The potential for introducing defects during processing becomes greater as the relative density of pressed and sintered powder metallurgy (PM) parts increases and more multilevel parts with complex geometric shapes are produced. This article discusses the potential defects in pressed and sintered PM parts: density variations, compaction and ejection cracks, microlaminations, poor degree of sintering, and voids from prior lubricant agglomerates. It describes the various methods applicable to green compacts: direct-current resistivity testing, radiographic techniques, computed tomography, and gamma-ray density determination. The article also discusses the methods for automated nondestructive testing of pressed and sintered PM parts: acoustic methods-resonance testing, eddy current testing, magnetic bridge comparator testing, ultrasonic techniques, radiographic techniques, gamma-ray density determination, and visual inspection.

Ultrasonic inspection is a nondestructive technique that is useful in both quality control and research applications for flaw detection in fiber-reinforced composite materials. This article describes ultrasonic nondestructive analysis by outlining its three basic types of scans. It reviews the important quality control techniques used during the manufacture of composite components by analyzing tooling control, material control, pattern orientation control, and in-process control.

Adhesive-bonded joints are extensively used in aircraft components and assemblies where structural integrity is critical. This article addresses the problem of how to inspect bonded assemblies so that all discrepancies are identified. It describes several inspection techniques and presents drawbacks and limitations of these techniques. Generic flaw types and flaw-producing mechanisms are listed in a table. The article discusses metal-to-metal defects, adherend defects, honeycomb sandwich defects, repair defects, and in-service defects. It reviews the methods applicable to the inspection of bonded structures, including visual inspection, ultrasonic inspection, X-ray radiography, and neutron radiography. The evaluation and correlation of inspection results are also discussed. The article concludes with information on the effects of ultrasonic wave interference in the ultrasonic inspection of adhesive-bonded joints.

This article discusses the concepts of quality control (QC) and quality assurance (QA), and clarifies the differences and similarities in the roles and responsibilities of QC and QA personnel. It describes the inspection procedures used to verify proper surface preparation and installation of the protective coating/lining system. Prior to beginning surface-preparation operations, many specifications will require a presurface-preparation inspection to verify the correction of fabrication defects and removal of surface contamination such as grease, oil, cutting compounds, lubricants, and chemical contaminants. When inspecting concrete prior to coating installation, three areas of concern exist: surface roughness, moisture content in concrete, and acidity/alkalinity of the surface. The article provides information on the industry standards for assessing surface cleanliness. It details postcoating application quality requirements, including measuring of dry-film thickness, assessing intercoat cleanliness, verifying minimum and maximum recoat intervals, performing holiday/pinhole detection, conducting cure/hardness testing, and assessing adhesion of the applied coating system.

Failure analysis is a process of acquiring specified information regarding the appropriateness of the design of a part, the competence with which the various steps of its manufacture have been performed, any abuse suffered by it in packing and transportation, or the severity of service under which failure has occurred. Beginning with a discussion of the various stages of failure analysis of glass and ceramic materials, this article focuses on descriptive and quantitative fracture surface analysis techniques that are used in the examination of glass and surfaces created by fracture and the interpretation of the fracture markings seen on these surfaces. Details are provided for the procedures for locating fracture origins, determining direction of crack propagation, learning the sequence of crack propagation, deducing the stress state at the time of fracture, and observing interactions between crack fronts and inclusions, etc. A separate fractography terminology is provided in this article.

Probability of detection (POD) assesses the performance of a non-destructive evaluation (NDE)-based inspection, which is a method used to determine the capability of an inspection as a function of defect type and defect size. This article provides an overview of the concept of POD, why it is needed, the history behind the development of POD, how POD assessments are performed, and how modeling and simulation can be integrated into the execution of a POD assessment. It describes the methods by which POD is determined. This includes detail on the experimental process to acquire the needed data, the mathematical methods to obtain a POD curve, and techniques to assess uncertainty in the POD curve as it is obtained from a limited data set. The concept of model-assisted POD (MAPOD) is introduced, with additional details and representative examples of MAPOD.

This article presents information regarding the use of protective coatings in municipal potable water systems, including raw water collection and transmission, water treatment plants, and treated water distribution. It provides useful guidance for the selection and use of protective coatings in these municipal water systems. The most commonplace corrosion-damage mechanisms are highlighted. The article describes the most common materials of construction found in municipal water systems, namely, cast iron, ductile iron, carbon steel, precast concrete cylinder pipe and reinforced concrete pipe, prestressed concrete tanks, and stainless steel. It provides information on the most common generic coating systems used for new steel tanks and water storage tanks. It concludes with a discussion of quality watch-outs when selecting or using protective coatings in municipal water systems.

Optical testing of plastics includes characterization of materials and analysis of optical components. This article focuses on procedures for testing various characteristics of optical components, including transmission and haze, yellowness, refractive index, birefringence, as well as surface irregularity, contamination, gloss, and color. It provides a short note on ad hoc testing, which is beneficial for practical applications in which lenses, prisms, and light pipes are being used and tested, as other test instruments are often not available.

This article provides a discussion on general nondestructive evaluation (NDE) science and considerations for specific technique selection. It explains the basic concept of flaw detection and evaluation and probability of detection. The article provides an overview of NDE methods with their applications, limitations, and advantages. It includes details on NDE codes, calibration standards, inspection frequency, guidance on how to perform inspections, applicability, and mandatory and nonmandatory practice. The article also provides tips on where to focus inspections in order to align with the likely areas of damage or degradation and a number of other aspects of inspection.

This article presents examples of the visual fracture examination that illustrate the procedure as it applies to failure analysis and quality determination. It describes the techniques and procedures for the visual and light microscopic examination of fracture surfaces with illustrations. The article also describes microscopic and macroscopic features of the different fracture mechanisms with illustrations with emphasis on visual and light microscopy examination. The types of fractures considered include ductile fractures, tensile-test fractures, brittle fractures, fatigue fractures, and high-temperature fractures.

Surface coatings are essential in all facilities that process nuclear materials or use nuclear fission for power generation. This article describes the coatings used in two basic types of Generation 3 nuclear reactor designs in the United States and their containment size. These reactors are the boiling water reactor (BWR) and pressurized water reactor (PWR). The article provides information on the loss-of-coolant accident (LOCA) identified as the design basis accident (DBA), which can rapidly de-water the core of an operating nuclear reactor. To avoid LOCA, both the BWR and the PWR include emergency core cooling systems. The article describes a DBA test and other coating performance parameters necessary for safety-related coating systems. It provides a detailed account of the selection criteria of coating types in a nuclear plant. The article concludes by highlighting protective coating strategies in Generation 3 Plants.

Maintenance coating is an important part of any meaningful asset-preservation strategy in facilities producing pulp and paper and other chemicals. This article discusses maintenance coating for carbon steel structures and process equipment exposed to normal external pulp and paper mill atmospheric conditions. The important requirements and standards for surface preparation are emphasized and common issues encountered in maintenance coating projects are described.

The success of a reliable non-destructive evaluation (NDE) application depends greatly on the expertise and thoroughness of the NDE engineering that is performed. This article discusses the general considerations of NDE in terms of NDE response and NDE system management and schedule. It describes the NDE engineering and NDE process control, along with some case studies related to the applications of NDE. The article reviews various models for predicting NDE reliability, such as ultrasonic inspection model, eddy current inspection model, and radiographic inspection model. It concludes with an example that illustrates the integration of an ultrasonic reliability model with a CAD system.

Film radiography requires the development of the exposed film so that the latent image becomes visible for viewing. It describes the general characteristics of film, including speed, gradient, and graininess, and the factors affecting film selection and exposure time. The article discusses the three major inspection techniques for tubular sections, namely, the double-wall, double-image technique; the double-wall, single-image technique; and the single-wall, single-image technique. It illustrates the arrangements of penetrameters and identification markers for the radiography of plates, cylinders, and flanges. The article discusses various control methods, including the use of lead screens; protection against backscatter and scatter from external objects; and the use of masks, diaphragms, collimators, and filtration. The radiographic appearance of specific types of flaws is also discussed. The article concludes with a discussion on two methods of radiographic film processing: manual and automatic processing.

Aluminum casting alloys are the most versatile of all common foundry alloys and generally have the highest castability ratings. Aluminum alloy castings are routinely produced by pressure-die, permanent-mold, green and dry-sand, investment, and plaster casting. This article describes factors affecting the selection of casting process and the general designation system for aluminum alloys. It provides useful information on mechanical test methods, selection of proper test specimens for accurate test methods, characteristics of premium engineered castings, and advantages of hot isostatic pressing.

This article introduces the principal methodologies and some advanced technologies that are being applied for nondestructive evaluation (NDE) of fiber-reinforced polymer-matrix composites. These include acoustic emission, ultrasonic, eddy-current, computed tomography, electromagnetic acoustic transducer, radiography, thermography, and low-frequency vibration methods. The article also provides information on NDE methods commonly used for metal-matrix composites.

This article discusses the fundamentals and operating principles of the following acoustic microscopy methods: scanning laser acoustic microscopy, C-mode scanning acoustic microscopy, and scanning acoustic microscopy. It describes the applications of acoustic microscopy for detecting defects in metals, ceramics, glasses, polymers, and composites with examples.

This article provides information on the municipal wastewater system components such as piping, pump stations, headworks, clarifiers, aeration structures, digesters, biosolids dewatering equipment, and sludge stabilization. It explains the major corrosion damage mechanisms to which those component parts of the system are exposed. It presents useful guidelines for selecting and using protective coatings in municipal sewerage collection systems and water reclamation facilities in wastewater treatment plants. The article includes annotated flow diagrams of a wastewater collection system, wastewater treatment plants, and spreadsheets listing the most widely used generic coating systems by structure and substrate material. It concludes with a section on quality watchouts when selecting or using protective coatings in municipal wastewater systems.

The biocompatibility of a material relates to its immunological response, toxicity profile, and ability to integrate with surrounding tissue without undesirable local or systemic effects on a patient. This article underscores the transformation of the medical device design ecosystem engaged as an integral part of the device ecosystem. It discusses the various applications of biomaterials, including orthopedic, cardiovascular, ophthalmic, and dental applications. The article describes the four major categories of biomaterials, such as metals, polymers, glass and ceramics, and composites. A discussion on natural materials, nanomaterials, and stem cells is also provided. The article concludes with information on examples of biomaterials applications, including endovascular devices, knee implants, and neurostimulation.

This article provides an overview of the corrosion theory relating to refractories on the basis of acid/base reactions, thermodynamics, and kinetic considerations. The tests to evaluate refractory corrosive wear are reviewed. The article describes the specific refractories used in steel, glass, aluminum, and chemical-resistant applications. Specific material issues that should be considered or evaluated when choosing or using refractory materials are discussed.