Honeycomb-cored sandwich panels increase part stiffness at a lower weight than monolithic composite materials. This article illustrates an area of a honeycomb-cored sandwich structure composite cross section that is viewed using transmitted polarized light. This area shows the differences in the constituents and resin intermingling. The article discusses the factors that govern the honeycomb core movement and honeycomb core crush, with illustrations. Some common tests performed on honeycomb composites to characterize the skin-to-core bond strength are the climbing drum peel and flatwise tensile tests. The article concludes with a description on the reasons for core failure, which are analyzed after these tests.

Microscopy is a valuable tool in materials investigations related to problem solving, failure analysis, advanced materials development, and quality control. This article describes the sample preparation techniques of composite materials. These techniques include mounting, rough grinding, and polishing. The preparation techniques of ultrathin sections are also summarized. The article explains the illumination methods used by reflected light microscopy to view a specimen. These consist of epi-bright-field illumination, epi-dark-field illumination, epi-polarized light, and epi-fluorescence. The article also provides information on transmitted light microscopy.

This article describes methods for analyzing impact-damaged composites in the aircraft industry. These include C-scan and x-radiography methods and optical microscopy. The article reviews brittle-matrix composite and tough-matrix composite failures. It explains the different types of composite failure mechanisms such as thermoplastic-matrix composite failure mechanisms, untoughened thermoset-matrix composite failure mechanisms, toughened thermoset-matrix composite failure mechanisms, dispersed-phase and rubber-toughened thermoset-matrix composite failure mechanisms, and particle interlayer-toughened composite failure mechanisms.

Microstructural analysis of the composite matrix is necessary to understand the performance of the part and its long-term durability. This article focuses on the microstructural analysis of engineering thermoplastic-matrix composites and the influence of cooling rate and nucleation on the formation of spherulites in high-temperature thermoplastic-matrix carbon-fiber-reinforced composites. It also describes the microstructural analysis of a bio-based thermosetting-matrix natural fiber composite system.

This article illustrates the polymer matrices used for composite materials. It describes the use of prepeg materials in manufacturing high-performance composites. The article discusses the various infusion processes for the development of fiber-reinforced composites, namely, resin transfer molding, vacuum-assisted resin transfer molding, and resin film infusion. It explains the composite- and matrix-toughening methods for fiber-reinforced composites, such as dispersed-phase toughening and interlayer toughening. The article concludes with information on optical microscopy, which provides an insight into the micro- and macrostructure of fiber-reinforced composites.

This article describes the various aspects relating to the selection and preparation of ultrathin-section specimens of fiber-reinforced polymeric composites for examination by transmitted light microscopy. It provides information on the contrast-enhancement methods used by transmitted-light microscopy and optimization of microscope conditions. Examples of composite ultrathin sections analyzed using transmitted-light microscopy contrast methods are also presented.

The analysis of composite materials using optical microscopy is a process that can be made easy and efficient with only a few contrast methods and preparation techniques. This article is intended to provide information that will help an investigator select the appropriate microscopy technique for the specific analysis objectives with a given composite material. The article opens with a discussion of macrophotography and microscope alignment, and then goes on to describe various illumination techniques that are useful for specific analysis requirements. These techniques include bright-field illumination, dark-field illumination, polarized-light microscopy, interference and contrast microscopy, and fluorescence microscopy. The article also provides a discussion of sample preparation materials such as dyes, etchants, and stains for the analysis of composite materials using optical microscopy.

Electromagnetic signals at microwave and millimeter-wave frequencies are well suited for inspecting dielectric materials and composite structures in many critical applications. This article presents a partial list of reported nondestructive testing (NDT) application areas for microwaves. It discusses the advantages and limitations of inspection with microwaves. The article discusses the physical principles, including reflection and refraction, absorption and dispersion, scattering, and standing waves. It provides a discussion on terahertz (THz) imaging for nondestructive evaluation (NDE). The article concludes with information on ground-penetration radar (GPR) that uses electromagnetic radiation and detects the reflected signals from subsurface structures.

Measuring the thickness of thin films can be accomplished in many ways. This article focuses on the optical method of single-wavelength ellipsometry, two multiple-wavelength methods of reflectometry and spectroscopic ellipsometry for measuring the thickness of thin films. The general capabilities, principles and applications of ellipsometry and reflectometry are discussed in terms of nondestructive methods.

Lightning damage in polymer composites is manifested by damage at both the macroscopic or visual level and within the material microstructure. This article illustrates the effects of the laboratory-generated lightning strikes on polymeric composites.

Optical testing of plastics includes characterization of materials and analysis of optical components. This article focuses on procedures for testing various characteristics of optical components, including transmission and haze, yellowness, refractive index, birefringence, as well as surface irregularity, contamination, gloss, and color. It provides a short note on ad hoc testing, which is beneficial for practical applications in which lenses, prisms, and light pipes are being used and tested, as other test instruments are often not available.

This article describes the dispersed-phase toughening of thermoset matrices by the development of multiphase-structure thermosetting matrices using rubber and/or thermoplastic materials. It discusses two main methods for manufacturing prepregs, namely, single-pass impregnation and double-pass impregnation. The article illustrates reflected-light optical microscopy techniques to evaluate the morphology of thermoplastic materials for determining the material quality and correlating key microstructural features with material performance.

Microstructural analysis of specialized types of magnetic materials is centered on the examination of optical, electron, and scanning probe metallographic techniques unique to magnetic materials. This article provides a comprehensive overview of magnetic materials, their characteristics and sample preparation procedures. It reviews the methods pertaining to the microstructural examination of bulk magnetic materials, including microscopy techniques specified to magnetic materials characterization, with specific examples. The techniques used in the study of magnetic domain structures (microstructure) include the magneto-optical Kerr method, the Faraday method, the Bitter technique, scanning electron microscopy (magnetic contrast Types I and II), scanning electron microscopy with polarization analysis, Lorentz transmission electron microscopy, and magnetic force microscopy. The article also illustrates the microstructure of different types of soft magnetic material and permanent magnets.

Infrared (IR) spectroscopy is a useful technique for characterizing materials and providing information on the molecular structure, dynamics, and environment of a compound. This article provides the basic principles and instrumentation of IR spectroscopy. It discusses the sampling techniques of IR spectroscopy, namely, attenuated total reflectance spectroscopy, diffuse reflectance spectroscopy, infrared reflection-absorption spectroscopy, emission spectroscopy, and photoacoustic spectroscopy, and chromatographic techniques. Explaining the qualitative analysis of IR spectroscopy, the article provides information on spectral absorbance-subtraction, analysis of components in spectral matrix mixture, and determination of exact peak location of broad profiles. It discusses the quantitative analysis that mainly includes Beer's law for single compound in single wave number. The article also exemplifies the applications of IR spectroscopy.

Infrared (IR) spectra have been produced by transmission, that is, transmitting light through the sample, measuring the light intensity at the detector, and comparing it to the intensity obtained with no sample in the beam, all as a function of the infrared wavelength. This article discusses the sampling techniques and applications of IR spectra as well as the molecular structure information it can provide. The discussion begins with a description of the general principle of IR spectroscopy. This is followed by a section on commercial IR instruments. Sampling techniques and accessories necessary in obtaining the infrared spectrum of a material are then discussed. The article presents various techniques and methods involved in IR qualitative analysis and quantitative analysis. It ends with a few examples of the applications of IR spectroscopy.

This article provides information on the basic components of a light microscope, including the illumination system, collector lens, and optical and mechanical components. It describes optical performance in terms of image aberrations, resolution, and depth of field. The article discusses the examination of specimen surfaces using polarized light, phase contrast, oblique illumination, dark-field illumination, bright-field illumination, interference-contrast illumination, and phase contrast illumination. Special techniques and devices that may be used with the optical microscope, to obtain additional information, are also described. The article concludes with information on photomicroscopy and macrophotography.

This article considers the two primary methods used for ultrasonic inspection: pulse-echo and the transmission methods. Pulse-echo inspection can be accomplished with longitudinal, shear, surface (Rayleigh), or Lamb (plate) waves using a diverse range of transducers. The article discusses the principles of each of these inspection methods. It describes the applications and the basic data formats for single-element transducer-based systems, including A-scans, B-scans, and C-scans. The article provides information on electronic equipment used for ultrasonic inspection. It also describes how specific material conditions produce and modify A-scan indications. The article provides information on the controls and their functions for the display unit of the electronic equipment. It describes the techniques used for the identification and characterization of flaws, namely, surface (Rayleigh) wave and ultrasonic polar scan techniques.

Microwaves (or radar waves) are a form of electromagnetic radiation with wavelengths between 1000 cm and 1 mm in free space. One of the first important uses of microwaves in nondestructive evaluation was for components such as waveguides, attenuators, cavities, antennas, and antenna covers (radomes). This article focuses on the microwave inspection methods that were subsequently developed for evaluation of moisture content in dielectric materials; thickness measurements of thin metallic coatings on dielectric substrates; and detection of voids, delaminations, macroporosity, inclusions, and other flaws in plastic or ceramic materials. It also discusses the advantages and disadvantages and the general approaches that have been used in the development of microwave nondestructive inspection.

Microwaves (or radar waves) are a form of electromagnetic radiation with wavelengths between 1000 cm and 1 mm in free space. One of the first important uses of microwaves in nondestructive evaluation was for components such as waveguides, attenuators, cavities, antennas, and antenna covers (radomes). This article focuses on the microwave inspection methods that were subsequently developed for evaluation of moisture content in dielectric materials; thickness measurements of thin metallic coatings on dielectric substrates; and detection of voids, delaminations, macroporosity, inclusions, and other flaws in plastic or ceramic materials. It also discusses the advantages and disadvantages and the general approaches that have been used in the development of microwave nondestructive inspection.

This article focuses on some of the factors pertinent to atomic absorption spectroscopy (AAS). It begins by describing the working principle, critical components, and construction of flame atomic absorption instrumentation. This is followed by sections discussing various types of interferences in AAS, namely vaporization, ionization, matrix interferences, and background correction. Some of the methods for the analysis of microliter-sized samples and methods of standard additions to the sample solution for generating calibration standards are then reviewed. The article concludes with a section on processes involved in matrix matching.