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Bonding strength
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Proceedings Papers
ITSC2024, Thermal Spray 2024: Proceedings from the International Thermal Spray Conference, 536-542, April 29–May 1, 2024,
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Plasma spraying is the most versatile coating process for depositing a wide range of materials to enhance material performance in harsh conditions. However, severe oxidation during the plasma spraying of metal coatings often results in coatings with high oxide content, limiting interlamellar bonding. Consequently, as-sprayed metal coatings offer inadequate protection against severe corrosion and wear. To address this challenge, we developed Ni-, Cu-, and Fe-based materials containing boron as a deoxidizer. This innovative approach effectively suppresses in-flight oxidation, producing oxide-free molten droplets and enabling the formation of bulk-like metal coatings with sufficient metallurgical bonding between splats. We employed a modified tensile test to evaluate the adhesive and cohesive strengths of these coatings. The Ni-based coatings exhibited adhesive strength exceeding 150 MPa on Fe-based substrates, while cohesive strength surpassed 260 MPa with a novel bond coat. Corrosion and gas penetration tests confirmed the creation of dense, bulk-like Ni-based alloy coatings, demonstrating their potential for various applications in severe service environments.
Proceedings Papers
ITSC2024, Thermal Spray 2024: Proceedings from the International Thermal Spray Conference, 617-622, April 29–May 1, 2024,
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In order to overcome the problem of insufficient abradability of existing metal based coatings that cannot meet the requirements of harsh working conditions, this article designs two types of metal based abradable sealing coating materials based on the particle structure of "peeling medium", and studies the basic performance and simulated working condition service performance of the coatings. The research shows that, after undergoing a 1000 hour heat exposure test at high temperature, the two coatings still maintain good hardness, bonding strength, and abradability, indicating that under long-term high-temperature service environment, the two coatings can fracture at the location where the abradable components are exposed, thereby maintaining the abradability and good thermal stability that meet the requirements of use.
Proceedings Papers
ITSC2023, Thermal Spray 2023: Proceedings from the International Thermal Spray Conference, 208-213, May 22–25, 2023,
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Direct cold spray deposition of Cu was not possible on carbon fiber-reinforced polymer composites (CFRPs) with thermosetting polymer as the matrix material due to substrate erosion. In a recent study, an epoxy-CFRP was successfully metallized through a hybrid coating process that involves three consecutive coating steps: (i) electroless deposition, followed by (ii) electrodeposition, and finally (iii) cold spray. In this present study, for the reduction of the coating process steps, a duplex metallic coating was developed on an epoxy-CFRPs by cold spray deposition of tin (Sn) to fabricate a continuous metallic interlayer, followed by Cu electrodeposition (i.e., SnCS-CuEP). The tensile adhesion bond strength and the electrical resistivity of the duplex coating were investigated. It was found that cold-sprayed Sn coating failed adhesively in the absence of the electrodeposited Cu coating. After the electrodeposition of Cu, cohesive failure of the cold-sprayed Sn coating took place. A “dissolution-deposition” mechanism has been established to explain the cohesive failure of the coldsprayed Sn coating after electrodeposition. The cohesive strength of the Sn coating is slightly higher than that of the previously fabricated three-step coating system. The electrical conductivity of the electrodeposited Cu coating was found to be 90% of bulk Cu. These results suggest that a duplex SnCS-CuEP coating can be fabricated on epoxy-CFRPs with relatively high electrical conductivity and slightly enhanced adhesion properties as compared to multilayered coatings fabricated using a three-step electroless deposition-electrodeposition-cold spray process.
Proceedings Papers
ITSC2023, Thermal Spray 2023: Proceedings from the International Thermal Spray Conference, 330-335, May 22–25, 2023,
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With an increasing demand for lower fuel consumption of different means of transportation, the demand for lightweight construction materials is rising. In this frame, usually metallic parts can be replaced by components consisting of fiberreinforced plastics. On the other hand, the components lose their electromagnetic field (EMF) shielding properties, which are required for many applications such as housings for electrical components. This issue can be solved by applying electrically conductive foils or meshes, often by a manual process that increases the time of production and process. In this publication, the application and parameter influence of thermally sprayed electrically conductive coatings for EMFshielding applications is discussed. Laser structuring is used as a novel surface preparation process, for the subsequent thermal spray process. The influence of the used laser-parameters is discussed accordingly. The coatings are applied by the wire-arc spray with Zinc feedstock as well as the atmospheric plasma spray (APS) process with Copper feedstock. It was found that coating properties such as adhesion strength, EMF-shield strength as well as electrical properties are provided by the proposed technology.
Proceedings Papers
ITSC2023, Thermal Spray 2023: Proceedings from the International Thermal Spray Conference, 336-343, May 22–25, 2023,
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Fluorinated polymer coatings are potential candidates for ice protection systems. The current work aims to develop such coatings using cold spray as a production method. A computational approach is used to design a new cold spray nozzle for the efficient deposition of adhesive perfluoroalkoxy alkane. The icephobicity of as-sprayed coatings are evaluated using three-fold characterization: surface’s wetting behavior, time-lapse study of water droplets freezing, and ice adhesion at both macro and microscopic levels. While the as-sprayed coatings exhibited sought superhydrophobic properties, their behavior changed when exposed to frost formation resulting in degraded wetting behaviors and much larger ice adhesion strength. This demonstrates the importance of frost formation when studying icephobic coatings.
Proceedings Papers
ITSC2023, Thermal Spray 2023: Proceedings from the International Thermal Spray Conference, 344-350, May 22–25, 2023,
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The metallic bond coat is generally utilized to increase the coating adhesion and the adhesion of thermal spray bond coat is of essential importance to applications. However, it usually depends on mechanical bonding with a low adhesive strength. In this study, a novel metal bond coat with high cohesion strength is proposed by plasma-spraying Mo-clad Ni-based or Fe-based spherical powder particles. Mo-cladding ensures the heating of spray particles to a high temperature higher than the melting point of Mo and prevents metal core from oxidation during spraying. Theoretical analysis on the splatsubstrate/ splat interface temperature and experimental examination into coating-substrate interface microstructure were performed to reveal the metallurgical bonding formation mechanism. The local melting of substrate surface and resultant bond coating by impacting high temperature droplets creates metallurgical bonding throughout the interfaces between substrate and bond coat, and within bond coat. The experiments were conducted with different substrates in different surface processing conditions including Ni-based alloy, stainless steel and low carbon steel. All pull-off tests yielded strong adhesion higher than the adhesives strength of 80 MPa. The present results revealed that Mo-clad metal powders can be used as new bond coat materials and high performance bond coat can be deposited by atmospheric plasma spraying.
Proceedings Papers
ITSC2023, Thermal Spray 2023: Proceedings from the International Thermal Spray Conference, 597-603, May 22–25, 2023,
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Battery manufacturing involves a large number of individual cells arranged in modules configured within a battery pack and connected either in series and/or parallel to deliver the required power and driving range. Cells within a module are linked using a tab-to-busbar connection as the electrical interconnect. Therefore, a battery pack contains a plurality of tab-to-busbar joints, and each must provide low electrical resistivity connection to minimize losses that may reduce the effective performance of the battery. In this work, the Dual Flow Cold Spray (DFCS) process, a modification of low-pressure cold spraying, was used to form low resistivity Cu+10%Zn and Al+10% Zn tab-to-busbar interconnects. As test coupons, 0.8 mm thick copper (Cu) was used to represent the busbar while 0.3 mm thick aluminum and nickel coated copper foils represented the respective electrode tabs. Low resistivity joint interconnects (≈100 μΩ) with high adhesion strength (≈120 MPa) have been formed. The influence of busbar surface preprocessing on the resistivity of the tab-to-busbar joints has been studied.
Proceedings Papers
ITSC 2022, Thermal Spray 2022: Proceedings from the International Thermal Spray Conference, 199-204, May 4–6, 2022,
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In addition to the proper functional properties, the adhesive strength represents one of the key criteria for industrial use of thermally sprayed coatings. Since conventional thermal spraying processes are almost carried out exclusively in air atmosphere, this leads to the oxidation of the particles and of interfaces within the coatings. As a result, conventional thermally sprayed metallic and metal-ceramic coatings are characterized by heterogeneous microstructures with interlamellar oxide fringes at the interfaces between individual splats and also between the coating and the substrate. This has a decisive influence on the bond strength and on the wear and corrosion protection properties of thermally sprayed coatings. The aim of this study is to present the potentials of thermal spraying processes carried out in a mixture of monosiliane and an inert gas at ambient pressure as an alternative to the known vacuum spraying process in order to prevent oxidation during the coating process. Using the example of arcsprayed coatings, it is demonstrated that the extremely low oxygen partial pressure in the silane-doped medium leads to coatings free of oxide seams with a reduced porosity and substantially enhanced properties.
Proceedings Papers
ITSC 2022, Thermal Spray 2022: Proceedings from the International Thermal Spray Conference, 1000-1005, May 4–6, 2022,
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Abradable seal coatings are widely employed in the gas turbine of aero-engine, which not only strength enough to resist the impact of external particles and airflow, but also excellent wear resistance. In the current study, we concentrate on APS sprayed Aluminum Bronze Polyester abradable coating that can be used in turbo engines both for seals and clearance control. A composite thermal spray powder, substantially in the form of clad particles each of which has coarse polyester powders and sub-particles of Cu-Al alloy powders, was prepared using mechanically clad process. Abradable seal coating was prepared by atmospheric plasma spraying. The microstructure, hardness, bonding strength, thermal shock resistance and corrosion resistance of coatings were researched. Properties of the coating were able to meet the application requirements. The coating microstructures and phase compositions were evaluated via SEM. The corrosion mechanisms of the coating were compared by analyzing the cross-sectional and top surface microstructures of the as-sprayed and eroded coatings.
Proceedings Papers
ITSC 2021, Thermal Spray 2021: Proceedings from the International Thermal Spray Conference, 107-114, May 24–28, 2021,
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This present work investigates the effect of electromagnetic fields on cold spray processes by means of an induction-heating cold spray (IHCS) system. Aluminum powder was cold sprayed onto inductively heated Ti6Al-4V (Ti64) substrates. These materials were selected to minimize the mechanical contribution to coating adhesion. As a result, changes in coating adhesion strength can be attributed to improved metallic bond formation due to the effect of the electromagnetic field. Four different initial substrate surface temperatures were used in the study to assess the role of initial temperature as well. Deposition efficiency and adhesion and tensile strength measurements were recorded and are used to characterize the hybrid coating process and compare it with traditional techniques.
Proceedings Papers
ITSC 2021, Thermal Spray 2021: Proceedings from the International Thermal Spray Conference, 189-196, May 24–28, 2021,
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Segregating the convoluted effects of particle size, impact temperature and velocity on deposition behavior and adhesion is of utmost interest to the cold spray field. The current study aims to associate the particle impact behavior and adhesion to its in-flight characteristics by studying and decoupling the influence of particle size, temperature and velocity for single particle impacts and full coatings. Experimental results reveal that in-situ peening processes contribute to the adhesion at low impact temperature while particle velocity controls the adhesion/cohesion at increased particle impact temperatures. The benefits of both bonding mechanisms are discussed in terms of measured adhesion/cohesion, bend-to-break fracture surfaces, pseudoplasticity, deposition efficiency and critical velocity. Computational fluid dynamics (CFD) results provide individual particle trajectory, size, temperature and velocity, of successfully deposited particles, which have led to the observed signs of metallurgical bonding.
Proceedings Papers
ITSC 2021, Thermal Spray 2021: Proceedings from the International Thermal Spray Conference, 203-208, May 24–28, 2021,
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Low pressure cold spraying is an attractive technique for onsite metal coating fabrication due to its compactness and portability. However, the bonding strength of the coating prepared by low pressure cold spraying is generally low, which restricts the further applications in engineering and industrial fields. To improve the bonding strength, pre-treatment on substrate surface can be an effective procedure. In this study, a low-temperature plasma treatment was applied to a pretreatment technique, and the effect of the treatment on particle bonding was compared with that of a laser treatment. Copper coatings on aluminum and copper substrates were selected and studied as basic metal materials. The SEM observation results show that the particle adhesion rate significantly increases by the laser and plasma treatments, due to the removal of the native oxide films on the substrates. The particle bonding on the plasma-treated substrate reveals better interfacial adhesion with less gap compared with the laser-treated one. The pre-treatment by low-temperature plasma can be an attractive technique to assist the cold spraying process due to the oxide removal ability and no thermal effect which can apply a wide range of materials.
Proceedings Papers
ITSC 2021, Thermal Spray 2021: Proceedings from the International Thermal Spray Conference, 235-240, May 24–28, 2021,
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In this study, a new physically-based finite element approach is proposed to model and predict the superficial oxide layer removal and the occurrence of localized metallic bonding during particle impacts. The process physics, based on explosive welding theory and experiments, and method implementation is presented. Prediction of critical velocity of copper is obtained and compared to experimental data to validate the model. Moreover, the model is also able to show the bonding locations at the interface between particles and substrate. The predicted bonding locations are consistent with experimental data from literature for several metals.
Proceedings Papers
ITSC 2021, Thermal Spray 2021: Proceedings from the International Thermal Spray Conference, 241-246, May 24–28, 2021,
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Cold spray process was chosen as a good candidate for dimensional restoration and protection of components. Commercially pure aluminum, aluminum-alloy or titanium were recommended for different applications. This paper investigates laser surface texturing association to enhance durability of sprayed coatings. Laser is easy automated, localized and reliable process. It was applied for prior-surface treatment. Textured surfaces were produced and compared to conventional treatments, such as grit-blasting, in terms of deposition efficiency and adhesion bond strength. Patterns promoted direct particle embedment. Particle-substrate interface exhibited significant temperature rate and strain in cavities. Intimate contacts and particle compressive states were assumed responsible for improvement. The particle deformation and bonding behaviors were evaluated and discussed for the different configurations. Thus, window of deposition was increased with laser surface texturing. Anchoring mechanisms increased two fold the adhesion strength compared to conventional pre-treatments. In one case, the interface was stronger than the coating cohesive strength.
Proceedings Papers
ITSC 2021, Thermal Spray 2021: Proceedings from the International Thermal Spray Conference, 396-401, May 24–28, 2021,
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Recently, cold spray (CS) technology has attracted extensive interest as an alternative to thermal spray methods to build a coating, which uses high kinetic energy solid particles to impact and adhere to the substrate. To date, numerous numerical studies have been carried out to investigate the deposition processes and associated mechanisms during multiple particle impact in CS. However, in the commonly used numerical techniques, the individual powder particles are often treated separately from one another, thus fail to properly consider the adhesion mechanisms during deposition. In this study, we propose a new numerical approach on base of peridynamics (PD), which incorporates interfacial interactions as a part of constitutive model to capture deformation, bonding and rebound of impacting particles in one unified framework. Two models are proposed to characterize the adhesive contacts: a) a long-range Lenard-Johns type potential that reproduce the mode I fracture energy by suitable calibrations, and b) a force - stretch relation of interface directly derived from the bulk materials mode I fracture simulations. The particle deformation behavior modeled by the peridynamic method compares well with the benchmark finite element method results, which indicates the applicability of the peridynamic model for CS simulation. Furthermore, it is shown that the adhesive contact models can accurately describe interfacial bonding between the powder particles and substrate.
Proceedings Papers
ITSC 2021, Thermal Spray 2021: Proceedings from the International Thermal Spray Conference, 410-415, May 24–28, 2021,
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Thermal spray coatings are widely used to protect materials from corrosion, wear, and oxidation, but they have yet to reach their full potential because of porosity limitations and the detrimental effects of oxidation on interlamellar bonding. This paper investigates an atmospheric plasma spraying process that deposits oxide-free dense metallic coatings with well bonded lamellae. The process produces ultrahigh temperature metallic droplets, up to 2650 °C, using specially designed powders that are deoxidized in-flight through the evaporation or gasification of oxides. The impact of these oxide-free ultrahigh temperature droplets has a spreading-fusing, self-metallurgical bonding effect resulting in fully dense bulk-like metallic coatings. Various coating materials, including NiCrMo, 304SS-Mo, NiCrBSi, and Al, are investigated, demonstrating the versatility of the new technique.
Proceedings Papers
ITSC 2021, Thermal Spray 2021: Proceedings from the International Thermal Spray Conference, 569-577, May 24–28, 2021,
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Assemblies containing fiber-reinforced plastic (FRP) and metal parts are typically fastened together via mechanical joining or adhesive bonding. Mechanical joining processes tend to weaken FRP parts by cutting fibers, while adhesives require long cures and often lead to inseparable material compounds. This paper evaluates a new joining method in which plastic parts are laser treated, then metallized via wire-arc spraying, and finally soldered to mating metal parts using a low-temperature process. Due to the effective increase in interface area resulting from laser structuring, bond strengths of up to 15.5 MPa can be achieved.
Proceedings Papers
ITSC 2021, Thermal Spray 2021: Proceedings from the International Thermal Spray Conference, 596-602, May 24–28, 2021,
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In cold spray, high adhesion of soft materials on hard substrates is commonly achieved by using helium as the propelling gas. This is the case of copper coatings on steel where adhesion may reach values as high as 60 to 80 MPa (glue failure), however, helium is a limited, expensive natural resource, and the use of more abundant nitrogen gas is preferred in an industrial setting. Unfortunately, when using nitrogen gas, little to no adhesion is obtained. In order to eliminate the use of helium gas we studied how laser assisted cold spray could lead to an improvement in adhesion of nitrogen sprayed copper coatings. In this work, several laser parameters (e.g., power and spot size) and process parameters (traverse speed, relative position laser spot vs. gas jet) were varied at a coupon level. Upon optimization, an equivalent adhesion to the coatings prepared with helium was obtained. Furthermore, the cross section of the coatings showed that the copper particles penetrated the steel, similar to what is observed when using helium gas. Optimization of these parameters for application to large diameter (~559 mm) cylinders was also performed. A discussion on the mechanisms which contribute to achieving high adhesion considering the use of helium versus laser assistance is provided.
Proceedings Papers
ITSC 2019, Thermal Spray 2019: Proceedings from the International Thermal Spray Conference, 755-760, May 26–29, 2019,
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In this study, nickel-base superalloy coatings are deposited on CrMoAl substrates by different spraying methods and the coatings are evaluated based on their microstructure, phase composition, surface and splat morphology, bond strength, and corrosion properties. In the experiments, NiCrAlY powders with a particle size range of 30-45 μm were sprayed by conventional air plasma and a new laser hybrid plasma spraying technique. The spraying parameters are presented along with test results, observations, and conclusions. The coatings produced by laser hybrid plasma spraying had an average porosity of 0.9%, a bonding strength of 117 MPa, and significantly better corrosion properties than the APS layers.
Proceedings Papers
ITSC 2019, Thermal Spray 2019: Proceedings from the International Thermal Spray Conference, 761-767, May 26–29, 2019,
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In this investigation, thermally sprayed cylindrical specimens are machined by turning with different cutting speeds. To ensure that process-induced shearing loads do not cause delamination, a fine helical dovetail structure is cut into the substrate before it is coated with FeCrNi alloy by air plasma spraying. Dovetail structures with different geometries were produced and their effectiveness is compared. The finish-machined surfaces of the FeCrNi coatings were examined and characterized with respect to feed marks, cracks, open pores, pull outs, and residual stresses. It is shown that surface roughness and the number of pull outs decrease with increasing cutting speed while residual stresses remain relatively unchanged, except for the orientation of the first principal stress.
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