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transmitted polarized light
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Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006662
EISBN: 978-1-62708-213-6
... Abstract Infrared (IR) spectra have been produced by transmission, that is, transmitting light through the sample, measuring the light intensity at the detector, and comparing it to the intensity obtained with no sample in the beam, all as a function of the infrared wavelength. This article...
Abstract
Infrared (IR) spectra have been produced by transmission, that is, transmitting light through the sample, measuring the light intensity at the detector, and comparing it to the intensity obtained with no sample in the beam, all as a function of the infrared wavelength. This article discusses the sampling techniques and applications of IR spectra as well as the molecular structure information it can provide. The discussion begins with a description of the general principle of IR spectroscopy. This is followed by a section on commercial IR instruments. Sampling techniques and accessories necessary in obtaining the infrared spectrum of a material are then discussed. The article presents various techniques and methods involved in IR qualitative analysis and quantitative analysis. It ends with a few examples of the applications of IR spectroscopy.
Book: Fractography
Series: ASM Handbook
Volume: 12
Publisher: ASM International
Published: 01 January 1987
DOI: 10.31399/asm.hb.v12.a0001834
EISBN: 978-1-62708-181-8
... intergranular and to determine if the fracture part is specific to any phase or constituent present. Although such specimens can be examined by scanning electron microscopy (SEM), light microscopy is more efficient for such work, and certain information, such as the color or polarization response of...
Abstract
This article presents examples of the visual fracture examination that illustrate the procedure as it applies to failure analysis and quality determination. It describes the techniques and procedures for the visual and light microscopic examination of fracture surfaces with illustrations. The article also describes microscopic and macroscopic features of the different fracture mechanisms with illustrations with emphasis on visual and light microscopy examination. The types of fractures considered include ductile fractures, tensile-test fractures, brittle fractures, fatigue fractures, and high-temperature fractures.
Book Chapter
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 November 1995
DOI: 10.31399/asm.hb.emde.a0003057
EISBN: 978-1-62708-200-6
... include reflected light microscopy using polarized light, scanning electron microscopy, transmission electron microscopy, energy dispersive analysis of X-rays, and wavelength dispersive analysis of X-rays. Macroscopic property characterization involves measurement of porosity, density, and surface area...
Abstract
This article describes testing and characterization methods of ceramics for chemical analysis, phase analysis, microstructural analysis, macroscopic property characterization, strength and proof testing, thermophysical property testing, and nondestructive evaluation techniques. Chemical analysis is carried out by X-ray fluorescence spectrometry, atomic absorption spectrophotometry, and plasma-emission spectrophotometry. Phase analysis is done by X-ray diffraction, spectroscopic methods, thermal analysis, and quantitative analysis. Techniques used for microstructural analysis include reflected light microscopy using polarized light, scanning electron microscopy, transmission electron microscopy, energy dispersive analysis of X-rays, and wavelength dispersive analysis of X-rays. Macroscopic property characterization involves measurement of porosity, density, and surface area. The article describes testing methods such as room and high-temperature strength test methods, proof testing, fracture toughness measurement, and hardness and wear testing. It also explains methods for determining thermal expansion, thermal conductivity, heat capacity, and emissivity of ceramics and glass and measurement of these properties as a function of temperature.
Series: ASM Handbook
Volume: 17
Publisher: ASM International
Published: 01 August 2018
DOI: 10.31399/asm.hb.v17.a0006469
EISBN: 978-1-62708-190-0
... (Rayleigh) wave and ultrasonic polar scan techniques. electronic equipment pulse-echo method single-element transducer-based system surface wave technique transducers transmission method ultrasonic inspection ultrasonic polar scan technique THIS ARTICLE CONSIDERS the two primary methods...
Abstract
This article considers the two primary methods used for ultrasonic inspection: pulse-echo and the transmission methods. Pulse-echo inspection can be accomplished with longitudinal, shear, surface (Rayleigh), or Lamb (plate) waves using a diverse range of transducers. The article discusses the principles of each of these inspection methods. It describes the applications and the basic data formats for single-element transducer-based systems, including A-scans, B-scans, and C-scans. The article provides information on electronic equipment used for ultrasonic inspection. It also describes how specific material conditions produce and modify A-scan indications. The article provides information on the controls and their functions for the display unit of the electronic equipment. It describes the techniques used for the identification and characterization of flaws, namely, surface (Rayleigh) wave and ultrasonic polar scan techniques.
Book Chapter
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 November 1995
DOI: 10.31399/asm.hb.emde.a0003027
EISBN: 978-1-62708-200-6
... transmission) that remains the same regardless of the direction or the polarization of transmitted light is said to be isotropic. A material for which the refractive index depends on the direction and polarization of light is anisotropic. An anisotropic material is said to be optically birefringent. Some...
Abstract
Optical testing of plastics includes characterization of materials and analysis of optical components. This article focuses on procedures for testing various characteristics of optical components, including transmission and haze, yellowness, refractive index, birefringence, as well as surface irregularity, contamination, gloss, and color. It provides a short note on ad hoc testing, which is beneficial for practical applications in which lenses, prisms, and light pipes are being used and tested, as other test instruments are often not available.
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 December 1998
DOI: 10.31399/asm.hb.mhde2.a0003244
EISBN: 978-1-62708-199-3
... alloys, grain size can be revealed adequately in the as-polished condition using polarized light. There are aspects of structure, termed macrostructure, which can be observed with the unaided eye. Macrostructural examination is often a prelude to microstructural examination but also includes...
Abstract
This article describes the methods and equipments involved in the preparation of specimens for examination by light optical microscopy, scanning electron microscopy, electron microprobe analysis for microindentation hardness testing, and for quantification of microstructural parameters, either manually or by the use of image analyzers. Preparation of metallographic specimens generally requires five major operations: sectioning, mounting, grinding, chemical polishing, and etching. The article provides information on the principles of technique selection in mechanical polishing, and describes the procedures, advantages, and disadvantages of electrolytic and chemical polishing. It also provides a detailed account of procedures, precautions, and composition for preparation and handling of etchants.
Series: ASM Handbook
Volume: 23
Publisher: ASM International
Published: 01 June 2012
DOI: 10.31399/asm.hb.v23.a0005685
EISBN: 978-1-62708-198-6
... generally refers to reflected light microscopy. In this method, light is reflected from the sample surface through the microscope objective to an eyepiece, view screen, or camera. Transmitted light is occasionally used for transparent and translucent materials. For low-magnification work (stereomicroscopy...
Abstract
This article focuses on the modes of operation, physical basis, sample requirements, properties characterized, advantages, and limitations of common characterization methods that are used to evaluate the physical morphology and chemical properties of component surfaces for medical devices. The methods include light microscopy, scanning electron microscopy, atomic force microscopy, energy-dispersive x-ray spectroscopy, Auger electron spectroscopy, secondary ion mass spectrometry, x-ray photoelectron spectroscopy, Fourier transform infrared spectroscopy, and Raman spectroscopy.
Book Chapter
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 November 1995
DOI: 10.31399/asm.hb.emde.a0003067
EISBN: 978-1-62708-200-6
... in modern automotive air conditioning systems, have created a need for better solar reduction glass. Solar control automotive glass must reduce the solar energy transmitted without reducing the visible light transmission below the legal limit of 70%. Solar glass either reflects or absorbs the sun's...
Abstract
This article reviews the applications of traditional glasses in architecture, transportation, construction, houseware, containers, and fibers. It also describes uses of specialty glasses for aerospace and military applications, biomedical and dental applications, chemical-resistant applications, lighting, information display, electronic processing and electronic devices, optical and ophthalmic products, and communications equipment.
Book: Surface Engineering
Series: ASM Handbook
Volume: 5
Publisher: ASM International
Published: 01 January 1994
DOI: 10.31399/asm.hb.v05.a0001295
EISBN: 978-1-62708-170-2
... evaporated metal on a microscope slide can be determined by measuring the fraction of transmitted light, after suitable calibration. This requires a special substrate, however; it is not an in-line technique and will not be considered here. A basic requirement for using optical methods for...
Abstract
Measuring the thickness of thin films can be accomplished in many ways. This article focuses on the optical method of single-wavelength ellipsometry, two multiple-wavelength methods of reflectometry and spectroscopic ellipsometry for measuring the thickness of thin films. The general capabilities, principles and applications of ellipsometry and reflectometry are discussed in terms of nondestructive methods.
Book Chapter
Series: ASM Handbook
Volume: 17
Publisher: ASM International
Published: 01 August 2018
DOI: 10.31399/asm.hb.v17.a0006475
EISBN: 978-1-62708-190-0
... the electromagnetic wave, that is, the interaction of the electric and magnetic fields with the conductivity, permittivity, and permeability of the material. Microwaves behave much like light waves in that they travel in straight lines until they are reflected, refracted, diffracted, or scattered...
Abstract
Electromagnetic signals at microwave and millimeter-wave frequencies are well suited for inspecting dielectric materials and composite structures in many critical applications. This article presents a partial list of reported nondestructive testing (NDT) application areas for microwaves. It discusses the advantages and limitations of inspection with microwaves. The article discusses the physical principles, including reflection and refraction, absorption and dispersion, scattering, and standing waves. It provides a discussion on terahertz (THz) imaging for nondestructive evaluation (NDE). The article concludes with information on ground-penetration radar (GPR) that uses electromagnetic radiation and detects the reflected signals from subsurface structures.
Book Chapter
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 December 1998
DOI: 10.31399/asm.hb.mhde2.a0003235
EISBN: 978-1-62708-199-3
... longer than those of light waves, microwaves penetrate deeply into materials, with the depth of penetration dependent on the conductivity, permittivity, and permeability of the materials. Microwaves are also reflected from any internal boundaries and interact with the molecules that constitute the...
Abstract
Microwaves (or radar waves) are a form of electromagnetic radiation with wavelengths between 1000 cm and 1 mm in free space. One of the first important uses of microwaves in nondestructive evaluation was for components such as waveguides, attenuators, cavities, antennas, and antenna covers (radomes). This article focuses on the microwave inspection methods that were subsequently developed for evaluation of moisture content in dielectric materials; thickness measurements of thin metallic coatings on dielectric substrates; and detection of voids, delaminations, macroporosity, inclusions, and other flaws in plastic or ceramic materials. It also discusses the advantages and disadvantages and the general approaches that have been used in the development of microwave nondestructive inspection.
Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006653
EISBN: 978-1-62708-213-6
..., absorbance is logarithmically related to the ratio of the incident ( I 0 ) and transmitted ( I ) light intensities, which limits the range of usable measurements ( Ref 3 ). Obtaining the maximum sensitivity requires optimization of each parameter, that is, maximum production of atoms for observation...
Abstract
This article focuses on some of the factors pertinent to atomic absorption spectroscopy (AAS). It begins by describing the working principle, critical components, and construction of flame atomic absorption instrumentation. This is followed by sections discussing various types of interferences in AAS, namely vaporization, ionization, matrix interferences, and background correction. Some of the methods for the analysis of microliter-sized samples and methods of standard additions to the sample solution for generating calibration standards are then reviewed. The article concludes with a section on processes involved in matrix matching.
Book: Corrosion: Materials
Series: ASM Handbook
Volume: 13B
Publisher: ASM International
Published: 01 January 2005
DOI: 10.31399/asm.hb.v13b.a0003844
EISBN: 978-1-62708-183-2
... the potential introduction or formation of reactive polar groups that may cause changes in compatibility and electrical and optical behavior of the polymer. Additionally, introduction of light-absorbing groups (chromophores) may cause discoloration and internal cyclization of polymer chains, resulting...
Abstract
Paints and protective coatings are the most common means of protecting materials from deterioration. This article focuses on coating degradation resulting from the environmental interaction with the coatings. The major environmental influences that result in coating degradation include energy (solar radiation, heat and temperature variation, and nuclear radiation), permeation (moisture, solvent retention, chemical, and oxygen), stress (drying and curing, vibration, and impact and abrasion), and biological influences (microbiological and macrobiological).
Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.9781627082136
EISBN: 978-1-62708-213-6
Book Chapter
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 November 1995
DOI: 10.31399/asm.hb.emde.a0003026
EISBN: 978-1-62708-200-6
... broad use for electrical wire and cable jackets. GRS, Buna S SBR Styrene-butadiene Electrical properties generally good but not specifically outstanding in any area Buna N, nitrile NBR Acrylonitrile-butadiene Electrical properties not outstanding; probably degraded by molecular polarity of...
Abstract
In terms of their electrical properties, plastics can be divided into thermosetting and thermoplastic materials, some of which are conductive or semiconductive. This article provides detailed information on factors that affect the property of plastics. It discusses the major test methods used to determine the following dielectric properties of plastics: dielectric breakdown voltage, dielectric strength, dielectric constant, dissipation factor, arc tracking resistance, insulation resistance, volume, and surface resistivity or conductivity. The test specifications and conditions, recommended by several U.S. and foreign testing organizations for characterizing the electrical properties of plastic materials are listed. The article describes the influence of these properties on selection of plastics for insulation application. An outline of the electromagnetic shielding and testing methods of electromagnetic interference are also provided. Designations, electrical properties, and applications of elastomers are tabulated.
Book Chapter
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 December 1998
DOI: 10.31399/asm.hb.mhde2.a0003236
EISBN: 978-1-62708-199-3
... (bubbler or squirter) techniques are most effective because they provide efficient and relatively uniform coupling between the search units and the test piece. In contrast to electromagnetic waves, such as light and x-rays, ultrasonic waves are mechanical waves consisting of oscillations, or...
Abstract
Ultrasonic inspection is a nondestructive method in which beams of high-frequency acoustic energy are introduced into a material to detect surface and subsurface flaws, to measure the thickness of the material, and to measure the distance to a flaw. This article provides a detailed account of ultrasonic flaw detectors, including ultrasonic transducers and types of search units and couplants. The article describes pulse-echo and transmission inspection methods and data interpretation. The general characteristics of ultrasonic waves and the factors influencing ultrasonic inspection are also addressed. The article concludes with a review of the advantages and disadvantages of ultrasonic inspection compared with other methods applications of the technique.
Series: ASM Handbook
Volume: 5B
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v05b.a0006073
EISBN: 978-1-62708-172-6
... exposure still occurs in indoor environments exposed to sunlight. Even though window glass filters out most UV light, the energy that transmits through the glass is still sufficient to degrade and fade most materials, including coatings over time. It is generally accepted that radiation in the visible...
Abstract
This article discusses the environmental influences on protective coating films that can result in deterioration. These environmental factors can be classified into four groups: (1) energy: solar, heat; (2) permeation: moisture, solvent, chemical, and gas; (3) stress: drying and curing-internal stress, and vibration-external stress; and (4) biological influences such as microbiological, mildew, and marine fouling.
Series: ASM Handbook
Volume: 17
Publisher: ASM International
Published: 01 August 2018
DOI: 10.31399/asm.hb.v17.a0006460
EISBN: 978-1-62708-190-0
... unpolarized light, whereas the use in reflection requires polarizing optics for optimal operation. Therefore, often in practice, especially if a large core multimode fiber is used to transmit light to the Fabry-Perot, the transmission configuration gains a sensitivity factor of approximately 2 with...
Abstract
Laser-ultrasonics is a particular implementation of ultrasonic nondestructive inspection in which ultrasound is generated and detected by lasers. This article discusses the various mechanisms that ensure ultrasound generation and explains the possibility to get the equivalent of phase-array by numerical processing of an array of previously acquired laser-ultrasonic signals. The article describes the ultrasound generation by thermoelastic mechanism and ablation or vaporization. It illustrates the principle of optical detection of ultrasound with confocal Fabry-Perot interferometer and photorefractive two-wave mixing interferometer. The article concludes with information on the industrial applications of laser-ultrasonics, including thickness measurement, flaw detection, and material characterization.
Series: ASM Handbook Archive
Volume: 10
Publisher: ASM International
Published: 01 January 1986
DOI: 10.31399/asm.hb.v10.9781627081788
EISBN: 978-1-62708-178-8
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 November 1995
DOI: 10.31399/asm.hb.emde.a0003062
EISBN: 978-1-62708-200-6
... strongly piezoelectric, and rapid strides have been made in their development and use as actuator motors, as ultrasonic transducers, and for electromechanical sensing. Piezoelectrics (PLZT) also elicit wide interest as electrooptic materials for such applications as high-speed shutters, switches, and light...
Abstract
Ceramic materials serve important insulative, capacitive, conductive, resistive, sensor, electrooptic, and magnetic functions in a wide variety of electrical and electronic circuitry. This article focuses on various applications of advanced ceramics in both electric power and electronics industry, namely, dielectric, piezoelectric, ferroelectric, sensing, magnetic and superconducting devices.