT area, all with no obvious detrimental effects on typical DC device parameters measured by nano-probing.

Advances in FIB (focused ion beam) chemical processes and in the Ga (gallium) beam profile are discussed; these advances are necessary for the successful failure analysis, circuit edit and design verification of advanced, sub-0.13µm Cu devices. Included in this article are: a novel FIB method (CopperRx) for smoothly milling thick, large grained Cu lines; H2O and O2 processes for cleanly cutting thin, smaller grained Cu lines, thereby forming electrically open interconnects; a XeF2 GAE (gas assisted etching) process for etching low k, CVD dielectrics such as F and C doped SiO2; H2O and XeF2 GAE processes for etching low k, spin-on, organic dielectrics such as SiLK; a recently developed recipe for the deposition of SiO2 based material with intermediate resistivity (10 6 µohm·cm) which is useful in the design verification of frequency sensitive, high speed analog and SOC (system on chip) circuits; an improved, more Gaussian Ga beam with less current density in the beam tails (VisION column) which provides higher resolution, real time images needed for end-point detection on sub 0.13µm features during milling.