This study presents a method to reduce thermal distortion in tubular automotive stabilizer bars by replacing batch furnace heating with individual conductive heating and implementing a press-quenching technique with a seven-point clamping fixture. Using finite element analysis, researchers optimized the clamping system to maintain critical dimensional tolerances while addressing the challenges of inhomogeneous temperature distribution through a programmed current profile. Statistical analysis confirmed significant improvement in dimensional stability compared to conventional quenching.

This study investigates the interaction between tempering processes and the formation of tempering transformation induced plasticity (T-TRIP) in 50CrMo4 steel during laser heat treatment. Various configurations, including single and double laser treatments, were examined along with different initial material states and heat treatment parameters.

This study focuses on evaluating the transferability of an established induction heat treatment simulation model to the sintered steel Fe-1.8%Cr-0.6%C (Astaloy CrA). As the porosity affects the electromagnetic, thermal and metallurgical material behavior during induction hardening, these material properties were experimentally determined as a function of temperature across all relevant phases.

This study examines the impact of thermal post processing, specifically induction hardening and tempering, on the fatigue performance of laser powder bed fusion (PBF-LB) manufactured AISI 4140 steel. Results highlight the importance of porosity control, with induction hardening effectively addressing near-surface porosity issues in non-machined parts.

To develop a behavior model, properties such as Young's modulus, viscous stress, kinematic hardening, isotropic hardening, yield strength and transformation-induced plasticity parameter (TRIP) for austenite and martensite were determined using a specially developed experimental set-up.

In this study, a single-sided carburized Almen strip made of Pyrowear 675 is used to investigate the effect of phase transformations on quench hardening distortion. Computer modeling is used to analyze the collected experimental data and demonstrate the underlying principles of distortions and residual stress.

This paper provides insights into the type and severity of gear distortions on each tooth during gap-to-gap hardening. The study compares distortions in gears from different manufacturing processes post-induction hardening and conventional case hardening. Analysis shows noticeable differences between induction hardened and reference steel in profile slope deviation, adjacent pitch deviation, and runout error, primarily linked to the induction hardening process.

This study focuses on replacing traditional gas-fired furnaces with sustainable low-pressure carburizing (LPC) and gas cooling methods. The project leverages advanced computational tools for predicting quenching outcomes (e.g., cooling rates, material properties, and distortions) to enable sustainable and efficient production.

Metal additive manufacturing is a molding method with a high degree of freedom because it can be created from high-strength materials using by CAD, etc. In recent years, there is a demand for metal additive manufacturing due to the demand for more complex mechanisms and shape in industrial products. However, the mechanical properties of metal additive manufacturing materials as metallic materials are not clear compared to metallic materials by melting method. In this study, two types of metal additive manufacturing (AM) materials with different lamination directions are carburized and heat treated to clarify the differences from general metallic materials and to clarify the causes. The carburized AM materials were confirmed to have a surface hardness of 550HV and a total carburization depth of 200 μm, but the amount of carburization differed depending on the orientation. In addition, when analyzed with a SEM, a metal structure was formed in an equiaxed crystal shape, and segregation of metal elements was observed.

It is well known that the maximum prior austenite grain size after carburizing heat treatment is approximately positively correlated with the maximum shear strain in the case of simple deformation of pre process as cold working treatment. On the other hand, it is generally known that the maximum shear strain and the maximum grain size do not correspond when complex cold working is performed, but the reason of these phenomena is not well known. Then, it is necessary to investigate the relationship between the applied strain during cold working with multiple steps and prior austenite grain size after heat treatment(GG). In this study, we used a processing method called HPT processing, which introduces shear strain by torsion deformation under applying high hydrostatic pressure to the top and bottom of a disk-shaped sample using a die, and investigated how GG changes due to the accumulation of dislocations by focusing on the strain amount | ± Δ ε| given in one pass controlled by a processing path called Cyclic-HPT (c-HPT) (4) and the total strain amount 𝛴| ± Δ ε| given to the sample by the accumulation of one pass. As a result, when finer strain is applied, the grain size does not necessarily become smaller, but rather there are boundary conditions that indicate the positive and negative grain size with respect to the number of strains. Similarly, for the grain size distribution, an increase and decrease in grain size was observed with respect to radial distance, so there are boundary conditions that indicate the positive and negative grain size with respect to distance. From these results, it is believed that this may be the mechanism for grain growth behavior in the case of cold working, which involves complex deformation.

This presentation will discuss the most common types of induction tooling failures and the best practices to improve the performance and longevity of inductor coils, bus bars quenches and related tooling. We will discuss the harsh environment of a typical induction machine installation and what can be done to reduce contamination, which is the leading cause of tooling failure. Robust tooling designs and how water cooling is essential to longevity shall be discussed. Cooling water temperature and how the water is presented and routed through the tooling components and the impact this has on performance and longevity shall be discussed. We will discuss the use of proper materials, fittings and hoses which are often overlooked and can be detrimental to a process if not correctly selected. We will cover the induction machine and how it is essential to have a proper earth ground and the importance of proper machine fixturing and alignment. We shall discuss the importance of scheduled machine maintenance, scheduled service and calibration. The presentation will summarize the most common types of failures, how maintenance is essential for longevity and the importance of high-quality robust tooling.

Induction surface hardening is a process often used in industrial applications to efficiently increase the lifetime of components. Recently, this process has been enhanced with the inductive short time austempering process, creating a martensitic-bainitic microstructure. It is well-known that in homogeneous mixed microstructures, an optimally adjusted volume fraction of bainite can significantly increase the lifetime of the components even further. Regarding inductive short time austempering, there is a lack of knowledge in characterizing and differentiating graded microstructures, which occur due to the temperature gradients within the process. Therefore, three methods were investigated: the analysis of the grayscale profile of metallographic sections, the hardness profile and the full width at half maximum (FWHM) profile from the intensity curve (rocking curve) of the X-ray diffraction pattern. These methods were initially applied to homogeneous structures and evaluated. The findings were then transferred to graded microstructures. Finally, the graded microstructures could be differentiated both via the hardness profile and the FWHM value, while the grayscale analysis only allowed qualitative statements to be made. It became evident that both the volume fractions and their structure are crucial for subsequent mechanical characterization. Since the martensitic microstructure is easier to identify, it serves as a reliable reference for evaluating the mixed microstructure. In summary, these findings offer the foundation for further characterization of graded martensitic-bainitic mixed microstructures.

Laser heat treating on Automotive stamping and trim dies has resulted in overall cost reductions, shorter processing times, improved quality. These improved results have resulted in multiple advantages for Original Equipment Manufacturers (OEMs) that use Laser Heat Treating when compared with OEMs treating identical dies with conventional methods. This article highlights the technical aspects of Laser Heat Treating, cost saving, and latest advancements associated with this process.

Gas carburizing with quenching is one of the most useful heat treatment processes for steel parts. However, after quenching distortion is still occurs. The nitriding and nitrocarburizing are the surface hardening heat treatment methods with low distortion, but these methods require the long treating time to obtain a thick hardened layer. Austenitic nitriding and quenching (ANQ) solves these problems. In ANQ process, nitrogen is infiltrated into the steel parts in austenite phase, and they are quenched to harden. The ANQ process can also be applied to cheap low carbon steel such as the Cold Rolled Carbon Steel Sheet. In this study, the effect of ANQ on mechanical properties was examined. For infiltrating the nitrogen into the steel parts, the steel parts were heating to 750°C or higher in an ammonia atmosphere and heating to 750°C or higher in a nitrogen glow discharge. After the ANQ process, hardness profiles, structure, nitrogen and carbon concentration profiles were observed. Also, distortion, tribological properties, impact value and fatigue strength were examined. The effective case depth, which is treated by ANQ, is larger than the effective case depth of gas nitrocarburizing for same period of time. Distortion of ANQ is much smaller than that of gas carbonitriding, and it is almost equal with that of gas nitrocarburizing. The seizure load is same as with other surface hardening heat treatment processes. The wear loss of ANQ is a lower, in the amount of about 1/2 that of the carbonitrided specimen and 1/3 that of the gas nitrocarburized specimen. The ANQ is an effective heat treatment process for parts which require wear resistance. The tempering softening resistance is improved by nitrogen infiltration. ANQ also improves the impact value and fatigue strength.

High-entropy alloys (HEA) are multinary alloys obtained by blending at least five metallic elements in compositions close to their isoatomic fractions (5–35 at%). Generally, HEAs are produced by arc melting and casting. However, the cast specimens undergo phase separation and have a non-uniform microstructure. In contrast to ingot metallurgy, powder metallurgy has several advantages such as the possibility of alloying metals with high melting points and large differences in melting points and specific gravity. Therefore, we investigated the preparation of HEAs by mechanical alloying (MA), which produces an alloy powder with a uniform microstructure, followed by consolidation by spark plasma sintering (SPS). In this study, CoCrFeNiTi HEA sintered after MA-SPS was subjected to direct current plasma nitriding with screen (S-DCPN) to evaluate the characteristics of the nitrided layer as a function of nitriding temperature. Ball milling with heptane in an argon atmosphere using pure powders of Co, Cr, Fe, Ni, and Ti as raw materials was performed for 50 h. Subsequently, sintered compacts were prepared by SPS and treated with S-DCPN at 673, 773, and 873 K for 15 h in 75% N 2 –25% H 2 at a gas pressure of 200 Pa. A screen made of austenitic stainless steel SUS316L was installed as an auxiliary cathode to ensure uniform heating and nitrogen supply during the plasma nitridation process. Then, X-ray diffraction test, cross-sectional microstructure observation, surface microstructure observation, cross-sectional hardness test, roughness test, glow discharge optical emission spectrometry, corrosion test, and wear test were performed on the nitrided samples. The corrosion test results demonstrated that corrosion resistance increased with decreasing nitriding temperature. Furthermore, the results of the roughness and wear tests confirmed that abrasive wear occurred on the specimens nitrided at 873 K.

In recent years, physical vapor deposition and chemical vapor deposition (CVD) methods have made significant advancements due to the growing demand for surface modification technologies. This study focuses on depositing diamond-like carbon (DLC) as a thin, hard film using plasma-enhanced CVD. DLC possesses properties such as high hardness, low friction, wear resistance, and chemical stability. However, a drawback is low adhesion caused by residual stress and differences in hardness between the film and the substrate material. Therefore, efforts are underway to improve adhesion by introducing a DLC intermediate layer containing metallic elements to reduce residual stress or by applying treatments to harden the substrate material, such as nitriding or carburizing. Active screen plasma nitriding (ASPN) is a nitriding method that eliminates edge effects and electrically insulates the sample during the process. However, during nitriding, deposits can cover the sample and slow down the nitriding rate. To address this, a nitriding method called "direct-current plasma nitriding with screen (S-DCPN)" has been developed. It involves applying a voltage to the sample and screen during ASPN to remove deposits via sputtering action, thereby increasing the nitriding rate. Although the duplex process of ASPN and DLC-coating deposition has been studied, there are limited reports on the duplex process with S-DCPN. This study investigates the effect of intermediate layer composition on mechanical properties by forming a nitrided layer on the surface of SUS304 through S-DCPN treatment, depositing a Si-DLC intermediate layer with varying compositions, and applying a DLC film on the top surface. The results demonstrate that the lower the Si ratio in the Si-DLC intermediate layer, the better the wear resistance. Furthermore, the study reveals that wear resistance and adhesion were improved compared to samples without S-DCPN treatment.

Surface modification involves the chemical or physical impartation of enhanced functionality to the surface of materials, and has become increasingly important in recent years. Nitriding is a surface modification method that hardens the surface of metallic materials by causing nitrogen to permeate and diffuse into the surface to form various nitrides or by supersaturating a solid solution of nitrogen in the metal. This is effective in improving the hardness, corrosion resistance, and wear resistance. Plasma nitriding, a type of nitriding process, has several advantages, such as low energy consumption, short processing time, and low environmental impact. In contrast, the conventional plasma nitriding method forms plasma on the surface of the treated material, which may cause phenomena that lead to defects in the treated material. Therefore, the directcurrent plasma nitriding with screen (S-DCPN) method reduces these problems because plasma is formed not only on the treated material but also on the surface of the screen. Stainless steel has excellent corrosion resistance; however, nitriding treatment above a certain temperature reduces the corrosion resistance owing to chromium nitride precipitation. In this study, the S-DCPN treatment, a type of plasma nitriding method, was applied to form a thick nitrided layer without reducing corrosion resistance. The S-DCPN treatment was performed using ferritic stainless steel SUS430 as the sample and austenitic stainless steel SUS304 as the screen material at treatment temperatures of 633 and 653 K, treatment times of 5 and 15 h, a gas pressure of 200 Pa, and a gas composition of 75% N 2 - 25% H 2 . Consequently, the α N phase with supersaturated nitrogen solid solution was identified under all conditions. Nitrogen diffusion and hardness increased with increasing treatment temperature and time. In the corrosion tests, corrosion resistance improved under all conditions.

Heat treatment of steels is a process of modifying the mechanical properties by solid-state phase transformations or microstructural changes through heating and cooling. The material volume changes with phase transformations, which is one of the main sources of distortion. The thermal stress also contributes to the distortion, and its effect increases with solidstate phase transformations, as the material stays in the plastic deformation field due to the TRIP effect. With the basic understanding described above, the sources of distortion from a quench hardening process can be categorized as: 1) nonuniform austenitizing transformation during heating, 2) nonuniform austenite decomposing transformations to ferrite, pearlite, bainite or martensite during quenching, 3) adding of carbon or nitrogen to the material, and forming carbides or nitrides during carburizing or nitriding, 4) coarsening of carbide in tempered martensite during tempering, 5) stress relaxation from the initial state, 6) thermal stress caused by temperature gradient, and 7) nonhomogeneous material conditions, etc. With the help of computer modeling, the causes of distortion by these sources are analyzed and quantified independently. In this article, a series of modeling case studies are used to simulate the specific heat treatment process steps. Solutions for controlling and reducing distortion are proposed and validated from the modeling aspect. A thinwalled part with various wall section thickness is used to demonstrate the effectiveness of stepped heating on distortion caused by austenitizing. A patented gas quenching process is used to demonstrate the controlling of distortion with martensitic transformation for high temperature tempering steels. The effect of adding carbon to austenite on size change during carburizing is quantified by modeling, and the distortion can be compensated by adjusting the heat treat part size.

The purpose of this study is to clarify the mechanical properties of the expanded austenite (S phase) formed in austenitic stainless steel (ASS). A small thin rolled plate of SUS304 with 0.5 mm thickness was used as test sample. The test sample was nitrided by active screen plasma nitriding (ASPN) at low processing temperature of 400 °C and 450 °C during 4 h processing time. S phase was formed on the surface of the test sample. The surface hardness of ASPN sample was higher than that of untreated sample. Furthermore, tensile tests and fracture surface observations revealed that the tensile strength was also improved compared to untreated samples.

Steel hardening is a long-standing practice that has accompanied human development over the last three millennia. For hardening, steel is heated to a high temperature to form austenite and subsequently cooled. During cooling, austenite transforms into various microstructural products, e.g. grain boundary ferrite, Widmanstätten ferrite, massive ferrite, pearlite, upper bainite, lower bainite,… and martensite. Martensite is the hardest of these products and is obtained when the applied cooling rate exceeds a critical value. This critical cooling rate for martensite formation is determined by the chemistry of the steel and is significantly reduced by increasing the content of alloying elements. Cooling from the austenite region by immersing the parts in water, generally provides this cooling condition. The transformation that leads to martensite is called martensitic and, unlike all other transformations that occur in steel, it does not involve the diffusion of atoms. Martensitic transformations begin when a characteristic temperature, the martensite start temperature Ms is reached during cooling. Ms is essentially determined by the chemical composition of the steel. Subsequently, martensitic transformations continue during further cooling below Ms. In contrast, no transformation occurs when the steel is held isothermally below Ms, indicating that the transformation is time independent, i.e. athermal. Consistently, martensitic transformations would not be suppressible, not even by applying the most rapid cooling possible.