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Published: 01 January 2000
Fig. 38 Viscosity ranges for different viscometers. Source: Ref 51
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Series: ASM Handbook
Volume: 8
Publisher: ASM International
Published: 01 January 2000
DOI: 10.31399/asm.hb.v08.a0003322
EISBN: 978-1-62708-176-4
... on the measurement of viscosity of semisolid alloy materials by using three types of viscometers: the coaxial cylinder viscometer, the cone-and-plate viscometer, and the capillary viscometer. forming bulk forming sheet-metal forming semisolid forming polymer extrusion process modeling compression test...
Abstract
Forming processes can be divided into three major categories: bulk forming, sheet-metal forming, and semisolid forming and polymer extrusion. This article introduces each process category with a description of the constitutive models. It outlines the required properties for process modeling and describes the test methods for determining these properties. The article discusses several compression tests used to determine stress-strain curves for bulk forming and tensile tests used to obtain stress-strain curves for sheet-metal forming. The article concludes with information on the measurement of viscosity of semisolid alloy materials by using three types of viscometers: the coaxial cylinder viscometer, the cone-and-plate viscometer, and the capillary viscometer.
Series: ASM Handbook
Volume: 22B
Publisher: ASM International
Published: 01 November 2010
DOI: 10.31399/asm.hb.v22b.a0005514
EISBN: 978-1-62708-197-9
... transition temperatures. The article schematically illustrates the laser flash apparatus for measuring the thermal diffusivity of solids and oscillation viscometer for measurements of the viscosity of metals. A summary of the measurement methods is presented in tables. adiabatic calorimetry calvet...
Abstract
The measurement of thermophysical properties of metal alloys, especially at high temperatures, is difficult because of the reactivity of some alloys. This article reviews the methods available for measurement of thermal and other physical properties for liquid, semi-solid, and solid commercial alloys, including adiabatic calorimetry, modulated calorimetry, Calvet calorimetry, single-pan calorimetry, and drop calorimetry. It describes differential scanning calorimetry and differential temperature analysis for measuring transition temperatures such as phase transformation or glass transition temperatures. The article schematically illustrates the laser flash apparatus for measuring the thermal diffusivity of solids and oscillation viscometer for measurements of the viscosity of metals. A summary of the measurement methods is presented in tables.
Image
Published: 31 December 2017
Fig. 3 Ostwald viscometer used to measure viscosity of Newtonian fluid. A given amount of fluid flows out of a container via a narrow capillary tube, and flow time is multiplied by a calibration factor to determine viscosity.
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Image
in Measurement of Thermophysical Properties at High Temperatures for Liquid, Semisolid, and Solid Commercial Alloys
> Metals Process Simulation
Published: 01 November 2010
Fig. 8 Design of oscillation viscometer for metals
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in Measurement of Thermophysical Properties at High Temperatures for Liquid, Semisolid, and Solid Commercial Alloys
> Metals Process Simulation
Published: 01 November 2010
Fig. 9 Schematic of rotating bob viscometer for measuring viscosity of liquid metals
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Image
Published: 01 January 2000
Fig. 35 A schematic of the coaxial cylinder viscometer. Source: Ref 51
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Image
Published: 01 February 2024
Fig. 125 Illustration of a glass Cannon-Fenske viscometer tube. When obtaining a viscosity measurement, the tube is typically filled as shown, equilibrated in a constant-temperature bath, and the time for the fluid to flow between the two marks on the tube is measured. The kinematic viscosity
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Image
Published: 01 February 2024
Fig. 18 Polyvinyl pyrrolidone K30 polymer concentration control using an Ubbelohde-type capillary viscometer and Abbe-type refractometer at 30 °C (85 °F) solution
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Book: Composites
Series: ASM Handbook
Volume: 21
Publisher: ASM International
Published: 01 January 2001
DOI: 10.31399/asm.hb.v21.a0003432
EISBN: 978-1-62708-195-5
... processibility and can be a measure of average molecular weight, the point at which the resin softens should be measured using a technique such as a cone and plate viscometer, a Brookfield viscometer, or a dilatometer. Infrared (IR) Spectroscopy This test is a rapid method for identifying chemical...
Abstract
This article focuses on epoxy because this resin category has widespread use and because it is tested using quality control measures typical of most resin systems. It explains that a typical resin system will consist of one or more epoxy resins, a curing agent, and a catalyst to control the rate of reaction. The article describes the component material tests, mixed resin system tests, and prepreg tests for the resin system. These tests include high-performance liquid chromatography, infrared spectroscopy, and gel permeation chromatography. The article contains a table that lists typical resin and prepreg property tests.
Series: ASM Handbook
Volume: 11B
Publisher: ASM International
Published: 15 May 2022
DOI: 10.31399/asm.hb.v11B.a0006849
EISBN: 978-1-62708-395-9
... ) is recommended for determining the logarithmic viscosity of a PVC compound and for assessing the consequences of processing using the base resin’s MW. Fig. 1 ASTM solution viscosity relationships Brookfield Viscosity Several ASTM documents are based on the inexpensive Brookfield viscometer...
Abstract
This article addresses some established protocols for characterizing thermoplastics and whether they are homogeneous resins, alloyed, or blended compositions or highly modified thermoplastic composites. It begins with a discussion on characterizing mechanical, rheological, and thermal properties of polymer. This is followed by a section describing molecular weight determination using viscosity measurements. Next, the article discusses the use of cone and plate and parallel plate geometries in melt rheology. It then reviews the processes involved in the analysis of thermoplastic resins by chromatography. Finally, the article covers three operations of thermoanalysis, namely differential scanning calorimetry, thermogravimetric analysis, and thermomechanical testing.
Book: Casting
Series: ASM Handbook
Volume: 15
Publisher: ASM International
Published: 01 December 2008
DOI: 10.31399/asm.hb.v15.a0005272
EISBN: 978-1-62708-187-0
... under the supervision of Professor Merton Flemings ( Ref 1 , 2 ). Spencer discovered that when the dendritic structure of a partially solidified Sn-15wt%Pb alloy was fragmented by shear in a Couette viscometer, a globular structure resulted. The apparent viscosity of the globular structure...
Abstract
Semisolid metal (SSM) processing, also known as semisolid metal casting, semisolid forming, or semisolid metal forging, is a special die casting process. This article discusses the origin and advantages of the SSM processing. It describes three major semisolid processing routes: thixocasting, rheocasting, and thixomolding.
Series: ASM Handbook
Volume: 18
Publisher: ASM International
Published: 31 December 2017
DOI: 10.31399/asm.hb.v18.a0006401
EISBN: 978-1-62708-192-4
Abstract
This article provides a brief introduction to lubrication as a method to reduce friction between two surfaces. It discusses the surface characteristics of parts and explores how lubrication helps separate two contacting surfaces and thereby decreases the coefficient of friction. The article details the classifications of lubrication regimes, namely, boundary, mixed, hydrodynamic, and elastohydrodynamic lubrications. It discusses the various types of lubricant materials and additives, including liquid lubricants, solid lubricants, gaseous lubricants, greases, green lubricants, and nanomaterials. The article also reviews the properties of lubricants. It describes the tribological evaluation of lubricants, including stribeck test, four-ball test, block-on-ring test, pin-in-vee test, and reciprocating motion test.
Series: ASM Handbook
Volume: 18
Publisher: ASM International
Published: 31 December 2017
DOI: 10.31399/asm.hb.v18.a0006411
EISBN: 978-1-62708-192-4
... of lubricants are the Ostwald viscometer and the rheometer. The Ostwald viscometer ( Fig. 3 ) measures the viscosity of Newtonian fluid. A given amount of fluid flows out of a container via a narrow capillary tube, and flow time is multiplied by a calibration factor to determine its viscosity. The rheometer...
Abstract
The function of lubricants is to control friction and wear in a lubricating system containing machine elements such as gears and bearings. This article discusses the basic properties of lubricants to help scientists and engineers understand the principles behind lubricant selection. It reviews the functions of additives, such as friction modifiers, antiwear additives, viscosity modifiers, corrosion inhibitors, oxidation inhibitors, dispersants, and detergents. The article discusses the physical properties of liquid lubricants and the performance characteristics of lubricants. It describes the most common lubricant categories and provides information on the health and safety aspects of using liquid lubricants. The article concludes with a discussion on the lubricant-application method that plays a vital role in how the lubricant functions.
Series: ASM Handbook
Volume: 23A
Publisher: ASM International
Published: 12 September 2022
DOI: 10.31399/asm.hb.v23A.a0006887
EISBN: 978-1-62708-392-8
... by centripetal stirring and centrifugal separation. The kinematic viscosities of the pastes that are created are continuously measured using a digital viscometer. The hysteresis profiles of the shearing speeds and stresses become saturated with the paste mixing time. The paste materials are injected from...
Abstract
Stereolithographic (STL) additive manufacturing (AM) can be used to fabricate practical components. This article discusses the processes involved in STL-AM of biological scaffolds, providing information on bioscaffold processing, cavity arrangements, and microlattice distributions. Within the last topic, the sub-topic of scaffold modulation is discussed.
Series: ASM Handbook
Volume: 11B
Publisher: ASM International
Published: 15 May 2022
DOI: 10.31399/asm.hb.v11B.a0006916
EISBN: 978-1-62708-395-9
... due to material degradation from the failure to remove moisture before molding. The short-chain molecules will have lower viscosity, indicating material degradation. Simple tests include the dilute solution viscosity (DSV) test (ASTM D2857) for various plastics or the rotational viscometer...
Abstract
This article focuses on manufacturing-related failures of injection-molded plastic parts, although the concepts apply to all plastic manufacturing processes It provides detailed examples of failures due to improper material handling, drying, mixing of additives, and molecular packing and orientation. It also presents examples of failures stemming from material degradation improper use of metal inserts, weak weld lines, insufficient curing of thermosets, and inadequate mixing and impregnation in the case of thermoset composites.
Series: ASM Handbook
Volume: 18
Publisher: ASM International
Published: 31 December 2017
DOI: 10.31399/asm.hb.v18.a0006366
EISBN: 978-1-62708-192-4
..., thicker lubricating film has better performance in protecting the contact from wear. Rotational viscometers are the most frequently used apparatus for viscosity measurement. One main drawback of rotational viscometers is that they are only applicable under atmospheric pressure. To evaluate the viscosity...
Abstract
This article introduces the structure, tribological properties, advantages, and applications of ionic liquids (ILs) as lubricating media. It discusses the mechanisms of IL lubrication for different contacts. The advances in studies focusing on tribological properties of a wide range of ILs are reviewed. The article concludes with the challenges that limit the applications of ILs in tribology engineering.
Book: Machining
Series: ASM Handbook
Volume: 16
Publisher: ASM International
Published: 01 January 1989
DOI: 10.31399/asm.hb.v16.a0002128
EISBN: 978-1-62708-188-7
...). Specification ASTM D 445-446 describes the instrumentation and technique for measuring kinematic viscosity. Viscometers of various designs permit flow under controlled conditions, and this flow is translated into viscosity at a specified temperature. Specification ASTM D 88 describes a method that uses...
Abstract
This article discusses the functions and chemistry of metal cutting or grinding fluids. It reviews the choice of cutting or grinding fluids that is influenced by the workpiece material, fluid characteristics, and machining operation. The article describes two application methods of cutting or grinding fluids: flooding and misting. It discusses and lists the American Society for Testing and Materials standard test procedures used in establishing control of cutting and grinding fluids. The article provides information on the storage, distribution, cleaning, and disposal of cutting and grinding fluids. It concludes with information on the health implications and biology of cutting fluids.
Series: ASM Handbook
Volume: 2A
Publisher: ASM International
Published: 30 November 2018
DOI: 10.31399/asm.hb.v02a.a0006498
EISBN: 978-1-62708-207-5
...) Fully liquid History of Semisolid Processing The concept of semisolid casting arose from pioneering work performed by Flemings and co-workers at MIT in the early 1970s. Spencer, a graduate student, was using a Couette viscometer to study the hot tearing of a Sn-15%Pb alloy and observed...
Abstract
Semisolid casting is a near-net shape manufacturing process capable of producing thick- and thin-walled complex-shaped components having excellent mechanical and functional performance. This article begins with a discussion on the history of semisolid processing and the advantages claimed for semisolid casting. It describes the four notable processes used to produce semisolid castings: thixocasting, rheocasting, thixomolding, and wrought processes. Most commercial aluminum semisolid casters use either thixocasting or rheocasting. The article discusses the die design, process conditions, and simulation for semisolid casting. It concludes with a review of several components produced by each of the various semisolid casting processes.
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