Residual stresses are unavoidable in heat treatment and surface engineering and their presence can be advantageous or disastrous for the performance of components. Residual stresses cannot be measured directly, but are determined from strain measurements, either non-destructively from diffraction-based methods, or destructively from relaxation-based methods. In this presentation, three examples of stress determination from strain measurements showcase some of the possibilities. In the first example lattice strains are determined with energy dispersive analysis with synchrotron radiation in relation to the phase fraction during martensite formation in a soft martensitic stainless steel. The second example shows synchrotron lattice determination with energy dispersive analysis during in-situ tensile loading of super martensitic stainless steel containing reverted austenite. The third example concerns determination of residual stresses in internally oxidized bulk metallic glass with laboratory X-ray diffraction analysis of lattice strains and displacements by stress relaxation during incremental ring-core excavation of micron-scale columns with focused ion beam milling in an SEM.

Carburizing and induction hardening are two surface heat treatments commonly used to increase wear resistance and fatigue performance of steel parts subject to cyclical torsional loading. It was originally hypothesized that performing an induction surface hardening heat treatment on parts previously carburized could provide further increased fatigue life, however initial torsional fatigue results from previous work indicated the opposite as the as-carburized conditions exhibited better torsional fatigue strength than the carburized plus induction surface hardened conditions. The aim of this work is to further elucidate these torsional fatigue results through metallography and material property characterization, namely non-martensitic transformation product (NTMP) analysis, prior austenite grain size (PAGS) analysis, and residual stress vs depth analysis using x-ray diffraction (XRD). A carburizing heat treatment with a case depth of 1.0 or 1.5 mm and an induction hardening heat treatment with a case depth of 0, 2.0, or 3.0 mm were applied to torsional fatigue specimens of 4121 steel modified with 0.84 wt pct Cr. The carburized samples without further induction processing, the 0 mm induction case depth, served as a baseline for comparison. The as-received microstructure of the alloy was a combination of polygonal ferrite and upper bainite with area fractions of approximately 27% and 73% respectively. The only conditions that exhibited NMTP were the as-carburized conditions. These conditions also exhibited larger average PAGS and higher magnitude compressive residual stresses at the surface compared to the carburized plus induction hardened conditions. The compressive residual stresses offer the best explanation for the trends observed in the torsional fatigue results as the conditions with NMTP present and larger PAGS exhibited the best torsional fatigue performance, which is opposite of what has been observed in literature.

The proposition that compressive residual stresses are beneficial in improving the service life of components subject to rolling contact fatigue is well documented. However, the exact nature of the relationship between effective case depth (ECD) and the residual stress state is not well understood for components with deep case depth (>0.050inches, 1.27mm). It is expected that compressive residual stresses will gradually transition to tensile stresses as the case depth increases beyond a threshold value. In addition, the strain-induced transformation of retained austenite and its influence on the residual stress state of components resulting from service was explored. This study measured the residual stress state of components prepared with various ECD before and after simulated service with the goal of determining where the compressive to tensile transition occurs. Residual stress and retained austenite measurements were conducted using X-ray diffraction.

Direct metal laser sintering (DMLS) is an established technology in metal additive manufacturing. This complex manufacturing process yields unique as-built material properties that influence mechanical performance and vary with different machine parameters. Part porosity and residual stresses, which lead to part failures, and grain structure, as it relates to mechanical properties and anisotropy of DMLS parts, require investigation for different print settings. This work presents results for density, residual stress, and microstructural inspections on designed test artifacts for the benchmarking of 3D metal printers. Results from printing artifacts on two separate DMLS printer models with default parameters show highly dense parts for both printers, with relative densities above 99.5%. Characterization of residual stress through cantilevered deflection specimens indicates similar resulting thermal stresses developed in both build processes, with deflection averages of 32.48% and 28.09% for the respective machines. Additionally, properties of the test artifact printed after adjusting default machine parameters for equal energy density are characterized.

Computer simulations are increasingly being used in the automotive industry to evaluate the state of stress in cylinder blocks during casting and heat treat processes. With recent advancements, it is now possible to model casting and quenching processes as well as residual stress and high cycle fatigue. However, calculating the final stress in cylinder blocks requires the integration of several software tools with different meshing topologies, numerical methods, data structures, and post-processing capabilities. The intent of this research is to develop an integrated virtual engineering environment that combines casting simulation, computational fluid dynamics, and finite element methods in order to simulate the manufacturing process from the beginning of casting, through water quenching heat treatment, to engine dynamometer testing. The computational environment is built on three CAE tools, Magmasoft, AVL Fire, and Abaqus, and required considerable amounts of research and development to validate each numerical method and the tools that facilitate data exchange between them.

The cooling history of carburized heat-treated gears plays a significant role in developing microstructure, hardness, and residual stress in the tooth that influences the fatigue performance of the gear. Evaluating gear carburizing heat treatment should include a microstructure and hardened depth evaluation. This can be done on an actual part or with a test piece. The best practice for a test piece is to use a section size that closely approximates the cooling rate at the gear flank of the actual gear. This study furthers work already presented showing the correct test piece size that should be used for different gear modules (tooth thicknesses). Metallurgical comparisons between test pieces, actual gears, and FEA simulations are shown.

A gas quenching method was developed by DANTE Solutions, in conjunction with the U.S. Army Combat Capabilities Development Command Aviation & Missile Center (DEVCOM AvMC), to control distortion in difficult to quench geometries. This new method addresses the nonuniform cooling inherent in most gas quenching processes. A prototype unit was constructed and tested with the aim of controlling the martensite formation rate uniformity in the component being quenched. With the ability of the DANTE Controlled Gas Quenching (DCGQ) unit to control the temperature of the quench gas entering the quench chamber, thermal and phase transformation gradients are significantly reduced. This reduction in gradients yields a more uniform phase transformation, resulting in reduced and predictable distortion. Being able to minimize and predict distortion during gas quenching, post heat treatment finishing operations can be reduced or eliminated, and as such, fatigue performance can be improved. This paper will discuss the prototype unit performance. Mechanical testing and metallographic analysis were also performed on Ferrium C64 alloy steel coupons and will be discussed. The results obtained showed that the slower cooling rate provided by the prototype did not alter the microstructure, hardness, strength, ductility, toughness, or residual stress of the alloy.

Excessive distortion was observed in many small components made from 1080 steel that was neutral hardened following stamping. A study was then undertaken to determine how to reduce the distortion of the heat-treated parts while maintaining proper hardness and microstructure. A numerical simulation based on Simheat software was conducted to determine the effect of elevated temperature on the quenching oil used and its impact on distortion and microstructure. A second oil designed to operate at higher temperatures was also examined. Using Simheat software, the two oils were compared based on predicted distortion, hardness, and microstructure and the results were subsequently validated using empirical methods. It was concluded that a significant improvement in distortion could be achieved by using a different oil and higher quench temperatures.

The notion that compressive residual stresses can extend the service life of components subject to rolling contact fatigue is well documented. However, the exact nature of the relationship between effective case depth and the residual stress state is not well understood for components with case depths greater than 0.050 in. (1.27 mm). It is expected that compressive residual stresses gradually transition to tensile stresses as case depth increases beyond a threshold value. This study will measure the residual stress state of components with different case depths before and after simulated service in order to determine where the compressive to tensile transition occurs. It will also investigate the role of retained austenite and the effect of strain-induced transformation caused by rolling contact. Residual stress and retained austenite measurements will be conducted using X-ray diffraction.

Plain carbon steel cylinders were heat treated and quenched in order to study the effects of heat treating on residual stresses and microstructure. Residual stress measurements were obtained via X-ray diffraction using the sin 2 Ψ method and microstructure was characterized based on the associated peak widths. Measurements were made both at the surface and through depth following electropolishing. Triaxial stress gradients were observed in all test samples with concomitant varying microstructural characteristics. The method used to measure residual stresses in this study is typical and recommended for general practice.

Forging processes include various steps to attain favorable material properties such as heat treatment, rapid quench, cold work stress relieving, and artificial aging. These steps, however, also contribute to bulk residual stress. Excessive bulk residual stresses cause a wide of problems, including part distortion during machining and in use, reduced crack initiation life, increased crack growth rates, and an overall reduction in part life. This paper summarizes recent work aimed at measurement-based assessment of bulk residual stresses in cold-compressed aluminum die forgings. The results show that forging process induced residual stress is a repeatable phenomenon with RMS repeatability less than 5% of yield.

Undesired distortion can arise during machining of metals from two main mechanisms: 1) release of bulk residual stress in the pre-form, and 2) deformation induced by the cutting tool. The interaction between these two mechanisms is explored herein using aluminum plate-shaped samples that have a large surface with variations of bulk residual stress (BRS), where that surface is subsequently milled and we observe milling-induced residual stress (MIRS) and distortion. Plate samples are cut from two kinds of large blocks, one kind stress-relieved by stretching and a second kind that had been solution heat treated, quenched, and aged. MIRS is measured following milling using hole-drilling with fine depth increments. Distortions of thin wafers cut at the milled surfaces are used to show how the interactions between BRS and MIRS change milling-induced distortion. Data from the study show that the directions of MIRS and distortion relative to the milling direction are changed when milling in samples with high BRS magnitude (roughly ±100 MPa), with the direction of maximum curvature rotating toward or away from the milling direction depending on the sign and direction of BRS. High magnitude BRS increased distortion, nearly doubling the amount found compared to milling in samples free of BRS.

This paper provides an overview of the types of residual stress that engineers deal with and the tools and techniques available to measure it. It identifies the causes of manufacturing-induced residual stress along with their effects. It summarizes the practical aspects of a wide range of measurement methods, including hole drilling, layer removal, contour, lab XRD, and synchrotron analysis. It assesses current challenges and gaps in determining stress in relation to stress type, stress component, microstructure, specimen geometry, materials type, and measurement location.

In this work, the authors employ computer modeling to investigate a quenching process recently demonstrated at Karlsruhe Institute of Technology. A matrix of models was run to assess the effects of heat transfer and phase transformation kinetics on residual stress and microstructure in a relatively thick walled tube. The experiments at Karlsruhe were conducted using a high pressure water quench to produce martensite and residual compressive stress in the bore of a 4140 steel tube. Results show that the timing and rate of martensite formation and bainite kinetics have a significant effect on both the in-process and residual stress state.

This paper presents the preliminary results of experiments designed to mimic typical machining and thermal processing practices for aerospace titanium alloys. The most significant finding is that multiple side mill passes result in lower magnitude compressive stresses than a single side pass, which suggests that successive interactions with the milling tool serves to relieve residual stresses at the surface. The most likely mechanism for this is that Ti exhibits significant springback during machining, and multiple tool passes essentially remove the “springback” layer. Each successive removal of material allows stress relaxation in the remaining surface layer. By contrast, with only a single pass, surface residual stresses did not sufficiently relax.

Blade curving due to quenching in the Japanese sword has been recognized by swordsmiths through the ages. In the late 1920s, Hattori noted that the sword curving is induced from not only martensitic transformation expansion in the near-edge region but also non-uniform elastic and plastic strains distributed in the section, based on his experimental results using cylindrical specimens. Our research for an updated explanation on the subject prepared Japanese sword (JS) type specimens made of the same steel and process as the Japanese sword, and model JS (MJS) type specimens with the almost same shape as the JS type specimens, which were machined from commercial carbon steel and austenite stainless steel bars. All specimens quenched by a swordsmith using the traditional way showed a usual curved shape with different curvatures. Curving, temperature, hardness, metallic structure and residual stress measurements for the specimens were performed to prepare their future simulation works.

The development of residual stress in an induction hardened small spur gear is numerically simulated. A full scale 3D simulation is utilized to obtain the results, providing the possibility to evaluate the complete distribution of residual stress in the hardened component. Electromagnetic and thermal solutions under induction heating conditions are obtained with Cedrat Flux 3D, whereas EDF Code Aster software is used for thermal simulation during the quenching stage, phase transformation, and stress-strain simulations. The simulated induction heating isotherms and distribution of residual stress are compared with experimental investigations done by Larregain et al. and Savaria et al.

Air quenching is a common manufacturing process to produce high strength metal component by rapidly cooling heated parts in a short period of time. With the advancement of finite element analysis (FEA) methods, it has been possible to predict thermal residual stress by computer simulation. However, the accuracy of FEA calculation is bounded by the accuracy of the temperature data, acquired either by thermocouple measurement, experimentally calibrated heat transfer coefficient (HTC) method, or computational fluid dynamics (CFD) calculation. While CFD methods have gained popularity, the practicality of CFD method is reduced by tedious mesh generation and costly computation that is only feasible to be performed on a supercomputer. When quenching media is a gas-phased fluid and quenching flow is steady, the flow and temperature fields exhibit certain characteristics that could lead to the development of enhanced HTC method that is more computation efficient and yet produces more accurate temperature data.

Thermochemical surface engineering by nitriding/carburizing of stainless steel causes a surface zone of expanded austenite, which improves the wear resistance of the stainless steel while preserving the stainless behavior. As a consequence of the thermochemical surface engineering, huge residual stresses are introduced in the developing case, arising from the volume expansion that accompanies the dissolution of high interstitial contents in expanded austenite. Modelling of the composition and stress profiles developing during low temperature surface engineering from the processing parameters temperature, time and gas composition is a prerequisite for targeted process optimization. A realistic model to simulate the developing case has to take the following influences on composition and stress into account: - a concentration dependent diffusion coefficient - trapping of nitrogen by chromium atoms - the effect of residual stress on diffusive flux - the effect of residual stress on solubility of interstitials - plastic accommodation of residual stress. The effect of all these contributions on composition and stress profiles will be addressed.

The very nature of global sourcing means that components must carry clear and detailed specifications for material, heat treatment, and test methods. Qualified global heat treat facilities can achieve good control of not only the common features such as surface and gradient hardness, but also of microstructure, core hardness, residual stress, and other critical metallurgical parameters. This paper will discuss a new concept for material specifications and more detailed heat treatment specifications for the global marketplace.