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Series: ASM Handbook
Volume: 8
Publisher: ASM International
Published: 01 January 2000
DOI: 10.31399/asm.hb.v08.a0003275
EISBN: 978-1-62708-176-4
... or IRHD testers; scratch hardness tests; and ultrasonic microindentation testing. This article reviews the procedures, equipment, and applications associated with these alternate hardness test methods. miscellaneous hardness test Leeb scale hardness testing scleroscope hardness testing durometer...
Abstract
Miscellaneous hardness tests encompass a number of test methods that have been developed for specific applications. These include dynamic, or "rebound," hardness tests using a Leeb tester or a Scleroscope; static indentation tests on rubber or plastic products using the durometer or IRHD testers; scratch hardness tests; and ultrasonic microindentation testing. This article reviews the procedures, equipment, and applications associated with these alternate hardness test methods.
Series: ASM Handbook
Volume: 8
Publisher: ASM International
Published: 01 January 2000
DOI: 10.31399/asm.hb.v08.a0003325
EISBN: 978-1-62708-176-4
... techniques include X-ray diffraction, neutron diffraction, Barkhausen noise analysis, and ultrasonic propagation analysis. The article concludes with an overview of weldability testing. bend strength ductility fracture toughness hardness hole drilling chip machining groove machining block...
Abstract
This article discusses the standard test methods that can be applied to many types of welds: tension, bending, impact, and toughness testing. It provides information on four qualification stages, namely, the weld material qualification, base material qualification, the weld procedure qualification, and the weld service assessment. The article describes two general types of measurements for residual stress in welds: locally destructive techniques and nondestructive techniques. Locally destructive techniques include hole drilling, chip machining, and block sectioning. Nondestructive techniques include X-ray diffraction, neutron diffraction, Barkhausen noise analysis, and ultrasonic propagation analysis. The article concludes with an overview of weldability testing.
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006761
EISBN: 978-1-62708-295-2
... testing, macroindentation hardness, microindentation hardness, and the impact toughness test. bend testing failure analysis impact toughness test macroindentation hardness microindentation hardness static load testing uniaxial compression testing uniaxial tension testing Mechanical Testing...
Abstract
Mechanical testing is an evaluative tool used by the failure analyst to collect data regarding the macro- and micromechanical properties of the materials being examined. This article provides information on a few important considerations regarding mechanical testing that the failure analyst must keep in mind. These considerations include the test location and orientation, the use of raw material certifications, the certifications potentially not representing the hardware, and the determination of valid test results. The article introduces the concepts of various mechanical testing techniques and discusses the advantages and limitations of each technique when used in failure analysis. The focus is on various types of static load testing, hardness testing, and impact testing. The testing types covered include uniaxial tension testing, uniaxial compression testing, bend testing, hardness testing, macroindentation hardness, microindentation hardness, and the impact toughness test.
Series: ASM Handbook
Volume: 8
Publisher: ASM International
Published: 01 January 2000
DOI: 10.31399/asm.hb.v08.a0003276
EISBN: 978-1-62708-176-4
... HARDNESS TESTING includes a variety of techniques that can be generally classified into the following categories ( Ref 1 ): Indentation tests (such as Brinell, Rockwell, Vickers, Knoop, and ultrasonic testing) Scratch tests (such as the Mohs test) Dynamic tests (such as the Shore test...
Abstract
This article reviews the factors that have a significant effect on the selection and interpretation of results of different hardness tests, namely, Brinell, Rockwell, Vickers, and Knoop tests. The factors concerned include hardness level (and scale limitations), specimen thickness, size and shape of the workpiece, specimen surface flatness and surface condition, and indent location. The article focuses on the selection for specific types of materials, such as steels, cast irons, nonferrous alloys, and plastics, and industrial applications, of hardness tests.
Book Chapter
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006757
EISBN: 978-1-62708-295-2
... often results in a suppression of the surface features that are desired. Flexible fiber-optic lighting is often the most appropriate method of illumination. Figure 9 shows a view of the fracture surface of a tensile test specimen from a cast steel that has suffered embrittlement, resulting in a “rock...
Abstract
Examination of a damaged component involves a chain of activities that, first and foremost, requires good observation and documentation. Following receipt and documentation, the features of damage can be recorded and their cause(s) investigated, as this article briefly describes, for typical types of damage experienced for metallic components. This article discusses the processes involved in visual or macroscopic examination of damaged material; the interpretation of fracture features, corrosion, and wear damage features; and the analysis of base material composition. It covers the processes involved in the selection of metallurgical samples, the preparation and examination of metallographic specimens in failure analysis, and the analysis and interpretation of microstructures. Examination and evaluation of polymers and ceramic materials in failure analysis are also briefly discussed.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003522
EISBN: 978-1-62708-180-1
... method of illumination. Figure 9 shows a view of the fracture surface of a tensile test specimen from a cast steel that has suffered embrittlement, resulting in a “rock candy” fracture. Fig. 9 Low-power light microscope view of a “rock candy” fracture in a tensile specimen taken from a cast...
Abstract
This article focuses on the visual or macroscopic examination of damaged materials and interpretation of damage and fracture features. Analytical tools available for evaluations of corrosion and wear damage features include energy dispersive spectroscopy, electron probe microanalysis, Auger electron spectroscopy, secondary ion mass spectroscopy, and X-ray powder diffraction. The article discusses the analysis and interpretation of base material composition and microstructures. Preparation and examination of metallographic specimens in failure analysis are also discussed. The article concludes with a review of the evaluation of polymers and ceramic materials in failure analysis.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006056
EISBN: 978-1-62708-175-7
... ranges for the American Society for Testing and Materials (ASTM) standard methods of particle sizing and distribution. It presents the methods used to analyze the chemical composition of cemented carbide materials in a tabular form. The article also presents information on microstructural evaluation...
Abstract
Quality control of cemented carbides includes the evaluation of physical and chemical properties of constituent raw material powders, powder blends/formulations, green compacts, and fully dense finished product. This article provides a summary of the underlying principles and size ranges for the American Society for Testing and Materials (ASTM) standard methods of particle sizing and distribution. It presents the methods used to analyze the chemical composition of cemented carbide materials in a tabular form. The article also presents information on microstructural evaluation and physical and mechanical property evaluation of cemented carbides.
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.9781627082952
EISBN: 978-1-62708-295-2
Book: Thermal Spray Technology
Series: ASM Handbook
Volume: 5A
Publisher: ASM International
Published: 01 August 2013
DOI: 10.31399/asm.hb.v05a.a0005730
EISBN: 978-1-62708-171-9
... the tests for the measurement of the hardness of coatings. The Vickers hardness test is the standard microhardness test employed for thermal spray coatings (Knoop microindentation hardness testing is less widely used). As shown in Fig. 1 , the Vickers hardness test uses a square-based diamond pyramid...
Abstract
This article describes the two commonly used standardized tests for determining the mechanical properties of thermal spray coatings: hardness testing and tensile adhesion testing. It discusses the destructive and non-destructive methods of residual-stress measurement. Electrochemical testing methodologies include two distinctly different methods: direct and alternating current impedance techniques for assessing the corrosion resistance of coating attributes. The article also reviews the testing methods for determining thermomechanical and environmental stability of thermal barrier coatings. It discusses the wear testing methodologies that are standardized by ASTM, including the pin-on-disk, block-on-ring, dry sand/rubber wheel, erosion, metallographic apparatus abrasion, fretting wear, cavitation, reciprocating ball-on-flat, impact, and rolling contact fatigue test. The article concludes with a discussion on the methods of testing abradability and erosion resistance in abradable coatings.
Series: ASM Handbook
Volume: 14B
Publisher: ASM International
Published: 01 January 2006
DOI: 10.31399/asm.hb.v14b.a0009000
EISBN: 978-1-62708-186-3
... treatments, or surface locations, depending on the measurement technique (indentation or impedance) and/or load used (smaller loads for thinner surface coating films). Particularly, the Vickers hardness tests are destructive due to the microindentation and thus can be used only after the completion...
Abstract
This article describes the laboratory techniques for direct measurement and quantification of die wear in verifying a proprietary die-wear predictor methodology. This method is based on a theoretical formula that can be used to predict the rate of die wear and the life of a die surface coating, applicable to both mild steel and high-strength steels stampings. The article discusses the behavior of the surface conditions through quantitative measurements and surface analyses conducted throughout the wear tests. The surface conditions include surface roughness, surface morphology, microstructure, interfacial friction, surface temperatures, and wear rate.
Book Chapter
Book: Thermal Spray Technology
Series: ASM Handbook
Volume: 5A
Publisher: ASM International
Published: 01 August 2013
DOI: 10.31399/asm.hb.v05a.a0005748
EISBN: 978-1-62708-171-9
.... release agent. porous substance. ablation. A self-regulating heat- and mass- acoustic emission. A measure of the integrity transfer process in which incident thermal accelerated corrosion test. Test method of a material as determined by sound emis- energy is expended by a loss of material. designed...
Abstract
This article is a compilation of definition of the terms related to thermal spray coating technology.
Book: Composites
Series: ASM Handbook
Volume: 21
Publisher: ASM International
Published: 01 January 2001
DOI: 10.31399/asm.hb.v21.a0003374
EISBN: 978-1-62708-195-5
.... The direct methods include the fiber pullout method, the single-fiber fragmentation method, the embedded fiber compression method, and the microindentation method. The indirect methods for fiber-matrix adhesion testing include the variable curvature method, the slice compression test, the ball compression...
Abstract
Fiber-matrix adhesion is a variable to be optimized in order to get the best properties and performance in composite materials. This article schematically illustrates fiber matrix interphase for composite materials. It discusses thermodynamics of interphase in terms of surface energy, contact angle, work of adhesion, solid surface energy, and wetting and wicking. The article describes the change in interphase depending on the reinforcing fiber such as glass fiber, polymeric fiber, and carbon fiber. It emphasizes fiber-matrix adhesion measurements by direct methods, indirect methods, and composite laminate tests. The effects of interphase and fiber-matrix adhesion on composite mechanical properties, such as composite on-axis properties, composite off-axis properties, and composite fracture properties, are also discussed.
Series: ASM Handbook
Volume: 11A
Publisher: ASM International
Published: 30 August 2021
DOI: 10.31399/asm.hb.v11A.a0006828
EISBN: 978-1-62708-329-4
... for Torch Brazing” C3.5 “Specification for Induction Brazing” C3.6 “Specification for Furnace Brazing” C3.8 “Specification for Ultrasonic Pulse-Echo of Brazed Joints” A5.8 “Specification for Filler Metals for Brazing and Braze Welding” Nondestructive Testing Some...
Abstract
The various methods of furnace, torch, induction, resistance, dip, and laser brazing are used to produce a wide range of highly reliable brazed assemblies. However, imperfections that can lead to braze failure may result if proper attention is not paid to the physical properties of the material, joint design, prebraze cleaning, brazing procedures, postbraze cleaning, and quality control. Factors that must be considered include brazeability of the base metals; joint design and fit-up; filler-metal selection; prebraze cleaning; brazing temperature, time, atmosphere, or flux; conditions of the faying surfaces; postbraze cleaning; and service conditions. This article focuses on the advantages, limitations, sources of failure, and anomalies resulting from the brazing process. It discusses the processes involved in the testing and inspection required of the braze joint or assembly.
Book Chapter
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 December 1998
DOI: 10.31399/asm.hb.mhde2.a0003241
EISBN: 978-1-62708-199-3
... is reasonably homogeneous. However, studies of microindentation hardness test results conducted over the, past several years on a wide range of loads have shown that results are not constant at very low loads. This problem, called the “indentation size effect” (ISE), has been attributed to fundamental...
Abstract
This article reviews the various types of mechanical testing methods, including hardness testing; tension testing; compression testing; dynamic fracture testing; fracture toughness testing; fatigue life testing; fatigue crack growth testing; and creep, stress-rupture, and stress-relaxation testing. Shear testing, torsion testing, and formability testing are also discussed. The discussion of tension testing includes information about stress-strain curves and the properties described by them.
Book
Series: ASM Handbook
Volume: 5
Publisher: ASM International
Published: 01 January 1994
DOI: 10.31399/asm.hb.v05.9781627081702
EISBN: 978-1-62708-170-2
Book Chapter
Book: Surface Engineering
Series: ASM Handbook
Volume: 5
Publisher: ASM International
Published: 01 January 1994
DOI: 10.31399/asm.hb.v05.a0005585
EISBN: 978-1-62708-170-2
... of liquid nitriding in which air is pumped through the molten bath creating agitation and increased chemical activity. AFS 50-70 test sand. A rounded quartz sand specified for use as an abrasive in the dry sandrubber wheel test (ASTM G 65). Using the thisU.S. Sieve Series, none of sand will be retained...
Abstract
This article is a compilation of terms related to surface engineering of irons, steels, and nonferrous metals.
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006754
EISBN: 978-1-62708-295-2
... or corrosion damage; find crack origin(s); take better photos than may be possible outside of the lab; allow the investigation to proceed Before subsequent destructive testing Ultrasonic testing Document presence or absence and size and orientation of secondary cracks Before subsequent destructive...
Abstract
Failure analysis is a process that is performed in order to determine the causes or factors that have led to an undesired loss of functionality. This article is intended to demonstrate proper approaches to failure analysis work. The goal of the proper approach is to allow the most useful and relevant information to be obtained. The discussion covers the principles and approaches in failure analysis work, objectives and scopes of failure analysis, the planning stages for failure analysis, the preparation of a protocol for a failure analysis, practices used by failure analysts, and procedures of failure analysis.
Series: ASM Handbook
Volume: 5A
Publisher: ASM International
Published: 01 August 2013
DOI: 10.31399/asm.hb.v05a.9781627081719
EISBN: 978-1-62708-171-9
Series: ASM Handbook
Volume: 8
Publisher: ASM International
Published: 01 January 2000
DOI: 10.31399/asm.hb.v08.a0003309
EISBN: 978-1-62708-176-4
... Abstract This article describes the types, mechanism, and typical test methods along with their configurations for the evaluation of hydrogen embrittlement, stress-corrosion cracking, and corrosion fatigue with an emphasis on fracture mechanics methodologies for metals. An overview...
Abstract
This article describes the types, mechanism, and typical test methods along with their configurations for the evaluation of hydrogen embrittlement, stress-corrosion cracking, and corrosion fatigue with an emphasis on fracture mechanics methodologies for metals. An overview on the environmentally assisted crack growth of polymers is also included. The article details the evaluation of nanoscale environmental effects and indentation-induced cohesive cracking. It also provides information on scanning probe microscopy.
Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0003789
EISBN: 978-1-62708-177-1
... will not suffice. Because test method ASTM B 328 ( Ref 1 ) cannot be used to measure density differences over short distances such as 0.25 to 6.25 mm (0.01 to 0.25 in.), the true amount of porosity must be determined by image analysis to facilitate local density measurement. When the specimen is properly prepared...
Abstract
This article provides information on the microstructure of powder metal alloys and the special handling requirements of porous materials. It covers selection, sectioning, mounting, grinding, and polishing, and describes procedures, such as washing, liquid removal, and impregnation, meant to preserve pore structures and keep them open for analysis. The article compares and contrasts the microstructures of nearly 50 powder metal alloys, using them to illustrate the effect of consolidation and compaction methods as well as particle size, composition, and shape. It discusses imaging equipment and techniques and provides data on etchants and etching procedures.
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