Nowadays, semiconductor components are widely used in home electronic appliances, vehicles, industrial motor controls and beyond. The performance and reliability of these components are becoming more crucial and critical. Generally, a semiconductor component consists of lead frames, wires, dies and die attaches. Within the die, the die backside metallization, also known as “BSM,” plays an important role in electronic component manufacturing. The BSM is a layer that promotes good adhesion, electrical properties and long-term stability as a conductive pathway to the circuits. As such, the inspection on BSM is needed to ensure robustness. Several conventional methods have been developed to analyze the die backside metallization. In this paper, we will discuss the inspection on backside metallization and comparison among five sample preparation methods: mechanical cross section with ion milling, mechanical cross section with FIB cleaning, die frontside decapsulation with FIB cut from die surface and FIB cut from die sidewall, and component frontside lapping with FIB from the remaining silicon. Result comparison will be discussed in case studies and the advantages and disadvantages of the five methods will be compared.

As advanced device technologies scale to 5nm with dimensions getting smaller and materials change, it is difficult to control the sample preparation delayering end pointing by polishing. Therefore, it requires an alternative solution such as Xe+ PFIB (Plasma Focused Ion beam) Microscopy for accurate delayering control. PFIB can be used for planar Failure Analysis (FA) delayering but also for nanoprobing sample preparation. This paper introduces the detail of nanoprobing sample preparation by PFIB and discusses nanoprobing results on 5nm FinFET technology.

Microscopic imaging and characterization of semiconductor devices and material properties often begin with a sample preparation step. A variety of sample preparation methods such as mechanical lapping and broad ion beam (BIB) milling have been widely used in physical failure analysis (FPA) workflows, allowing internal defects to be analyzed with high-resolution scanning electron microscopy (SEM). However, these traditional methods become less effective for more complicated semiconductor devices, because the cross-sectioning accuracy and reliability do not satisfy the need to inspect nanometer scale structures. Recent trends on multi-chip stacking and heterogenous integration exacerbate the ineffectiveness. Additionally, the surface prepared by these methods are not sufficient for high-resolution imaging, often resulting in distorted sample information. In this work, we report a novel correlative workflow to improve the cross-sectioning accuracy and generate distortion-free surface for SEM analysis. Several semiconductor samples were imaged with 3D X-ray microscopy (XRM) in a non-destructive manner, yielding volumetric data for users to visualize and navigate at submicron accuracy in three dimensions. With the XRM data to serve as 3D maps of true package structures, the possibility to miss or destroy the fault regions is largely eliminated in PFA workflows. In addition to the correlative workflow, we will also demonstrate a proprietary micromachining process which is capable of preparing deformation-free surfaces for SEM analysis.

This paper evaluates the use of plasma etching for preparing TEM specimens to analyze high aspect ratio 3D NAND integrated circuits. By controlling plasma etching parameters, a relatively high material removal rate could be obtained. Moreover, through the control of etch time, the top region of the test specimens could be completely removed down through the expected number of layers, making it possible to resolve details throughout the entire sample, particularly in the middle region of the 3D NAND, using TEM cross-section analysis.

Planar deprocessing is a vital failure analysis technique for semiconductor devices. The basic concept is to expose an area of interest (AOI) by removing unnecessary material while maintaining planarity and surface evenness. Finger deprocessing is a widely used material removal technique, particularly for fin field-effect transistors (FinFETs). Here, success depends on certain factors, one of which is the location of the AOI. If the AOI is near the edge of the chip, finger deprocessing can be very difficult because material removal rates are much higher there than at the center of the chip. Plasma focused ion beam (PFIB) planar deprocessing is the preferred solution in such cases, but many labs cannot afford a PFIB system. To address this challenge, a sample preparation method has been developed that uses dummy chips to effectively eliminate edges. With dummy chips placed edge-to-edge with test chips, planar deprocessing can be achieved using conventional finger deprocessing techniques. This paper describes the newly developed method, step by step, and presents two examples demonstrating its use.

Convention hand polishing, which is widely used for delayering, is becoming increasingly difficult as metal lines and stacks in semiconductor devices get thinner. For one thing, endpointing at the exact targeted layer and region of interest is a major challenge. The presence of cobalt and its propensity to oxidize, thus complicating electrical measurements, is another challenge. In this study, the authors demonstrate an alternative delayering method based on plasma focused ion beam (PFIB) milling aided by DX gas. The workflow associated with the new method is more efficient than that of conventional hand polishing and can help prevent cobalt oxidation.

This paper describes a procedure for preparing packaged GaN devices for photon emission microscopy from the backside, which has proven to be an effective method for isolating faults. The deprocessing technique was developed for GaN devices formed on thick p ++ silicon substrates mounted in quad-flat no-lead (QFN) packages connected by gold wires. It consists of mechanical polishing, which removes backside metal and packaging material, and selective etching, which quickly etches the silicon while leaving the gold wires intact for electrical measurements. The authors describe each step of the process in detail and explain how emission spots are marked with a UV laser and analyzed in a FIB-SEM system to determine the underlying cause of failure.

This paper presents a large-volume workflow for fast failure analysis of microelectronic devices. The workflow incorporates a stand-alone ps-laser ablation tool and a FIB-SEM system. As implemented, the picosecond laser is used to quickly remove large volumes of bulk material while the Xe plasma FIB provides precise end-pointing to the feature of interest and fine surface polishing after laser ablation. The paper presents several application examples, including a full workflow to prepare artefact-free, delamination-free cross-sections in an AMOLED mobile display and the preparation of devices and packages (including flip chips) of varying size. It also covers related issues such as CAD navigation, data correlation, and the use of bitmap overlays for end-pointing.

This paper describes how electron beam induced current (EBIC) analysis is used to determine the doping profile of p-n junctions and identify defective devices. The limitations of both chemical etching and EBIC are discussed as is the use of ion milling as a potential method for enhancing resolution. The findings in this paper add to the understanding of EBIC and provide insights to further improvements in its use in failure analysis.

This paper presents a die-level sample preparation technique that uses selective etch chemistry and laser interferometry to expose the entire top metal layer surface for electrical fault isolation. It also describes a novel e-beam based probing technique called StaMPS which is used to isolate logic structure failures through SEM image contrasts. By landing SEM probe tips on exposed metal pads and controlling logic states via an applied bias, different levels of contrast are created highlighting structural failure locations. Die-level sample preparation combined with e-beam fault isolation optimizes turnaround time by delayering die in less than an hour and by locating several types of defects in a single sample.

Integrated circuit (IC) delayering workflows are highly reliant on operator experience to determine processing end points. The current method of end point detection during IC delayering uses qualitative correlations between the thickness and color of dielectric films observed via optical microscopy. The goal of this work is to quantify this relationship using computer vision. As explained in the paper, the authors trained a convolutional neural network to estimate the thickness of dielectric films based on images and measurements recorded during processing. The trained vision model explained 39% of the variance in dielectric film thickness with a mean absolute error of approximately 47 nm. The paper describes the entire workflow, including verification testing, and addresses the primary sources of error.

Global thinning is a technique that enables backside failure analysis and radiation testing. In some devices, it can also lead to increased thresholds for single-event latchup and upset. In this study, we examine the impacts of global thinning on 28 nm node FPGAs. Test devices are thinned to 50, 10, and 3 μm via CNC milling. Lattice damage, in the form of dislocations, extends about 1 μm below the surface, but is removed by polishing with colloidal SiO2. As shown by finite-element modeling, thinning increases compressive global stress in the Si while solder bumps (in flip-chip packages) increase stress locally. The results are confirmed by stress measurements obtained through Raman spectroscopy, although more complex models are needed to account for nonlinear effects in devices thinned to 3 μm and heated to 125°C. Thermal imaging shows that increased local heating occurs with increased thinning, but the maximum temperature difference across the 3-μm die is less than 2°C. Ring oscillators throughout the FPGA fabric slow about 0.5% after thinning and another 0.5% when heated to 125°C, which is attributed to stress changes in the Si.

This paper presents a method that allows top view SEM inspection on GaN devices previously subjected to PEM analysis from the backside and the associated sample preparation procedures. By filling the backside cavity with glob-top resin and epoxying the device to a piece of silicon, it is possible to remove all covering layers with a sequence of wet etches. A dried Ag liquid strap eliminates SEM charging problems and backside laser marks are made visible from the front side using an IR wavelength. The paper describes each step of the process in detail along with the results of the frontside SEM inspection.

This paper explains how the authors determined the cause of a fast-to-rise failure discovered during scan chain testing of an image sensor. The failed device was mounted on a portable card that facilitates transfer between test platforms in an electro-optical probing (EOP) system. Initial fault localization was conducted through backside PEM, but the results were inconclusive. The part was then analyzed on a digital scan chain tester to check for flaws in the daisy chain of shift registers. Through broken scan chain analysis, the potential cause of the problem (a failing flip-flop) was narrowed down to a few chain links and ultimately pinpointed using EOP fault isolation techniques. The failed device was then deprocessed by parallel lapping and analyzed in a SEM, revealing a broken poly gate as the physical cause of failure.

The journey to the circuit layer will be described by first discussing baseline processes of laser assisted chemical etching (LACE) steps before the focused ion beam (FIB) workflow. These LACE processes take advantage of a dual 532 nm continuous wave (CW) and pulse laser system, however limitations and overhead that is transferred over to the FIB operator will be demonstrated. Experiments show an additional third 355 nm ultraviolet (UV) pulse laser process introduction into the workflow can further reduce the remaining silicon thickness (RST) relieving FIB overhead. In addition, complex pulse laser patterning techniques will show a refinement to nonuniform produced silicon. Finally, other pulse laser patterning techniques such as polygon etch capability will allow laser etching around and in-between features to enhance circuit layer accessibility for debug operations.

Physical FA innovations in advanced flip-chip devices are essential, especially for die-level defects. Given the increasing number of metal layers, traditional front-side deprocessing requires a lot of work on parallel lapping and wet etching before reaching the transistor level. Therefore, backside deprocessing is often preferred for checking transistor-level defects, such as subtle ESD damage. This paper presents an efficient technique that involves precise, automated die thinning (from 760µm to 5µm), high-resolution fault localization using a solid immersion lens, and rigorous KOH etch. Using this technique, transistor-level damage was revealed on advanced 7nm FinFET devices with flip-chip packaging.

Three-dimensional device (FinFET) doping requirements are challenging due to fin sidewall doping, crystallinity control, junction profile control, and leakage control in the fin. In addition, physical failure analyses of FinFETs can frequently reach a “dead end” with a No Defect Found (NDF) result when channel doping issues are the suspected culprit (e.g., high Vt, low Vt, low gain, sub-threshold leakage, etc.). In new technology development, the lack of empirical dopant profile data to support device and process models and engineering has had, and continues to have, a profound negative impact on these emerging technologies. Therefore, there exists a critical need for dopant profiling in the industry to support the latest technologies that use FinFETs as their fundamental building block [1]. Here, we discuss a novel sample preparation method for cross-sectional dopant profiling of FinFET devices. Our results show that the combination of low voltage (<500eV), shallow angle (~10 degree) ion milling, dry etching, and mechanical polishing provides an adequately smooth surface (Rq<5Å) and minimizes surface amorphization, thereby allowing a strong Scanning Capacitance Microscopy (SCM) signal representative of local active dopant (carrier) concentration. The strength of the dopant signal was found to be dependent upon mill rate, electrical contact quality, amorphous layer presence and SCM probe quality. This paper focuses on a procedure to overcome critical issues during sample preparation for dopant profiling in FinFETs.

Focused Ion Beam sample preparation for electron microscopy often requires large volumes of material to be removed. Prior efforts to increase the rate of bulk material removal were mainly focused on increasing the primary ion beam current. Enhanced sputtering yield at glancing ion beam incidence is known, but has not found widespread use in practical applications. In this study, etching at glancing ion beam incidence was explored for its advantages in increasing the rate of bulk material removal. Anomalous enhancement of material removal was observed with single raster etching in along-the-slope direction with toward-FIB raster propagation at glancing ion beam incidence. Material removal was inhibited with raster propagation away from FIB. The effects of glancing angle and ion dose on depth of cut and volume of removed material were also recorded. We demonstrated that the combination of single-raster etching in along-the-slope direction by raster propagating toward-FIB at glancing incidence and a “staircase” type of etching strategy holds promise for reducing the process time for bulk material removal in FIB sample preparation applications.

Advanced packages such as 2.5D will continue to grow in demand as performance increases are needed in various applications. Failure analysis must adapt to the changes in the interfaces, materials and structures being developed and now utilized. Traditional techniques and tools used for selectively removing materials to isolate and analyze defects need to evolve alongside these packages. A CF4-free Microwave Induced Plasma (MIP) process is used to remove underfill (UF) with minimal alteration of other materials on the samples, a process which has become more difficult on 2.5D modules. UF is removed using this MIP process to allow subsequent analysis on interposer interconnects and ìbumps in crosssection. SEM inspection, Electron Beam Absorbed Current (EBAC), and FIB are techniques used post cross-sectional UF removal of these 2.5D structures. The benefits of the specific MIP process through case studies are presented. Specifically, the use of an automatic cleaning step and a CF4-free downstream O2 plasma allow easy removal of UF without damaging other structures of interest with little tool recipe development.

Focused Ion Beam (FIB) circuit edit allows for rapid prototyping of potential semiconductor design changes without the need to run a full manufacturing cycle in a semiconductor Fab. By FIB editing a completed module, thorough testing on the bench or in a full system can be achieved. Logic can be toggled, validation of speed enhancements performed, and constructive and destructive failure analysis can be enabled. In order to fulfill all the needs of clients in a rapidly evolving SOC driven market, simply modifying existing devices by “rewiring” circuits is becoming insufficient. Often the team is tasked with making very repeatable structures to aid the circuit analysis group. These include relatively precise resistors for tuning RF circuits (part of an RC network), adding known loads or delays, et cetera. Naturally resistive FIB deposited metal lines connected to the existing circuitry can be used in this capacity. FIB chip edit is considered to be a “Direct Write” process. The beam pattern in conjunction with process gases defines the regions of milling and deposition. Unfortunately, FIB edit is rarely an exact science. In many cases, a number of characteristics seem to be outside the realm of precise repeatable control. This is evident not only in individual tool operational logs but also in FIB tool matching, where maintaining identical system performance within the lab is difficult or nearly impossible. These characteristics are highly dependent on precursor reservoir composition and flow, surface adsorption conditions, beam patterning integrity, and the total interaction space of competing back sputtering during the new material structure formation. Due to these factors, the shape, composition and electrical performance of metal and insulator depositions vary over an often unacceptable range. As a result, we were not meeting the needs of some critical customer applications. Direct written precision resistive structures displayed several issues for which iterative edits were required to compensate for variability. When attempting to create an exact resistance, this process was not reliable, nor was it repeatable enough for accurate circuit performance trimming. Space-constrained serpentine resistors or multiple discrete resistors side-by-side showed the greatest process variability. Metal deposition processes tend to be somewhat self-limiting, so thick boxprofile lines are difficult to form. Conductive material deposited outside of the pattern definition (overspray) results in line-to-line leakages. Attempts to remove the overspray thru ion beam assisted etch-back tends to damage the deposited conductors and underlying insulators. The low-k region between lines can become cross-linked, experience gallium doping, and become tungsten impregnated. This lowered the resistivity of the insulator, increased the resistivity of the conductor, and produced variability in the device which was especially an issue when dealing with varying initial substrates. GLOBALFOUNDRIES began a project to create a more robust repeatable resistive structure by removing several variables. Rather than direct writing lines onto a top surface layer, a confined deposition based on the concepts of dual damascene processing used with copper layers in modern semiconductor fabrication will be employed. The damascene process begins with the definition of a box to be filled with a conductive material. The process of ion beam gas assisted anisotropic etching/milling has a far more predictable outcome than ion beam induced deposition. It is possible to create a surface box mill or even a deep drilled via of desired dimensions with a more consistent repeatability. Deposition of tungsten into a confined region using, for example, a W(CO)6 precursor and a Ga+ ion beam results in an excellent via fill. Using this behavior, precision resistors can be created with metal deposition within the trenches which are created by the gas assisted mill. An enclosed space can be filled nearly void-free, and has repeatable electrical parameters. The self-limiting factors with tungsten deposition go away as sputtered material becomes trapped within the well resulting in a near limitless Zheight potential. The constant dielectric with a uniform and contained tungsten fill can allow for a well-defined resistivity for the FIB deposited tungsten material. Having a known resistivity, calculation of dimensions for resistive and inductive structures during the design process becomes feasible. With process variability under control, structures can be formed reliably enough to offer this as a service to customers.