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Leander F. Pease, III, Douglas L. Pease
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Image
Unsintered iron powder. Surface of part, which had been contacted by the up...
Available to Purchase
in Metallography and Microstructures of Powder Metallurgy Alloys
> Metallography and Microstructures
Published: 01 December 2004
Fig. 21 Unsintered iron powder. Surface of part, which had been contacted by the upper punch at 275 MPa (20 tsi). Arrow shows the particle boundaries that will disappear during proper sintering. SEM. 750×
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Fracture surface of a heat treated P/M steel where the fracture occurred in...
Available to Purchase
in Metallography and Microstructures of Powder Metallurgy Alloys
> Metallography and Microstructures
Published: 01 December 2004
Fig. 28 Fracture surface of a heat treated P/M steel where the fracture occurred in the unsintered state. Top arrow shows the compacted surface. Right arrow points to rounded particle surfaces with no indication of ductile cups and cones that would be typical of a fracture in the sintered
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in Metallography and Microstructures of Powder Metallurgy Alloys
> Metallography and Microstructures
Published: 01 December 2004
Fig. 29 Same material as Fig. 28 but a fracture surface deliberately created in the sintered and heat treated state. Arrow points to sharp asperities where the particles were torn away from the adjacent material on the opposite fracture surface. Such asperities are not created when a P/M
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Book Chapter
Compressibility and Compactibility of Metal Powders
Available to PurchaseBook: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006032
EISBN: 978-1-62708-175-7
... green strength hardness lubrication metal powders particle shape particle size Rattler test transverse bend test COMPRESSIBILITY AND COMPACTIBILITY are terms that define the ability to form “green” (unsintered) compact from the die pressing of powders. In general terms, compressibility...
Abstract
This article describes several factors, which help in determining the compressibility of metal powders: particle shape, density, composition, hardness, particle size, lubrication, and compacting. It discusses the uses of annealing metal powders and describes compressibility testing of the powders. The article details green strength and its mechanism and the variables affecting the strength. It also discusses two test methods for determining the green strength: the Rattler test and the transverse bend test.
Book: Machining
Series: ASM Handbook
Volume: 16
Publisher: ASM International
Published: 01 January 1989
DOI: 10.31399/asm.hb.v16.a0002126
EISBN: 978-1-62708-188-7
... shaped into a green (unsintered) body, which is then sintered to achieve the necessary densification. In hot pressing, the shaping is performed during sintering. Hot Pressing Hot pressing involves heating the powder in a die, along with the simultaneous application of a high uniaxial pressure...
Abstract
Ceramics are materials with the potential for a wide range of high-speed finishing operations and for high removal rate machining of difficult-to-machine materials. This article describes the production process, composition, properties, and applications of ceramic tool materials. It presents a comprehensive discussion on the properties and composition of alumina-base tool materials, including alumina and titanium carbide, alumina-zirconia, and silicon carbide whisker reinforced alumina, and silicon nitride base tool materials.
Book Chapter
Metallography and Microstructures of Powder Metallurgy Alloys
Available to PurchaseSeries: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0003789
EISBN: 978-1-62708-177-1
..., meant to preserve pore structures and keep them open for analysis. The article compares and contrasts the microstructures of nearly 50 powder metal alloys, using them to illustrate the effect of consolidation and compaction methods as well as particle size, composition, and shape. It discusses imaging...
Abstract
This article provides information on the microstructure of powder metal alloys and the special handling requirements of porous materials. It covers selection, sectioning, mounting, grinding, and polishing, and describes procedures, such as washing, liquid removal, and impregnation, meant to preserve pore structures and keep them open for analysis. The article compares and contrasts the microstructures of nearly 50 powder metal alloys, using them to illustrate the effect of consolidation and compaction methods as well as particle size, composition, and shape. It discusses imaging equipment and techniques and provides data on etchants and etching procedures.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006074
EISBN: 978-1-62708-175-7
... Molded parts are designated as being in the “green” or unsintered state following common terminology used for die-compacted metal powder parts. The usual next step is sintering to increase density to a maximum value close to theoretical or to a designed lower value for intentionally porous structures...
Abstract
This article describes the unique aspects of cold isostatic pressing (CIP) in comparison with die compaction, for powder metallurgy parts. It details the components of CIP equipment, including pressure vessels, pressure generators, and tooling material. The article reviews the part shapes and their influence in determining tap density of the filled mold. It provides a discussion on process parameters, such as dwell time, depressurization rate, evaluation of green strength and density, and thermal processing, and illustrates a process flowchart for the production of CIP parts.
Book: Machining
Series: ASM Handbook
Volume: 16
Publisher: ASM International
Published: 01 January 1989
DOI: 10.31399/asm.hb.v16.a0002193
EISBN: 978-1-62708-188-7
... and cutting tool parameters as well as some P/M material and production process parameters. These parameters discussed include the particle size, part geometry, porosity, compaction and sintering methods. In addition, the article presents guidelines for the various machining processes, namely, turning...
Abstract
Powder metallurgy is a near-net shape process capable of producing complex parts with little or no need for secondary operations such as machining, joining, or assembly. However, the inability to produce certain geometrical figures such as transverse holes, undercuts, and threads frequently necessitates some machining, particularly drilling. This article provides a discussion on the measures that can optimize the machining of P/M materials. It reviews the factors influencing machinability of P/M components, including workpiece and tool material properties, cutting conditions, machine and cutting tool parameters as well as some P/M material and production process parameters. These parameters discussed include the particle size, part geometry, porosity, compaction and sintering methods. In addition, the article presents guidelines for the various machining processes, namely, turning and boring, milling, drilling, grinding, reaming, burnishing, tapping, and honing and lapping.
Book Chapter
Environmental Impact, Health, and Safety for Additive Manufacturing
Available to PurchaseSeries: ASM Handbook
Volume: 24A
Publisher: ASM International
Published: 30 June 2023
DOI: 10.31399/asm.hb.v24A.a0006960
EISBN: 978-1-62708-439-0
... by the process often result in some level of vapor emissions (metal fumes, volatile organic compounds, and ultrafine particles for polymers) that also must be captioned and controlled. Finally, a number of secondary elements that may be altered or contaminated must be controlled, cleaned, and/or disposed...
Abstract
This article provides an overview of the concepts of environmental, health, and safety (EH&S) risk incidents, then discusses these concepts relative to additive manufacturing (AM): the multiple intrants, process parameters, and equipment, as well as the resulting products and wastes. The article discusses additive manufacturing hazards, which are broken down into material hazards, equipment/process hazards, and facility hazards. The environmental impact of AM and the development of EH&S standards for AM also are covered in the article.
Book Chapter
Powder-Bed Fusion of Polymers
Available to PurchaseSeries: ASM Handbook
Volume: 23A
Publisher: ASM International
Published: 12 September 2022
DOI: 10.31399/asm.hb.v23A.a0006883
EISBN: 978-1-62708-392-8
... of polymers; TPBF, thermal powder-bed fusion Polymers are by far the most common materials for 3D printing technology, with diverse applications. High utilization rate, wide materials range, and easy manufacturing process are the common advantages of using powder particles for fabrication ( Ref 4...
Abstract
According to International Organization for Standardization (ISO)/ASTM International 52900, additive manufacturing (AM) can be classified into material extrusion, material jetting, vat photo polymerization, binder jetting, sheet lamination, powder-bed fusion (PBF), and directed-energy deposition. This article discusses the processes involved in polymer powder 3D printing using laser fusion/ sintering and fusing agents and energy, as well as the thermally fused PBF. It provides information on polymer powder parameters and modeling, the powder-handling system, powder characterization, the flowability of powder feedstock, and polymer part characteristics. The article describes the types of polymers in PBF, the processes involved in powder recycling, and the prospects of PBF in AM. In addition, the biomedical application of polyether ether ketone (PEEK) is also covered.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006109
EISBN: 978-1-62708-175-7
... composition cohesive strength compressibility flow rate frictional properties green strength metal powders particle morphology powder segregation rectangular test bar springback tap density POWDER METALLURGY (PM), metal injection molding, and additive manufacturing have grown considerably...
Abstract
This article describes the methods for determining the flow rate of metal powders. It examines the factors affecting flow rate, apparent density, and angle of repose of metal powders. The article reviews the frictional properties, cohesive strength, frictional properties, tap density, and compressibility of metal powders. It explains the mechanisms of powder segregation. The article provides information on green strength and springback value of rectangular test bar. It concludes with a discussion on the chemical composition of metal powders.
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 December 1998
DOI: 10.31399/asm.hb.mhde2.a0003185
EISBN: 978-1-62708-199-3
... Abstract This article focuses on the significant fundamental powder characteristics, which include particle size, particle size distribution, particle shape, and powder purity, followed by an overview of general and individual powder production processes such as mechanical, chemical...
Abstract
This article focuses on the significant fundamental powder characteristics, which include particle size, particle size distribution, particle shape, and powder purity, followed by an overview of general and individual powder production processes such as mechanical, chemical, electrochemical, atomizing, oxide reduction, and thermal decomposition processes. It also covers the consolidation of powders by pressing and sintering, as well as by high density methods. Further emphasis is provided on the distinguishing features of powders, their manufacturing processes, compacting processes, and consolidated part properties. In addition, a glossary of powder metallurgy terms is included.
Series: ASM Handbook
Volume: 20
Publisher: ASM International
Published: 01 January 1997
DOI: 10.31399/asm.hb.v20.a0002486
EISBN: 978-1-62708-194-8
... the powders. Because a die or mold provides the container for the consolidation step, the ease of manufacture of the container and the ability to remove a green compact (unsintered) from the container, in most cases, determines the allowable shape complexity of a given part. Tolerances Control...
Abstract
This article begins with a discussion on general powder metallurgy design considerations that assist in the selection of the appropriate processing method. It reviews powder processing techniques, conventional press-and-sinter methods, and full-density processes to understand the design restrictions of each powder processing method. The article provides comparison of powder processing methods based on their similarities, differences, advantages, and disadvantages. It concludes with a discussion on design issues for the components of powder processing technologies.
Series: ASM Handbook
Volume: 1
Publisher: ASM International
Published: 01 January 1990
DOI: 10.31399/asm.hb.v01.a0001044
EISBN: 978-1-62708-161-0
... to produce green compacts. These are then sintered, or diffusion bonded, at elevated temperatures in a furnace with a protective atmosphere. During sintering, the constituents usually do not melt, and the compacts become substantially strengthened by the development of bonds between individual particles...
Abstract
Certain metal products can be produced only by powder metallurgy; among these products are materials whose porosity is controlled. Successful production by powder metallurgy depends on the proper selection and control of process variables: powder characteristics; powder preparation; type of compacting press; design of compacting tools and dies; type of sintering furnace; composition of the sintering atmosphere; choice of production cycle, including sintering time and temperature; and secondary operations and heat treatment. When the application of a powder metallurgy part requires high levels of strength, toughness, or hardness, the mechanical properties can be improved or modified by infiltration, heat treatment, or a secondary mechanical forming operation such as cold re-pressing or powder forging. The article also discusses the effect of the secondary processes on P/M mechanical properties.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006111
EISBN: 978-1-62708-175-7
... longer times. Figure 9 illustrates how microstructure is influenced by sintering time at 1120 °C (2050 °F). Figure 9(a) , a microstructure of an unsintered bar, shows the individual particles, grains within particles, and graphite located primarily at the pores formed between particles. Figure 9(b...
Abstract
This article provides information on the most frequently used atmospheres in commercial sintering of powder metallurgy iron and steel materials. These include endothermic, exothermic, dissociated ammonia, pure hydrogen, and nitrogen-base atmospheres. The article discusses sintering of iron and iron-graphite powder, iron-copper and iron-copper graphite, and alloy steels. The effects of various sinter conditions on the amount of combined carbon formed in the steel are also discussed. The article concludes with information on high-temperature sintering and sinter hardening.
Book Chapter
Materials Standards and Test Method Standards for Powder Metallurgy
Available to PurchaseBook: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006019
EISBN: 978-1-62708-175-7
... and tests for such properties as particle size, apparent density, tap density, flow rate, compressibility, and green strength. Powder characteristics are directly related to the method used to produce the powder, and properties such as reactivity, shape, and hardness of the powder particles influence...
Abstract
The organizations that are most active in the development of standards for powder metallurgy (PM) are the American Society for Testing and Materials (ASTM), Metal Powder Industries Federation (MPIF), and International Standards Organization (ISO). This article presents the test method standards, materials standards, and material designation codes for PM materials. It provides information on the codes for structural parts, PM soft magnetic materials, PM self-lubricating bearings, metal injection molded materials, and powder forged materials.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006112
EISBN: 978-1-62708-175-7
... Abstract Powder forging is a process in which unsintered, presintered, and sintered powder metallurgy preforms are hot formed in confined dies. This article provides information on the basic forms of powder forging and describes the material considerations, process considerations...
Abstract
Powder forging is a process in which unsintered, presintered, and sintered powder metallurgy preforms are hot formed in confined dies. This article provides information on the basic forms of powder forging and describes the material considerations, process considerations, and mechanical properties of powder forged (PF) steels. It reviews the parameters involved in quality assurance tests for PF parts. The article includes examples of PF components and highlights the reasons for selecting them over those made by competing forming methods.
Series: ASM Handbook
Volume: 14A
Publisher: ASM International
Published: 01 January 2005
DOI: 10.31399/asm.hb.v14a.a0003988
EISBN: 978-1-62708-185-6
... particle inspection mechanical properties metallographic analysis nondestructive testing powder characteristics powder forging quality assurance tests tool design POWDER FORGING is a process in which an unsintered, presintered, or sintered powder metal preform is forged in a confined or trapped...
Abstract
Powder forging is an extension of the conventional press and sinter powder metallurgy process, which is recognized as an effective technology for producing a variety of parts to net or near-net shape. This article focuses on the material considerations, such as powder characteristics, alloy development, and inclusion assessment; and process considerations, such as process stages, tool design, and secondary operations; of ferrous alloy powder forging. The mechanical properties of powder forged materials are also reviewed. The article discusses the quality assurance tests for powder forged materials: the part dimensions and surface finish measurement, magnetic particle inspection, metallographic analysis, and nondestructive testing. It concludes with a discussion on the applications of powder forged parts with examples.
Book Chapter
Glass Processing
Available to PurchaseSeries: ASM Desk Editions
Publisher: ASM International
Published: 01 November 1995
DOI: 10.31399/asm.hb.emde.a0003065
EISBN: 978-1-62708-200-6
..., are particularly detrimental. Rather than melting, they form discrete defects, which necessitates the scrapping of any glass containing them. The preferred size distribution of sand contains no more than 5 to 10% of particles retained on 40 mesh, and no more than 5 to 10% can pass 140 mesh. Particle size...
Abstract
The large majority of the commercially important glasses are processed from a carefully calculated batch of raw materials that is then melted in special furnaces. Providing an introduction to melting practices of glass production, this article focuses on various finishing methods of glass products, including forming, grinding and polishing, and explores the advantages, disadvantages and steps involved in sol-gel process. It also discusses the types, processes and properties of annealed, laminated, and tempered glass, and presents the steps involved in glass decoration. The article gives a detailed account of production, properties and application of fiberglass, optical fibers, glass spheres and ceramic glasses, and describes the forms, classification, compositions and properties of glass/metal and glass-ceramic/metal seals.
Series: ASM Handbook
Volume: 23A
Publisher: ASM International
Published: 12 September 2022
DOI: 10.31399/asm.hb.v23A.a0006859
EISBN: 978-1-62708-392-8
... for Cellular Responses to Particles In Vitro” ASTM International F 1904-14 “Standard Practice for Testing the Biological Responses to Particles In Vivo” ASTM International F 1983-14 “Standard Practice for Assessment of Compatibility of Absorbable/Resorbable Biomaterials for Implant Applications...
Abstract
Powder-bed fusion (PBF) is a group of additive manufacturing (AM) processes that includes selective laser sintering, selective laser melting, and electron beam melting. This article explains the processes and parameters of PBF systems that are used for biomedical applications. It also presents the desirable properties of biomedical devices and the advantages of using PBF systems for biomedical applications.
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