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Wear testing
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Proceedings Papers
IFHTSE2024, IFHTSE 2024: Proceedings of the 29th International Federation for Heat Treatment and Surface Engineering World Congress, 97-106, September 30–October 3, 2024,
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High-entropy alloys (HEA) are multinary alloys obtained by blending at least five metallic elements in compositions close to their isoatomic fractions (5–35 at%). Generally, HEAs are produced by arc melting and casting. However, the cast specimens undergo phase separation and have a non-uniform microstructure. In contrast to ingot metallurgy, powder metallurgy has several advantages such as the possibility of alloying metals with high melting points and large differences in melting points and specific gravity. Therefore, we investigated the preparation of HEAs by mechanical alloying (MA), which produces an alloy powder with a uniform microstructure, followed by consolidation by spark plasma sintering (SPS). In this study, CoCrFeNiTi HEA sintered after MA-SPS was subjected to direct current plasma nitriding with screen (S-DCPN) to evaluate the characteristics of the nitrided layer as a function of nitriding temperature. Ball milling with heptane in an argon atmosphere using pure powders of Co, Cr, Fe, Ni, and Ti as raw materials was performed for 50 h. Subsequently, sintered compacts were prepared by SPS and treated with S-DCPN at 673, 773, and 873 K for 15 h in 75% N 2 –25% H 2 at a gas pressure of 200 Pa. A screen made of austenitic stainless steel SUS316L was installed as an auxiliary cathode to ensure uniform heating and nitrogen supply during the plasma nitridation process. Then, X-ray diffraction test, cross-sectional microstructure observation, surface microstructure observation, cross-sectional hardness test, roughness test, glow discharge optical emission spectrometry, corrosion test, and wear test were performed on the nitrided samples. The corrosion test results demonstrated that corrosion resistance increased with decreasing nitriding temperature. Furthermore, the results of the roughness and wear tests confirmed that abrasive wear occurred on the specimens nitrided at 873 K.
Proceedings Papers
HT 2019, Heat Treat 2019: Proceedings from the 30th Heat Treating Society Conference and Exposition, 166-176, October 15–17, 2019,
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Controlled nitriding and ferritic nitrocarburizing can significantly improve the corrosion and wear resistance of carbon and low-alloy steels. The framework for maintaining these processes is based on standards, such as AMS 2759/10 and 2759/12A, that specify tolerances for control parameters. This work investigates the impact of admissible deviations in control parameters on the performance of treated alloy samples. The findings of the study demonstrate that although tolerances are allowed, precise control in specific furnace classes is necessary to consistently obtain superior results.
Proceedings Papers
Rafael Magalhães Triani, Lucas Fuscaldi De Assis Gomes, Luiz Carlos Casteletti, Amadeu Lombardi Neto, George Edward Totten
HT 2019, Heat Treat 2019: Proceedings from the 30th Heat Treating Society Conference and Exposition, 200-206, October 15–17, 2019,
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This work investigates the effect of boriding and thermo-reactive deposition on 15B30 steel. The results presented in the paper show that these thermochemical treatments produce boride and carbide rich layers that improve surface hardness and wear resistance, and they do so without the adverse effects of adding more boron to the alloy.
Proceedings Papers
HT2015, Heat Treat 2015: Proceedings from the 28th Heat Treating Society Conference, 383-389, October 20–22, 2015,
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In the recent years, there has been a remarkable increase in the use of deep cryogenic treatment (DCT) for enhancing performance of tool steels. It is a supplementary treatment where components are treated below subzero temperatures for several cryo-soaking hours. This paper focuses on to study the effect of deep cryogenic treatment and cryo-soaking time on microstructural and mechanical properties of AISI H-13 tool steel. Deep cryogenic treatment at different cryo-soaking time (16-48 hours) were applied and tool steel performance was analyzed by using mechanical, fatigue and wear testings. The microstructural evolutions during DCT were evaluated by using scanning electron microscope (SEM). It was observed that microstructural modifications like increase in carbide density, fine and uniform martensitic structure during DCT had significantly improved properties which were influenced by cryo-soaking time.
Proceedings Papers
Fábio Edson Mariani, Gustavo Bortoluci de Assis, Luiz Carlos Casteletti, Amadeu Lombardi Neto, George Edward Totten
HT2015, Heat Treat 2015: Proceedings from the 28th Heat Treating Society Conference, 692-695, October 20–22, 2015,
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Gray cast iron is primarily used for its low cost, high damping capacity, and excellent machinability. These properties are attributed to the presence of free graphite and the high fluidity of the molten metal, which allows for the easy casting of complex parts with thin walls. Applying suitable coatings can enhance wear resistance and broaden the material's range of applications. Niobium carbide, known for its high hardness, is a promising candidate for this purpose. In this study, samples of gray cast iron with the composition 3.47% C, 2.39% Si, 0.55% Mn, 0.15% Ni, 0.65% Cu, and the balance Fe were subjected to a niobizing powder thermo-reactive diffusion treatment. The coating mixture consisted of ferro-niobium, NH 4 Cl, and Al 2 O 3 , and the treatment was conducted at 900 °C for 2 hours. The resulting layers exhibited hardness values of 2000 HV, characteristic of niobium carbides. Micro-adhesive and micro-abrasive wear tests showed a significant increase in wear resistance due to this treatment.