Time-of-flight diffraction (TOFD) is an ultrasonic technique used to detect diffracted waves from crack tips and to size the cracks from the arrival times of those waves. This article discusses the basic considerations and provides information on probe selection, gain setting, and instrumentation of TOFD. It describes the numerous effects that result from modifying the probe characteristics. The article provides the American Society of Mechanical Engineers (ASME), the European Committee for Standardization (CEN), and the International Standardization Organization (ISO) recommendations for the reference blocks according to applicable codes and standards. It also provides the ASME, CEN, and ISO recommendations for examination of welds. The article concludes with information on the interpretation and analysis of TOFD images with an aid of sizing algorithms.

Particle size and size distribution have a significant effect on the behavior of metal powders during their processing. This article provides an overview of the sample preparation process for particle size measurement, which is a key step in the measurement of particle size distributions. Common particle size measuring techniques discussed in this article include sieve analysis, quantitative image analysis, laser diffraction, sedimentation methods, aerodynamic time-of-flight method, electrical zone sensing, and photon correlation spectroscopy. The advantages and disadvantages of these methods are reviewed.

This article discusses the inspection/reference standards that are absolutely critical for proper application of ultrasonic inspection systems. Many of the standards and specifications for ultrasonic inspection require the use of standard reference blocks. The article lists the variables that should be considered when selecting standard reference blocks and describes the three types of standard blocks ordinarily used for calibration or reference: area-amplitude blocks, distance-amplitude blocks, and blocks of the type sanctioned by the International Institute of Welding. It reviews the determination of area-amplitude and distance-amplitude curves of a straight-beam pulse-echo ultrasonic inspection system. The article discusses the three principal conventional manual ultrasonic sizing techniques: 6 dB drop technique, maximum-amplitude technique, and 20 dB drop technique. It provides information on the dimension-measurement applications of ultrasonic inspection methods.

Neutrons are a principal tool for the study of lattice vibrational spectra in materials. This article provides a detailed account of fission and spallation methods of neutron production that are capable of producing sufficient intensity to be useful in neutron scattering research. It describes the instrumentation required for, and advancements made in, neutron powder diffraction. The article further explains the texture and residual stress (macrostresses and microstresses) problems that are analyzed using the neutron powder diffraction method. It also outlines the single-crystal neutron diffraction technique, and provides examples of the applications of neutron diffraction.

Nondestructive testing (NDT), also known as nondestructive evaluation (NDE), includes various techniques to characterize materials without damage. This article focuses on the typical NDE techniques that may be considered when conducting a failure investigation. The article begins with discussion about the concept of the probability of detection (POD), on which the statistical reliability of crack detection is based. The coverage includes the various methods of surface inspection, including visual-examination tools, scanning technology in dimensional metrology, and the common methods of detecting surface discontinuities by magnetic-particle inspection, liquid penetrant inspection, and eddy-current testing. The major NDE methods for internal (volumetric) inspection in failure analysis also are described.

This article focuses on the aspects associated with inspection related to pressure vessels and pipework. These aspects include inspection policy, inspection planning and procedures, inspection strategy, inspection methodology, preparation for inspection, invasive inspection, internal visual inspection, and non-invasive inspection. Inspection execution, risk-based inspection, competence assurance of inspection personnel, inspection coverage, inspection periodicity, inspection anomaly criteria, assessment of fitness, and reporting requirements, are also discussed. The article addresses the data acquisition, reporting and trending, and review and audit for the inspection. It reviews inspection techniques, including visual inspection, ultrasonic inspection, and radiographic inspection.

This article is a brief guide to information sources on nondestructive testing (NDT). It provides examples of some of the standards bodies commonly used by NDT personnel. These include the American Society for Testing and Materials (ASTM) International, European Committee for Standardization (CEN), American Society of Mechanical Engineers (ASME), International Organization for Standardization (ISO), Aerospace Industries Association (AIA), American Welding Society (AWS), American Petroleum Institute (API), and American Society for Nondestructive Testing (ASNT). All of these organizations used industry subject-matter experts and a consensus process in the development of their codes and standards.

Visual inspection (VI) is the oldest inspection technique man has used as a quality-control tool to evaluate products, assess their final form in terms of fabrication accuracy and external features based on experience, and decide on their acceptance or rejection. This article discusses the basic principles of visual inspection in terms of direct visual examination and indirect visual examination as well as advantages and limitations of visual inspection. It reviews the factors affecting the effectiveness of VI as a nondestructive testing (NDT): lighting conditions of observation, condition of surface under inspection, physical state/condition of inspector, proper training of personnel and level of expertise, and knowledge of applicable standards. The article provides schematic illustrations of rigid borescopes, fiberscopes, and videoscopes. It concludes with a discussion on automated optical inspection systems.

This article provides a brief introduction to neutron diffraction as well as its state-of-the-art capabilities. The discussion covers the general principles of the neutron, neutron-scattering theory, generation of neutrons, types of incident radiation, and purposes of single-crystal neutron diffraction, powder diffraction, and pair distribution function analysis. The relationship between detector space and reciprocal space are presented. Various factors involved in sample preparation, calibration, and techniques used for analyzing diffraction data are described. The article also presents application examples and possible future developments in neutron diffraction.

Ultrasonic inspection is a family of nondestructive methods in which beams of high-frequency mechanical waves are introduced into materials, using transducers, for the detection and characterization of both surface and subsurface anomalies and flaws in the material. This article describes the basic equipment in ultrasonic inspection systems, and lists the advantages and disadvantages of these systems. It discusses the applications of ultrasonic inspection and also the general characteristics of ultrasonic waves in terms of wave propagation, longitudinal waves, transverse waves, surface waves, and lamb waves. The article reviews the major variables in ultrasonic inspection, including frequency, acoustic impedance, angle of incidence, and beam intensity. It discusses the attenuation of ultrasonic beams and provides information on the pulse-echo and transmission methods for implementing ultrasonic inspection.

This article provides an overview of the characteristics of Rayleigh waves plus methods for generation and detection of waves, including using piezoelectric transducers or noncontact techniques such as lasers, electromagnetic acoustic transducers, or air-coupled ultrasonics. It reviews the methods for using Rayleigh waves for defect detection and materials characterization, alongside nonlinear ultrasonic inspection and surface acoustic wave (SAW) microscopy. The article concludes with information on the standards that use Rayleigh waves for nondestructive evaluation (NDE) of different structures.

This article describes the fundamental aspects of three nondestructive evaluation (NDE) methods of solid-state welds in terms of operation principles. These methods are radiography, ultrasound, and eddy current methods. The article provides examples of these NDE techniques performed on various types of flaws resulting from solid-state welding processes.

A number of nondestructive evaluation (NDE) methods, such as radiography, ultrasound, and eddy current, are available to detect flaws in solid materials. This article describes the fundamental aspects of these NDE methods in terms of operation principles. It presents some examples of the methods performed on various types of flaws resulting from solid-state welding processes.

This article describes the test techniques that are available for monitoring crack initiation and crack growth and for obtaining information on fatigue damage in test specimens. These techniques include optical methods, the compliance method, electric potential measurement, and gel electrode imaging methods. The article discusses the magnetic techniques that are primarily used as inspection techniques for detecting fatigue cracks in structural components. It details the principles and operation procedures of the liquid penetrant methods, positron annihilation techniques, acoustic emission techniques, ultrasonic methods, eddy current techniques, infrared techniques, exoelectron methods, and gamma radiography. The article explains the microscopy methods used to determine fatigue crack initiation and propagation. These include electron microscopy, scanning tunneling microscopy, atomic force microscopy, and scanning acoustic microscopy. The article also reviews the X-ray diffraction technique used for determining the compositional changes, strain changes, and residual stress evaluation during the fatigue process.

This article discusses the central aspect of anisotropy modeling, namely, texture measurement and analysis. It provides an overview of the methods available for characterizing crystallographic preferred orientation, or texture, in polycrystalline materials. These methods include pole figure measurement and electron backscatter diffraction (EBSD). The article describes the process considerations for pole figure measurement, including X-ray diffraction, neutron diffraction, stereographic projection, equal area projection, graphing pole figures, typical textures, and orientation distribution. It also deals with the limitations and challenges associated with the EBSD, and applications of the diffraction.

This article is a brief account of low-energy ion-scattering spectroscopy (LEIS) for determining the atomic structure of solid surfaces. It begins with a description of the general principles of LEIS. This is followed by a section providing information on the equipment used for LEIS. Various steps involved in the sample preparation, calibration, and data analysis are then discussed. The article concludes with a section on the applications and interpretation of LEIS in material analysis, including discussion on surface structural analysis, layer-by-layer (Frank-van der Merwe) growth, and low-energy atom-scattering spectroscopy.

This article considers the two primary methods used for ultrasonic inspection: pulse-echo and the transmission methods. Pulse-echo inspection can be accomplished with longitudinal, shear, surface (Rayleigh), or Lamb (plate) waves using a diverse range of transducers. The article discusses the principles of each of these inspection methods. It describes the applications and the basic data formats for single-element transducer-based systems, including A-scans, B-scans, and C-scans. The article provides information on electronic equipment used for ultrasonic inspection. It also describes how specific material conditions produce and modify A-scan indications. The article provides information on the controls and their functions for the display unit of the electronic equipment. It describes the techniques used for the identification and characterization of flaws, namely, surface (Rayleigh) wave and ultrasonic polar scan techniques.

This article lists the system parameters of the friction welding process and describes the four categories of monitoring and control of the manufacturing process. It discusses the monitoring methods of a rotary friction welded sample, for determining in-process quality of ferrous alloys, and dissimilar metals using acoustic emission. The article reviews the feasibility of detecting the presence of ferrite during microstructural evolution of friction welding of three austenitic stainless steels: 310, 304, and 255. It also explains the in-process quality control of friction welding.

This article focuses on failure analyses of aircraft components from a metallurgical and materials engineering standpoint, which considers the interdependence of processing, structure, properties, and performance of materials. It discusses methodologies for conducting aircraft investigations and inspections and emphasizes cases where metallurgical or materials contributions were causal to an accident event. The article highlights how the failure of a component or system can affect the associated systems and the overall aircraft. The case studies in this article provide examples of aircraft component and system-level failures that resulted from various factors, including operational stresses, environmental effects, improper maintenance/inspection/repair, construction and installation issues, manufacturing issues, and inadequate design.

Ultrasonic inspection is a nondestructive method in which beams of high-frequency acoustic energy are introduced into a material to detect surface and subsurface flaws, to measure the thickness of the material, and to measure the distance to a flaw. This article provides a detailed account of ultrasonic flaw detectors, including ultrasonic transducers and types of search units and couplants. The article describes pulse-echo and transmission inspection methods and data interpretation. The general characteristics of ultrasonic waves and the factors influencing ultrasonic inspection are also addressed. The article concludes with a review of the advantages and disadvantages of ultrasonic inspection compared with other methods applications of the technique.