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transmitted polarized light
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Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0009083
EISBN: 978-1-62708-177-1
... Abstract Honeycomb-cored sandwich panels increase part stiffness at a lower weight than monolithic composite materials. This article illustrates an area of a honeycomb-cored sandwich structure composite cross section that is viewed using transmitted polarized light. This area shows...
Abstract
Honeycomb-cored sandwich panels increase part stiffness at a lower weight than monolithic composite materials. This article illustrates an area of a honeycomb-cored sandwich structure composite cross section that is viewed using transmitted polarized light. This area shows the differences in the constituents and resin intermingling. The article discusses the factors that govern the honeycomb core movement and honeycomb core crush, with illustrations. Some common tests performed on honeycomb composites to characterize the skin-to-core bond strength are the climbing drum peel and flatwise tensile tests. The article concludes with a description on the reasons for core failure, which are analyzed after these tests.
Image
Published: 01 December 2004
Fig. 10 Fracture morphology of a primary-phase-toughened matrix composite after impact. (a) Onset of hackle formation and strain in front of the crack tip. Transmitted polarized light, full wave plate, 40× objective. (b) Hackles in the interlayer region of the composite. Transmitted polarized
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in Matrix Microstructure Analysis of Fiber-Reinforced Composites[1]
> Metallography and Microstructures
Published: 01 December 2004
plane. Transmitted polarized light, 10× objective. (b) Sectioned through the thickness and parallel to the fiber plane. Transmitted polarized light, 40× objective. (c) Close-up view of a spherulite that nucleated at the tip of a carbon fiber. Transmitted polarized light, 100× objective
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Image
Published: 01 December 2004
polarized light, full wave plate, 20× objective. (b) Hackle formation in the interlayer region. Transmitted polarized light, full wave plate, 40× objective. (c) Fracture in the interlayer area. Transmitted polarized light, full wave plate, 40× objective
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Image
Published: 01 December 2004
Fig. 4 Crystallinity in thermoplastic-matrix carbon fiber composites. (a) Crystalline region in the center area of a woven carbon fabric composite cross section. Ultrathin section, transmitted polarized light with a full wave plate (540 nm), 20× objective. (b) Fiber-induced spherulite growth
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Image
Published: 01 December 2004
Fig. 12 Fracture morphology in a particle interlayer-toughened thermoset-matrix composite. (a) Strain birefringence in the interlayer particles. Transmitted polarized light, 20× objective. (b) Some of the particles are found to bridge the formed cracks, and some particles are torn. Transmitted
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Image
Published: 01 December 2004
Fig. 7 Micrographs of an untoughened-matrix carbon fiber composite material after impact damage. (a) Fracture morphology showing no signs of hackle formation. Transmitted polarized light, full wave plate, 40× objective. (b) Area ahead of the crack tip. Transmitted polarized light, full wave
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Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0009081
EISBN: 978-1-62708-177-1
..., including matrix strains and fracture morphology, can be determined with the development of ultrathin sections and transmitted polarized light or one of many other contrast methods. Through the use of these techniques, a complete analysis of the damage response of fiber-reinforced composite materials...
Abstract
This article describes methods for analyzing impact-damaged composites in the aircraft industry. These include C-scan and x-radiography methods and optical microscopy. The article reviews brittle-matrix composite and tough-matrix composite failures. It explains the different types of composite failure mechanisms such as thermoplastic-matrix composite failure mechanisms, untoughened thermoset-matrix composite failure mechanisms, toughened thermoset-matrix composite failure mechanisms, dispersed-phase and rubber-toughened thermoset-matrix composite failure mechanisms, and particle interlayer-toughened composite failure mechanisms.
Image
Published: 01 December 2004
Fig. 2 Ultrathin section of an area of a honeycomb sandwich composite structure showing the effects of core movement during manufacturing and the resulting deformation and separation of the prepreg plies. (a) Transmitted crossed polarized light, 20× objective. (b and c) Transmitted polarized
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Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0009082
EISBN: 978-1-62708-177-1
... differential scanning calorimetry, x-ray analysis, or density measurements, these analytical methods provide little, if any, information on the origin and microstructure of the crystallinity in the composite. To determine the morphology of thermoplastic-matrix composites, transmitted polarized-light microscopy...
Abstract
Microstructural analysis of the composite matrix is necessary to understand the performance of the part and its long-term durability. This article focuses on the microstructural analysis of engineering thermoplastic-matrix composites and the influence of cooling rate and nucleation on the formation of spherulites in high-temperature thermoplastic-matrix carbon-fiber-reinforced composites. It also describes the microstructural analysis of a bio-based thermosetting-matrix natural fiber composite system.
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in Thin Section Preparation and Transmitted Light Microscopy for Fiber-Reinforced Composites[1]
> Metallography and Microstructures
Published: 01 December 2004
Fig. 13 Crystals formed in a high-temperature thermoplastic-matrix composite. Transmitted polarized light, 40× objective
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Published: 01 December 2004
Fig. 8 Hackle formation in a high-temperature thermosetting-matrix composite after impact. Transmitted polarized light, full wave plate, 40× objective
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Image
Published: 01 December 2004
Fig. 13 Fiber-matrix interfacial failure in an interlayer-toughened thermoset-matrix composite. Transmitted polarized light, full wave plate, 20× objective
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Published: 01 December 2004
Fig. 9 Interlayer strain and fracture after impact of a toughened thermo-setting-matrix composite. Transmitted polarized light, full wave plate, 40× objective
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in Matrix Microstructure Analysis of Fiber-Reinforced Composites[1]
> Metallography and Microstructures
Published: 01 December 2004
Fig. 3 Matrix morphology differences of an engineering thermoplastic glass fiber composite that was exposed to different cooling rates. (a) Slow cooling rate. (b) Quenched to room temperature. Micrographs were taken from ultrathin sections. Transmitted polarized light, 40× objective
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in Matrix Microstructure Analysis of Fiber-Reinforced Composites[1]
> Metallography and Microstructures
Published: 01 December 2004
Fig. 2 Micrographs taken from ultrathin sections of a high-temperature thermoplastic-matrix carbon fiber composite that were exposed to different cooling rates. (a) Slow cooled. (b) Fast cooled followed by annealing. (c) Fast cooled. Transmitted polarized light, 100× objective
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Book: Composites
Series: ASM Handbook
Volume: 21
Publisher: ASM International
Published: 01 January 2001
DOI: 10.31399/asm.hb.v21.a0003464
EISBN: 978-1-62708-195-5
...-fluorescence. The article also provides information on transmitted light microscopy. composite materials epi-bright-field illumination epi-dark-field illumination epi-fluorescence epi-polarized light failure analysis illumination methods mounting polishing quality control reflected light...
Abstract
Microscopy is a valuable tool in materials investigations related to problem solving, failure analysis, advanced materials development, and quality control. This article describes the sample preparation techniques of composite materials. These techniques include mounting, rough grinding, and polishing. The preparation techniques of ultrathin sections are also summarized. The article explains the illumination methods used by reflected light microscopy to view a specimen. These consist of epi-bright-field illumination, epi-dark-field illumination, epi-polarized light, and epi-fluorescence. The article also provides information on transmitted light microscopy.
Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0009071
EISBN: 978-1-62708-177-1
... section. Ultrathin section, transmitted polarized light with a full wave plate (540 nm), 20× objective. (b) Fiber-induced spherulite growth. Ultrathin section, transmitted polarized light with a full wave plate (540 nm), 20× objective. (c) Large spherulitic growth in a carbon fiber composite. Ultrathin...
Abstract
This article illustrates the polymer matrices used for composite materials. It describes the use of prepeg materials in manufacturing high-performance composites. The article discusses the various infusion processes for the development of fiber-reinforced composites, namely, resin transfer molding, vacuum-assisted resin transfer molding, and resin film infusion. It explains the composite- and matrix-toughening methods for fiber-reinforced composites, such as dispersed-phase toughening and interlayer toughening. The article concludes with information on optical microscopy, which provides an insight into the micro- and macrostructure of fiber-reinforced composites.
Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0009076
EISBN: 978-1-62708-177-1
...: Bright field Polarized light Phase contrast Differential interference contrast (DIC), also known as Nomarski Modulation contrast, also known as Hoffman modulation contrast Epi-illumination Optical staining The various methods of transmitted optical microscopy are used to enhance...
Abstract
This article describes the various aspects relating to the selection and preparation of ultrathin-section specimens of fiber-reinforced polymeric composites for examination by transmitted light microscopy. It provides information on the contrast-enhancement methods used by transmitted-light microscopy and optimization of microscope conditions. Examples of composite ultrathin sections analyzed using transmitted-light microscopy contrast methods are also presented.
Image
Published: 01 December 2004
Fig. 19 An illustration of the three Faraday effect geometries identified by the relative orientation of the incident polarized light transmitted compared to the magnetization direction. (a) Longitudinal Faraday effect: oblique incidence of polarized light transmitted through a material
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