Voids in fiber-reinforced composite materials are areas that are absent of the composite components: matrix (resin) and fibers. Voids have many causes but generally can be categorized as voids due to volatiles or as voids that result from entrapped air. This article describes the analysis of various types of voids. It reviews techniques for analysis of voids at ply-drops, voids due to high fiber packing, and voids that occur in honeycomb core composites. The final section of the article discusses void documentation through the use of nondestructive inspection techniques and density/specific gravity measurement methods.

Honeycomb-cored sandwich panels increase part stiffness at a lower weight than monolithic composite materials. This article illustrates an area of a honeycomb-cored sandwich structure composite cross section that is viewed using transmitted polarized light. This area shows the differences in the constituents and resin intermingling. The article discusses the factors that govern the honeycomb core movement and honeycomb core crush, with illustrations. Some common tests performed on honeycomb composites to characterize the skin-to-core bond strength are the climbing drum peel and flatwise tensile tests. The article concludes with a description on the reasons for core failure, which are analyzed after these tests.

This article outlines the requirements and methods associated with the inspection of brazements. It emphasizes the incorporation of these requirements into the overall quality system. The article reviews the acceptance limits, design limitations, and nondestructive and destructive inspection techniques involved in the brazement inspection. Selected case studies are also provided for further reference.

Visual examination, using the unaided eye or a low-power optical magnifier, is typically one of the first steps in a failure investigation. This article presents the guidelines for selecting samples for scanning electron microscope examination and optical metallography and for cleaning fracture surfaces. It discusses damage characterization of metals, covering various factors that influence the damage, namely stress, aggressive environment, temperature, and discontinuities.

Ultrasonic inspection is a nondestructive technique that is useful in both quality control and research applications for flaw detection in fiber-reinforced composite materials. This article describes ultrasonic nondestructive analysis by outlining its three basic types of scans. It reviews the important quality control techniques used during the manufacture of composite components by analyzing tooling control, material control, pattern orientation control, and in-process control.

This article describes how composite specimens are sectioned, documented, and labeled during sample preparation. The mounting procedures for the specimen are summarized. The article explains sample clamping, which involves not mounting the specimens using an adhesive or casting resin and corresponds to clamped samples used in automated polishing heads. It details that cavity molds involve mounting the composite specimens using a casting resin in a preset mold. The article also discusses the mounting of composite materials for hand polishing.

The analysis of composite materials using optical microscopy is a process that can be made easy and efficient with only a few contrast methods and preparation techniques. This article is intended to provide information that will help an investigator select the appropriate microscopy technique for the specific analysis objectives with a given composite material. The article opens with a discussion of macrophotography and microscope alignment, and then goes on to describe various illumination techniques that are useful for specific analysis requirements. These techniques include bright-field illumination, dark-field illumination, polarized-light microscopy, interference and contrast microscopy, and fluorescence microscopy. The article also provides a discussion of sample preparation materials such as dyes, etchants, and stains for the analysis of composite materials using optical microscopy.

Maintainability is a function of the durability, damage tolerance, and repairability of a structure. This article discusses the configurations of composite structures, such as sandwich, stiffened-skin, and monolithic structures, used in commercial aircraft composites. It describes the considerations for maintainability of the composite structures during the conceptual design phase. Sources of the defects and damage, such as manufacturing defects and in-service defects, are reviewed. The article describes the nondestructive inspection methods that are used in the repair of composite structures to locate damage, characterize the extent of damage, and ensure post-repair quality. It lists suggestions that can be used as design guidelines for adhesive bonding, general composite structure, sandwich structure, material selection, and lightning-strike protection. The article also provides the basic considerations for personnel, facilities, and equipment during maintenance.

This article presents a discussion on the U.S army's position on corrosion control for wheeled tactical vehicles. It addresses the army requirement for corrosion control. The U.S. Army Tank-automotive and Armaments Command (TACOM) defines the corrosion prevention and control requirements in the procurement document. The article summarizes requirements from a procurement document. As required by the procurement contract, corrosion-control technologies used in a vehicle system need to be evaluated to determine their benefit. The article provides information on testing systems, which help to meet the army's needs. It includes information on supplemental corrosion protection, which improves the corrosion resistance of a material.

This article describes the failure analysis procedures for composites and the techniques to be used in these analyses. These procedures include a review of the available in-service records, materials and processing methods, print requirements, and manufacturing records; visual analysis and nondestructive part evaluation; and verification of materials and processing methods. The article discusses the determination of fiber, matrix, and void volume fractions and verification of ply lay-up and orientation. A review of composites processing parameters; fractography and surface analysis; and mechanical testing and stress analysis is also presented.

Microscopy is a valuable tool in materials investigations related to problem solving, failure analysis, advanced materials development, and quality control. This article describes the sample preparation techniques of composite materials. These techniques include mounting, rough grinding, and polishing. The preparation techniques of ultrathin sections are also summarized. The article explains the illumination methods used by reflected light microscopy to view a specimen. These consist of epi-bright-field illumination, epi-dark-field illumination, epi-polarized light, and epi-fluorescence. The article also provides information on transmitted light microscopy.

This article presents a brief description of the fundamental characteristics of concrete and its constituents for understanding concrete fracture surfaces. It discusses the following two types of fractures: fractures induced in the laboratory and existing (service) fractures. The article provides a discussion on how existing crack surfaces differ from induced fractures: color, hardness, luster, depth of carbonation, deposits on crack surfaces, and propagation around or through aggregates.

Examination of a damaged component involves a chain of activities that, first and foremost, requires good observation and documentation. Following receipt and documentation, the features of damage can be recorded and their cause(s) investigated, as this article briefly describes, for typical types of damage experienced for metallic components. This article discusses the processes involved in visual or macroscopic examination of damaged material; the interpretation of fracture features, corrosion, and wear damage features; and the analysis of base material composition. It covers the processes involved in the selection of metallurgical samples, the preparation and examination of metallographic specimens in failure analysis, and the analysis and interpretation of microstructures. Examination and evaluation of polymers and ceramic materials in failure analysis are also briefly discussed.

This article reviews the mechanical behavior and fracture characteristics that discriminate structural polymers from metals, including plastic deformation. It provides overviews of crack propagation and fractography. The article presents the distinction between ductile and brittle fracture modes. Several case studies of field failure in various polymers are also presented to illustrate the applicability of available analytical tools in conjunction with an understanding of failure mechanisms.

This article begins with a discussion on the criteria for evaluating computer programs for composites structural analysis, including database capabilities, types of engineering calculations supported, interface and operating systems, and technical support. It describes the capabilities of programs, such as CompositePro, ESAComp, and V-Lab that provide a graphical interface, built-in databases, and integrated modules for the different types of analyses. The article reviews the modules of other programs used for composite analysis. The programs include ASCA, CADEC, CoDA, COMPASS, ESDU, LAP, PROMAL, and SACL. The article concludes with information on on-line programs and recourses.

This article focuses on the visual or macroscopic examination of damaged materials and interpretation of damage and fracture features. Analytical tools available for evaluations of corrosion and wear damage features include energy dispersive spectroscopy, electron probe microanalysis, Auger electron spectroscopy, secondary ion mass spectroscopy, and X-ray powder diffraction. The article discusses the analysis and interpretation of base material composition and microstructures. Preparation and examination of metallographic specimens in failure analysis are also discussed. The article concludes with a review of the evaluation of polymers and ceramic materials in failure analysis.

This article presents the concept of fracture mechanisms in general terms in order to impart a practical understanding as well as enable readers to develop the ability to identify the basic fracture mechanisms correctly based on microscope observations. The key microscopic features of fracture surfaces are described and illustrated for the important types of fracture mechanisms. It provides a detailed discussion on environmentally assisted crack initiation and growth.

In this article, a basic summary of fracture mechanisms in carbon and alloy steels is presented, along with numerous examples of these fractures. These examples include ductile fracture, brittle cleavage fracture, intergranular fracture, fatigue fracture, and environmentally assisted failure mechanisms.

High-temperature-resistant polymers are used in aerospace, electronic, and other applications that demand outstanding elevated-temperature physical and mechanical properties. This article discusses the general characteristics of condensation-type polyimides and polymerization of monomer reactants (PMR) polyimides. It provides information on the applications of PMR-15 with illustrations.

This article focuses on the various coatings used on Department of Defense (DoD) systems. These include electroplated coatings; conversion coatings; supplemental oils, waxes, and lubricants; organic paint coatings; and other finishes such as vacuum deposits, mechanical plating, thermal spray coatings, and hot-dip coatings. The article also lists the test requirements and time to failure of the coatings.