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thermoset
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Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0009080
EISBN: 978-1-62708-177-1
... Abstract This article describes the dispersed-phase toughening of thermoset matrices by the development of multiphase-structure thermosetting matrices using rubber and/or thermoplastic materials. It discusses two main methods for manufacturing prepregs, namely, single-pass impregnation...
Abstract
This article describes the dispersed-phase toughening of thermoset matrices by the development of multiphase-structure thermosetting matrices using rubber and/or thermoplastic materials. It discusses two main methods for manufacturing prepregs, namely, single-pass impregnation and double-pass impregnation. The article illustrates reflected-light optical microscopy techniques to evaluate the morphology of thermoplastic materials for determining the material quality and correlating key microstructural features with material performance.
Book Chapter
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 November 1995
DOI: 10.31399/asm.hb.emde.a0003010
EISBN: 978-1-62708-200-6
... Abstract A thermosetting resin, or thermoset, is a synthetic organic polymer that cures to a solid, infusible mass by forming a three-dimensional network of covalent chemical bonds. Significant applications include construction and thermoset engineering plastics. This article discusses...
Abstract
A thermosetting resin, or thermoset, is a synthetic organic polymer that cures to a solid, infusible mass by forming a three-dimensional network of covalent chemical bonds. Significant applications include construction and thermoset engineering plastics. This article discusses the general and family characteristics of thermosetting resin families, including allyls, aminos (urea formaldehyde and melamine formaldehyde), cyanates, epoxies, polybenzimidazoles, unsaturated polyesters, thermoset polyimides, phenolics, and vinyl esters. It also explains processing methods, including curing and curing agents. The article provides descriptions of commercial product forms and the wide array of applications of thermosetting resins. It also tabulates the performance properties (mechanical, thermal, electrical and chemical resistance) of some families of unfilled or unreinforced thermosetting resins and reinforced or filled grades.
Series: ASM Handbook
Volume: 11B
Publisher: ASM International
Published: 15 May 2022
DOI: 10.31399/asm.hb.v11B.a0006924
EISBN: 978-1-62708-395-9
... to vitrification T cure Cure temperature, a process parameter T g Glass transition temperature, a material property T g0 T g for uncured thermoset with degree of conversion α = 0 gel T g T g for thermoset with degree of conversion α gel T g∞ T g for fully cured...
Abstract
This article discusses the most common thermal analysis methods for thermosetting resins. These include differential scanning calorimetry, thermomechanical analysis, thermogravimetric analysis, and dynamic mechanical analysis. The article also discusses the characterization of uncured thermosetting resins as well as the curing process. Then, the techniques to characterize the physical properties of cured thermosets and composites are presented. Several examples of stress-strain curves are shown for thermosets and thermoplastic polymers.
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Published: 01 January 2005
Fig. 2 Thermoset elastomers are long-chain polymers connected by cross links represented by circled Xs.
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Published: 01 December 2004
Fig. 8 Residual curing agent particles in a thermoset-matrix glass fiber composite. Reflected-light phase contrast, 40× objective
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in Thin Section Preparation and Transmitted Light Microscopy for Fiber-Reinforced Composites[1]
> Metallography and Microstructures
Published: 01 December 2004
Fig. 11 Micrographs of a thermoset-matrix carbon fiber composite material comparing the use of two different ramp rates in the cure cycle. (a) 2.8 °C/min (5 °F/min). Transmitted light, phase contrast, 20× objective. (b) 0.56 °C/min (1 °F/min). Transmitted light, phase contrast, 20× objective
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Published: 01 December 2004
Fig. 12 Fracture morphology in a particle interlayer-toughened thermoset-matrix composite. (a) Strain birefringence in the interlayer particles. Transmitted polarized light, 20× objective. (b) Some of the particles are found to bridge the formed cracks, and some particles are torn. Transmitted
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Published: 01 December 2004
Fig. 13 Fiber-matrix interfacial failure in an interlayer-toughened thermoset-matrix composite. Transmitted polarized light, full wave plate, 20× objective
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Published: 01 November 1995
Fig. 35 Percent elongation versus temperature for thermoset polyester resin and resin-matrix composites
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Published: 01 November 1995
Fig. 36 Ultimate tensile strength versus temperature for thermoset polyester resin and resin-matrix composites. Ranges are due to property differences among compression, transfer, and injection molding processes.
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Published: 01 November 1995
Fig. 37 Ultimate shear strength versus temperature for thermoset polyester-matrix composites
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Published: 01 November 1995
Fig. 38 Dielectric constant versus temperature for thermoset polyester resin and resin-matrix composites
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Published: 01 November 1995
Fig. 39 Elastic tensile modulus versus temperature for thermoset polyester resin and resin-matrix composites
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Published: 01 November 1995
Fig. 40 Ultimate compressive strength versus temperature for thermoset polyester resin and resin-matrix composites
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Published: 01 November 1995
Fig. 41 Dissipation factor versus temperature for thermoset polyester resin and resin-matrix composites
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Published: 01 November 1995
Fig. 42 Thermal conductivity versus temperature for thermoset polyester resin and resin-matrix composites. Source: Ref 8
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Published: 01 November 1995
Fig. 43 Coefficient of thermal expansion versus temperature for thermoset polyester resin and resin-matrix composites. 10 −6 /K × 5 9 = μin./in. × °F
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Published: 01 November 1995
Fig. 44 Dielectric strength versus temperature for thermoset polyester resin and resin-matrix composites
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