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thermogravimetric analysis
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Book Chapter
Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006673
EISBN: 978-1-62708-213-6
... Abstract Thermogravimetric analysis (TGA) is a thermal analysis technique that measures the amount and rate of change in the weight of a material as a function of temperature or time in a controlled atmosphere. This article provides a detailed account of the concepts of TGA, covering...
Abstract
Thermogravimetric analysis (TGA) is a thermal analysis technique that measures the amount and rate of change in the weight of a material as a function of temperature or time in a controlled atmosphere. This article provides a detailed account of the concepts of TGA, covering the various criteria to be considered for specimen preparation and calibration of TGAs. The use of thermogravimetric analysis data in the assessment of failure analysis of plastics and the combined usage of TGA with other techniques to understand the changes in the sample are also covered. The article provides examples of applications and provides information on the interpretation of TGA.
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Published: 01 November 1995
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Published: 01 January 2002
Fig. 8 Thermogravimetric analysis thermogram showing the weight-loss profile for a typical plastic resin
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Published: 01 January 2002
Fig. 9 Thermogravimetric analysis thermogram representing a typical semicrystalline plastic resin
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Published: 01 January 2002
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Published: 01 January 2002
Fig. 11 Thermogravimetric analysis thermogram showing a high level of residual stress in an amorphous plastic resin
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Published: 01 January 2002
Fig. 37 Thermogravimetric analysis weight-loss profile comparison showing a reduction in the thermal stability of the discolored surface material relative to the base material
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in Analysis and Prevention of Environmental- and Corrosion-Related Failures
> Failure Analysis and Prevention
Published: 15 January 2021
Fig. 22 Thermogravimetric analysis thermogram from rubber strands of failed bungee cord sample indicating ~20% rubber and ~80% filler
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in Analysis and Prevention of Environmental- and Corrosion-Related Failures
> Failure Analysis and Prevention
Published: 15 January 2021
Fig. 23 Thermogravimetric analysis thermogram from rubber strands of competitors’ bungee cord sample indicating ~80% rubber and ~20% filler
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Published: 15 May 2022
Fig. 33 Relative thermal stability of polymers by thermogravimetric analysis (TGA); 10 mg (0.15 gr) at 5 °C/min (9 °F/min), in nitrogen. HDPE, high-density polyethylene; PMMA, polymethyl methacrylate; PTFE, polytetrafluoroethylene; PVC, polyvinyl chloride
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Published: 15 May 2022
Fig. 34 Thermogravimetric analysis (TGA) of silica- and carbon-filled polytetrafluoroethylene (PTFE); 10 mg (0.15 gr) at 5 °C/min (9 °F/min). Source: Ref 25
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Published: 15 May 2022
Fig. 35 Thermogravimetric analysis (TGA) of polyvinyl chloride (PVC), 21.41 mg (0.33 gr), 20 °C/min (36 °F/min) to 950 °C (1740 °F), in nitrogen
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Published: 15 May 2022
Fig. 36 Thermogravimetric analysis-Fourier transform infrared spectroscopy (TGA-FTIR) of polyvinyl chloride (PVC)
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Published: 15 May 2022
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Published: 15 May 2022
Fig. 12 Thermogravimetric analysis of encapsulating materials, 20 to 30 mg (0.3 to 0.5 gr), 10 °C/min (18 °F/min), air at 40 mL/min. Courtesy of Motorola Semiconductor Products Division
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Published: 15 May 2022
Fig. 13 Relative thermal stability of polymers by thermogravimetric analysis; 10 mg (0.15 gr) at 5 °C/min (9 °F/min) in nitrogen. PVC, polyvinyl chloride; PMMA, polymethylmethacrylate; HDPE, high-density polyethylene; PTFE, polytetrafluoroethylene; PI, polyimide
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Published: 15 May 2022
Fig. 14 Thermogravimetric analysis of silica and carbon-filled polytetrafluoroethylene (PTFE); 10 mg (0.15 gr) at 5 °C/min (9 °F/min). Source: Ref 53
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Published: 15 May 2022
Fig. 15 Thermogravimetric analysis tracing of postcured Ethacure 300/6-FDA (hexafluoropropane dianhydride) at 10 °C/min (18 °F/min) in nitrogen
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Published: 15 May 2022
Fig. 16 Thermogravimetric analysis tracing of postcured Ethacure 300/PMDA (pyromellitic dianhydride) at 10 °C/min (18 °F/min) in nitrogen
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in Physical, Chemical, and Thermal Analysis of Thermoplastic Resins
> Characterization and Failure Analysis of Plastics
Published: 15 May 2022
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