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Published: 01 June 2016
Fig. 8 Alpha case after vacuum heat treatment of uncoated Ti-6Al-4V. Vacuum heat treated at 700 °C (1300 °F) for 30 min at 10 −4 torr. Alpha-case depth: 10 μm (0.0004 in.). The α-case depth is clearly defined by the solid white band on the surface. Preparation: Kroll’s reagent and 2% ammonium
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Published: 09 June 2014
Fig. 49 Surface heat treatment conditions showing (a) vacuum carburizing and (b) contour refining condition. Source: Ref 48
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Series: ASM Handbook
Volume: 24
Publisher: ASM International
Published: 15 June 2020
DOI: 10.31399/asm.hb.v24.a0006561
EISBN: 978-1-62708-290-7
... Abstract This article focuses on various vacuum heat treating processes for additively manufactured parts, namely annealing and stress relieving, solid-solution annealing, and solution treating and aging. It addresses several practical concerns involved in using vacuum heat treatment, including...
Abstract
This article focuses on various vacuum heat treating processes for additively manufactured parts, namely annealing and stress relieving, solid-solution annealing, and solution treating and aging. It addresses several practical concerns involved in using vacuum heat treatment, including temperature measurement, unvented cavities, loose powder, and direct contact of metals in the high-temperature vacuum. The article provides a short discussion on sintering and evaporation of metals in vacuum furnaces.
Image
Published: 01 December 2008
Fig. 30 Treatment cycle of a 75 Mg (80 ton) vacuum arc degassing-heated melt. 1, tapping; 2, additions of C + Al + 0.5% CaO; 3, temperature check; 4, sampling and temperature check; 5, addition of 1.5% alloys + 0.5% CaO; 6, temperature check; 7, additions + 0.5% CaO; 8, degassing; 9, venting
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Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006128
EISBN: 978-1-62708-175-7
..., austenitizing, and vacuum heat treatment. It explains the result of these tempering processes with HSS M2 grade of HATS. austenitizing heat treatment high-potential high-alloy tool steels martensitic microstructure salt bath heat treatment secondary-hardening high-alloy tool steel tempering vacuum...
Abstract
High-potential high-alloy tool steels (HATS) containing martensitic microstructure with undissolved hard phases are achieved by a number of complex heat treating cycles, predominantly tempering. This article focuses on three tempering treatments, namely, salt bath heat treatment, austenitizing, and vacuum heat treatment. It explains the result of these tempering processes with HSS M2 grade of HATS.
Series: ASM Handbook
Volume: 4A
Publisher: ASM International
Published: 01 August 2013
DOI: 10.31399/asm.hb.v04a.a0005813
EISBN: 978-1-62708-165-8
... of a steel grade with excellent hardenability. A detailed introduction into the technology of vacuum heat treatment including LPC is given in Ref 1 . Physical Principles When acetylene comes in contact with the surface of the steel at temperatures above 870 °C (1600 °F), it dissociates thermally...
Abstract
Low-pressure carburizing (LPC) is one of the most popular case-hardening processes and is applied to increase the fatigue limit of dynamically loaded components. It takes place in a pressure range between 5 and 15 mbar (4 and 11 torr) and at temperature range between 870 and 1050 deg C. The LPC process runs in two different types of equipment: single-chamber furnaces and treatment chambers. This article reviews the use of simulation software for prediction of carbon profiles and typical quality control procedures. It describes the physical principles and typical applications of LPC.
Series: ASM Handbook
Volume: 4E
Publisher: ASM International
Published: 01 June 2016
DOI: 10.31399/asm.hb.v04e.a0006283
EISBN: 978-1-62708-169-6
... Abstract This article provides a detailed discussion on heat treatment of titanium alloys such as alpha alloys, alpha-beta alloys, and beta and near-beta alloys. Common processes include stress-relief, annealing, solution treating, aging, quenching, and age hardening. It provides information...
Abstract
This article provides a detailed discussion on heat treatment of titanium alloys such as alpha alloys, alpha-beta alloys, and beta and near-beta alloys. Common processes include stress-relief, annealing, solution treating, aging, quenching, and age hardening. It provides information on the effects of alloying elements on alpha/beta transformation. The article also discusses the heat treating procedures, and the furnaces used for heat treating titanium and titanium alloys.
Series: ASM Handbook
Volume: 2
Publisher: ASM International
Published: 01 January 1990
DOI: 10.31399/asm.hb.v02.a0001085
EISBN: 978-1-62708-162-7
...) and exhibits very large grains, has low room-temperature ductility (∼6% elongation). Ductility can be substantially improved by lowering hydrogen content via vacuum heat treatment (∼1 Pa, or 10 −2 torr) in the high α region (550 to 640 °C, or 1020 to 1180 °F). The time required for hydrogen outgassing depends...
Abstract
Uranium is a moderately strong and ductile metal that can be cast, formed, and welded by a variety of standard methods. This article presents an overview of the processing and properties of uranium and uranium alloys with a brief overview of the principal hazards and precautions associated with processing depleted uranium and methods to control mild radioactivity, chemical toxicity, and pyrophoricity. It also describes the classification and heat treatment of uranium and uranium alloys. Furthermore, the article provides graphical representation of the effect of alloy composition, cooling rate, and aging temperature on microstructure, crystal structure, and mechanical properties of uranium and uranium alloys.
Series: ASM Handbook
Volume: 4B
Publisher: ASM International
Published: 30 September 2014
DOI: 10.31399/asm.hb.v04b.a0005955
EISBN: 978-1-62708-166-5
... alloys. atmosphere furnaces heating elements pumps quenching stainless steel titanium alloys tool steel vacuum carburizing vacuum furnaces vacuum heat treatment vacuum nitriding VACUUM ATMOSPHERES have become the first choice of many heat treaters as a result of the advent of space...
Abstract
Vacuum heat treating consists of thermally treating metals and alloys in cylindrical steel chambers that have been pumped down to less than normal atmospheric pressure. This article provides a detailed account of the operations and designs of vacuum furnaces, discussing their pressure levels, resistance heating elements, quenching systems, work load support, pumping systems, and temperature control systems. It describes the classification of instruments used for measuring and recording pressure inside a vacuum processing chamber. Common devices include hydrostatic measuring devices and devices for measuring thermal and electrical conductivity. The article also describes the applications of the vacuum heat treating process, namely, vacuum nitriding and vacuum carburizing. Finally, it reviews the heat treating process of tool steels, stainless steels, Inconel 718, and titanium and its alloys.
Book Chapter
Book: Casting
Series: ASM Handbook
Volume: 15
Publisher: ASM International
Published: 01 December 2008
DOI: 10.31399/asm.hb.v15.a0005199
EISBN: 978-1-62708-187-0
... treatment and their relative capabilities. These methods can be categorized under four major groups ( Fig. 12 ): stirring, injection, vacuum, and heating processes ( Ref 18 ). Fig. 12 Processes for secondary steelmaking. Stirring process: (a) bottom injection and (b) lance injection. Injection...
Abstract
This article discusses the most common methods of melting steels, namely, electric arc and induction melting. It describes the classification of refractories by an index of the “basicity” of the slag formed on the steel surface. The article provides a discussion on the converter metallurgy, which includes melt refinement in argon oxygen decarburization (AOD) vessels and vacuum oxygen decarburization (VODC) in a converter vessel. It also discusses ladle metallurgy, which includes vacuum induction degassing, vacuum oxygen decarburization, and vacuum ladle degassing.
Series: ASM Handbook
Volume: 4B
Publisher: ASM International
Published: 30 September 2014
DOI: 10.31399/asm.hb.v04b.a0005931
EISBN: 978-1-62708-166-5
... of this article is on atmosphere furnaces, with some coverage on controls for vacuum furnaces. More information on vacuum furnace controls is in the article, “Vacuum Heat Treatment and Equipment,” in this Volume. Mechanical Motion Components Heat treating operations require the reliable monitoring...
Abstract
Heat treating furnaces require different control systems and integration for achieving optimum technical results and enabling safe operation. This article focuses on atmosphere furnaces, with some coverage on controls for vacuum furnaces. Heat treating operations require reliable monitoring and control of motion and position of various mechanical components with the help of mechanical limit switches, proximity sensors, and distance- and position-measuring devices. Using inputs from both flow meters and sensors, such as thermocouples and oxygen sensors, flow measurement control systems must be able to adjust the flow of gases for process optimization. The operator interface of a furnace-control system displays critical information such as the furnace temperature, atmosphere status, alarms, electronic chart recorders, recipe, and maintenance. A supervisory control and data-acquisition (SCADA) system is used to monitor, collect, and store data from multiple pieces of equipment.
Series: ASM Handbook
Volume: 4D
Publisher: ASM International
Published: 01 October 2014
DOI: 10.31399/asm.hb.v04d.a0005980
EISBN: 978-1-62708-168-9
...-bath heat treatment results in higher distortion than various vacuum heat treatments with high-pressure gas quenching, but the results indicate that there is also a significant scatter for gas quenching depending on the detailed quenching conditions. Experiments with similar sized plates, including...
Abstract
Distortion, encompassing all irreversible dimensional changes, is of two main types: size distortion and shape distortion. This article provides an overview of the nature and causes of distortion and discusses the process and material aspects of distortion specific to steels and tool steels. It also discusses the prediction of distortion and residual stresses by heat treatment simulation for optimizing production processes. The advantages and limitations of heat treatment simulation are also described.
Series: ASM Handbook
Volume: 4E
Publisher: ASM International
Published: 01 June 2016
DOI: 10.31399/asm.hb.v04e.a0006256
EISBN: 978-1-62708-169-6
... designs used for heating or heat treating of unalloyed uranium: molten salt baths, inert-atmosphere furnaces, and vacuum furnaces. Finally, it presents procedures that are examples of heat treatment used to meet certain specifications of ultimate tensile strength, yield strength, and elongation...
Abstract
Heat treatment of depleted uranium (DU) alloys with 4.0 wt% or more molybdenum or equivalent is similar to that of dilute alloys. This article discusses the metallurgical characteristics and processing considerations of DU and its alloys, and describes the control of grain size and orientation using beta treatment. It lists the typical mechanical properties of DU as functions of the amount of cold work and hardness data of uranium rod, and describes the annealing of cold-worked DU. The article also describes the heat treatment of dilute alloys of DU, focusing on the three basic furnace designs used for heating or heat treating of unalloyed uranium: molten salt baths, inert-atmosphere furnaces, and vacuum furnaces. Finally, it presents procedures that are examples of heat treatment used to meet certain specifications of ultimate tensile strength, yield strength, and elongation.
Series: ASM Handbook
Volume: 4B
Publisher: ASM International
Published: 30 September 2014
DOI: 10.31399/asm.hb.v04b.a0005957
EISBN: 978-1-62708-166-5
..., shaker hearth furnace, tip-up furnace, vacuum furnace, walking beam furnace Solution heat treatment Aerodynamic heat treating furnace, bell furnace, box furnace, elevator hearth furnace, pit furnace, pusher furnace, roller hearth furnace, vacuum furnace Stress relieving Aerodynamic heat treating...
Abstract
Furnaces are one of the most versatile types of industrial appliances that span many different areas of use. This article discusses the classification of various furnaces used in heat treating based on the mode of operation (batch-type furnaces and continuous-type furnaces), application, heating method, mode of heat transfer, type of materials handling system, and mode of waste heat recovery (recuperation and regeneration). It provides information on uniform temperature distribution, the general requirements and selection criteria for insulation materials, as well as the basic safety requirements of these furnaces.
Series: ASM Handbook
Volume: 4D
Publisher: ASM International
Published: 01 October 2014
DOI: 10.31399/asm.hb.v04d.a0005958
EISBN: 978-1-62708-168-9
.... atmosphere furnaces austenitizing fluidized-bed furnaces gas nitriding heat treatment plasma nitriding quenching salt bath furnaces salt bath nitrocarburizing tempering tool steel vacuum furnaces THE HEAT TREATMENT of tool steels covers an extremely wide variety of different requirements...
Abstract
This article provides a detailed discussion on the heating equipment used for austenitizing, quenching, and tempering tool steels. These include salt bath furnaces, controlled atmosphere furnaces, fluidized-bed furnaces, and vacuum furnaces. The article discusses the types of nitriding and nitrocarburizing processes and the equipment required for heat treating tool steels to improve hardness, wear resistance, and thermal fatigue. The various nitriding and nitrocarburizing processes covered are salt bath nitrocarburizing, gas nitriding and nitrocarburizing, and plasma nitriding and nitrocarburizing.
Series: ASM Handbook
Volume: 4A
Publisher: ASM International
Published: 01 August 2013
DOI: 10.31399/asm.hb.v04a.a0005822
EISBN: 978-1-62708-165-8
... solution treatment and prior to aging. Shrink Fits Cooling the inner member of a complex part to below ambient temperature can be a useful way of providing an interference fit. Care must be taken, however, to avoid the brittle cracking that may develop when the inner member is made of heat treated...
Abstract
Cold treating of steel can be used to enhance the transformation of austenite to martensite and improve the stress relief of castings and machined parts. Cryogenic treatment of steel is a distinct process that uses extreme cold to modify the performance of materials. This article explains the practices employed and equipment used in the cold treatment of steel. It also presents the results of using cryogenic treatment to enhance steel properties.
Series: ASM Handbook
Volume: 4D
Publisher: ASM International
Published: 01 October 2014
DOI: 10.31399/asm.hb.v04d.a0005973
EISBN: 978-1-62708-168-9
... heat treatment vanadium Introduction ALL COLD-WORK TOOL STEELS described in this chapter are medium- to high-alloy grades that show good hardenability. Hardening of these grades is nowadays usually performed in vacuum furnaces with high pressure gas quenching, but some grades of lower...
Abstract
This article focuses on various heat-treating practices, namely, normalizing, annealing, stress relieving, preheating, austenitizing, quenching, tempering, and nitriding for cold-work tool steels. The cold-work tool steels include medium-alloy air-hardening tool steels, high-carbon high-chromium tool steels, and high-vanadium-powder metallurgy tool steels. The article also describes the properties, types, nominal compositions and designations of these cold-work tool steels.
Book Chapter
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 December 1998
DOI: 10.31399/asm.hb.mhde2.a0003198
EISBN: 978-1-62708-199-3
... enclosures that are evacuated to partial pressures compatible with the particular metals and processes. Vacuum is substituted for the more commonly used protective gas atmospheres during either part or all of the heat treatment. Furnace equipment used in vacuum heat treating differs widely in size, shape...
Abstract
Batch furnaces and continuous furnaces are commonly used in heat treating. This article provides a detailed account of various heat treating equipment and its furnace types, including salt bath equipment (externally heated, immersed-electrode and submerged-electrode furnaces), and fluidized-bed equipment (external-resistance-heated fluidized beds). It describes various auxiliary equipment used in cold-wall furnaces, namely, heating elements and pumping systems. Five types of heat-resistant alloys are used for furnace parts, trays, and fixtures: Fe-Cr alloys, Fe-Cr-Ni alloys, Fe-Ni-Cr alloys, nickel-base alloys and cobalt-base alloys. The article lists the recommended applications for alloys for parts and fixtures for various types of heat treating furnaces.
Book Chapter
Book: Casting
Series: ASM Handbook
Volume: 15
Publisher: ASM International
Published: 01 December 2008
DOI: 10.31399/asm.hb.v15.a0005348
EISBN: 978-1-62708-187-0
... than or equal to PTS para-toluosulfonic acid V-D vacuum degassing PUCB phenolic urethane cold box VID vacuum induction degassing maximum deviation PUN phenolic urethane no-bake VIDP vacuum induction degassing and pouring minus; negative ion charge PWHT postweld heat treatment VIM vacuum induction...
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 December 1998
DOI: 10.31399/asm.hb.mhde2.a0003173
EISBN: 978-1-62708-199-3
... are needed, a second desulfurization treatment can be carried out. Steel heats may also be degassed using inert gas and vacuum. The melt is placed in the vacuum degassing vessel and the pressure above the melt is reduced, allowing hydrogen and nitrogen to be removed from the bath. To reach maximum...
Abstract
The melting process often includes refining and treating the metal. The choice of which type of melting to use depends on a number of factors: type of alloy being melted, the local cost of electric power, and local environmental regulations. This article discusses the principles, furnace types, charging practices of metal melting methods, namely induction melting, cupola melting, arc melting, crucible melting, reaction melting, and vacuum melting, and the refractories and charging practice of reverberatory furnaces. Molten metal treatment of steels and aluminum also is discussed in the article.
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