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Metallurgical Analysis and Preparation
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Proceedings Papers
ITSC 2002, Thermal Spray 2002: Proceedings from the International Thermal Spray Conference, 390-396, March 4–6, 2002,
Abstract
PDF
This study investigates the effect of mounting materials on microstructure and property measurements obtained from thermal spray coatings. Various epoxies and embedding techniques are used and a wide range of layers are examined, including HVOF sprayed WC-Co, Cr 3 C 2 -NiCr, and Al 2 O 3 -TiO 2 ; plasma sprayed Cr 2 O 3 , YSZ, WC-Co, and Ni-Al; and arc sprayed copper and silicon bronze. Image analysis measurements of area percent porosity, thickness, lamellar spacing, and unmelted particles and the results of hardness tests show substantial variation relative to the method used to encapsulate soft and porous coatings. Results indicate that the ideal mounting system for thermal spray coatings would consist of a low viscosity epoxy, to maximize penetration depth, and a high cured hardness, for adequate protection of surfaces and open porosity of hard coating materials. Paper includes a German-language abstract.
Proceedings Papers
ITSC 2002, Thermal Spray 2002: Proceedings from the International Thermal Spray Conference, 397-401, March 4–6, 2002,
Abstract
PDF
A systematic study of sample preparation methods tailored to different types of thermal spray coatings was recently conducted. This paper presents the results of investigations on polishing methods and materials and their effect on the quality of cuts. The results show that the type of polishing cloth used has a major influence on layer breakouts, while the direction of rotation and embedding medium have relatively little effect. Paper includes a German-language abstract.
Proceedings Papers
ITSC 2002, Thermal Spray 2002: Proceedings from the International Thermal Spray Conference, 402-407, March 4–6, 2002,
Abstract
PDF
This paper evaluates an electrochemical mapping method for determining the corrosion resistance and structural integrity of thermally sprayed coatings. In the test setup, a potentiostat is suspended over the test sample, forming an electrochemical cell. The circuit is completed through an electrolyte-containing porous tip. Capillary forces keep the electrolyte on the surface of the tip, preventing transfer to the substrate surface. In the investigation, electrochemical, spatially resolved measurements are carried out on flame and vacuum plasma sprayed nickel-base coatings and compared with the results of salt spray testing. It is observed that the new method offers many advantages being faster, nondestructive, and quantitative in nature. Paper includes a German-language abstract.