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Book Chapter
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 December 1998
DOI: 10.31399/asm.hb.mhde2.a0003239
EISBN: 978-1-62708-199-3
... devices and thermal devices. The response of the photon-effect devices depends on the wavelength of the received radiation; therefore, the output signal depends on the wavelength of the infrared signal. Thermal detectors respond only to the heating caused by the incoming radiation, and the output signal...
Abstract
Thermal inspection comprises all methods in which heat-sensing devices or substances are used to detect irregular temperatures. Inspection of workpieces can be used to detect flaws and undesirable distribution of heat during service. Though there are several methods of thermal inspection and many types of temperature-measuring devices and substances, this article focuses only on thermography, which is the mapping of isotherms, or contours of equal temperature, over a test surface, and on thermometry, which is the measurement of temperature. Thermography techniques can be classified as contact thermographic methods using cholesteric liquid crystals, thermally quenched phosphors, and heat-sensitive paints, and noncontact techniques using hand-held infrared scanners, high-resolution infrared imaging systems, and thermal wave interferometer systems. Contact thermometric inspection devices include bolometers, thermocouples, thermopiles, and meltable substances, whereas radiometers and pyrometers come under the noncontact category.
Series: ASM Handbook
Volume: 17
Publisher: ASM International
Published: 01 August 2018
DOI: 10.31399/asm.hb.v17.a0006451
EISBN: 978-1-62708-190-0
.... It then describes infrared detectors, such as quantum detectors and thermal/nonquantum detectors, for thermoelastic stress analysis. The article discusses the theoretical aspects for producing thermoelastic stress analysis data and the applications amenable to thermoelastic stress analysis. It concludes...
Abstract
Thermoelastic stress analysis (TSA) an increasingly popular infrared (IR)-based technique for measuring stress on the surface of a part subjected to time-varying loads. This article begins by providing a theoretical and historical background of thermoelastic stress analysis. It then describes infrared detectors, such as quantum detectors and thermal/nonquantum detectors, for thermoelastic stress analysis. The article discusses the theoretical aspects for producing thermoelastic stress analysis data and the applications amenable to thermoelastic stress analysis. It concludes with information on the qualitative applications of thermoelastic stress analysis.
Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006659
EISBN: 978-1-62708-213-6
.... Common GC detectors are the thermal conductivity cell detector, flame ionization detector, electron capture detector, sulfur chemiluminescence detector, and nitrogen-phosphorus detector. gas chromatography detectors gas chromatography Overview CHROMATOGRAPHY is about separating (often...
Abstract
This article is dedicated to gas chromatography (GC), covering the chromatographic method and primary components of a modern GC apparatus. The components include the carrier gas cylinder, flow controller and pressure regulator, sample inlet and injection port, column oven, and detector. Common GC detectors are the thermal conductivity cell detector, flame ionization detector, electron capture detector, sulfur chemiluminescence detector, and nitrogen-phosphorus detector.
Series: ASM Handbook
Volume: 4C
Publisher: ASM International
Published: 09 June 2014
DOI: 10.31399/asm.hb.v04c.a0005853
EISBN: 978-1-62708-167-2
.... This is the advantage of an IR thermometer: it can measure temperatures as low as –50 °C (–50 °F), and it can work 24 hours a day without a break. To measure IR energy requires a detector. Infrared thermometers use two basic types of detectors: thermal or quantum. A thermal detector is actually heated or cooled...
Abstract
This article provides an overview of the basic theory of infrared (IR), including emissivity and E slope. It explains how the IR thermometer works, and provides guidance on choosing a thermometer, in particular, deciding between a two-color and a single-wavelength thermometer and installing and maintaining them. The article discusses typical applications of induction heating, and describes how the IR thermometer controls the temperature. While the majority of the article discusses spot thermometers, thermal imagers, which are fast and are used for both research and control of the induction process, are also addressed.
Series: ASM Handbook Archive
Volume: 10
Publisher: ASM International
Published: 01 January 1986
DOI: 10.31399/asm.hb.v10.a0001746
EISBN: 978-1-62708-178-8
... compounds formed in the combustion zone. The article provides information on infrared and thermal-conductive detectors, which are used for the detection of CO2 and SO2. Finally, it addresses the requirements of a sample to undergo total and selective combustion, and presents examples showing...
Abstract
High-temperature combustion is primarily used to determine carbon and sulfur contained in a variety of materials. This article illustrates the principle of combustion and focuses on the characteristics of accelerators. It provides information on the process of separating oxide compounds formed in the combustion zone. The article provides information on infrared and thermal-conductive detectors, which are used for the detection of CO2 and SO2. Finally, it addresses the requirements of a sample to undergo total and selective combustion, and presents examples showing the applications of high-temperature combustion. .
Series: ASM Handbook
Volume: 24
Publisher: ASM International
Published: 15 June 2020
DOI: 10.31399/asm.hb.v24.a0006564
EISBN: 978-1-62708-290-7
... to the nature of the thermal phenomena. These include the wavelength range, sensitivity, frame rate, and integration time. The sensitivity of a thermal detector is rated by its noise-equivalent temperature difference (NETD). This metric is the temperature difference between the target and the sensor...
Abstract
This article covers in-line process monitoring of the metal additive manufacturing (AM) methods of laser and electron beam (e-beam) powder-bed fusion (PBF) and directed-energy deposition (DED). It focuses on methods that monitor the component directly throughout the build process. This article is organized by the type of AM process and by the physics of the monitoring method. The discussion covers two types of monitoring possible with the PBF process: monitoring the area of the powder bed and component and monitoring the melt pool created by the laser or e-beam. Methods for layer monitoring include optical and thermal methods that monitor light reflected or emitted in the visible and infrared wavelengths, respectively. Monitoring methods for laser directed-energy deposition (DED) discussed are those that measure the size and shape of the melt pool, the temperature of the melt pool, and the plasma generated by the laser as it interacts with the molten metal.
Book Chapter
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 December 1998
DOI: 10.31399/asm.hb.mhde2.a0003229
EISBN: 978-1-62708-199-3
... through acoustic method and bubble testing. The article gives a short note on types of leak detectors, sulfur hexafluoride detectors and mass-spectrometer. It tabulates the pressure and vacuum system leak-testing methods and discusses the application of gas detectors in leak testing. acoustic method...
Abstract
Leak testing is used to determine the rate at which a liquid or gas penetrates from inside a component or assembly to the outside, or vice versa. This article discusses the type of leaks, namely real leaks, and virtual leaks. It describes the leak testing of fluid systems at pressure through acoustic method and bubble testing. The article gives a short note on types of leak detectors, sulfur hexafluoride detectors and mass-spectrometer. It tabulates the pressure and vacuum system leak-testing methods and discusses the application of gas detectors in leak testing.
Image
Published: 01 January 1986
, sample holding chamber; 12, electrode (impulse) furnace; 13, dust filter; 14, heated rare earth copper oxide; 15, flow control; 16, infrared detector/readout; 17, thermal-conductive detector/readout
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Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006642
EISBN: 978-1-62708-213-6
... of the target isotope (dimensionless); m x is the mass of the analyte element (grams); M a is the molar mass of the analyte element (g · mol −1 ); Γ is the gamma-ray abundance (dimensionless); ε is the full-energy photopeak efficiency of the detector (dimensionless); Φ th is the thermal neutron fluence...
Abstract
This article provides a detailed account of the concepts and applications of neutron activation analysis (NAA), covering the basic principles and neutron reactions of NAA as well as calibration methods used for NAA. The discussion also covers the factors pertinent to analytical sensitivity achievable with NAA, common neutron sources, sample-handling technique, and automated systems of NAA. The categories of NAA covered are instrumental neutron activation analysis, epithermal neutron activation analysis, radiochemical neutron activation analysis, 14 MeV fast neutron activation analysis, delayed neutron activation analysis, and prompt gamma activation analysis.
Series: ASM Handbook Archive
Volume: 10
Publisher: ASM International
Published: 01 January 1986
DOI: 10.31399/asm.hb.v10.a0001747
EISBN: 978-1-62708-178-8
... copper oxide; 13, Mg(ClO 4 ) 2 desiccant; 14, silica gel column; 15, thermal conductive detector/readout; 16, flow rotameter Fig. 5 Insert gas fusion system for detecting nitrogen and oxygen. 1, Helium supply; 2, two-stage pressure regulator; 3, NaOH-impregnated clay; 4, Mg(ClO 4 ) 2...
Abstract
Inert gas fusion is a method of determining the quantitative content of gases in ferrous and nonferrous materials where gases, such as hydrogen, nitrogen, and oxygen, are physically and chemically adsorbed by the materials and later removed and swept by from the fusion area by an inert carrier gas. This article describes the operating principles and sample selection of inert gas fusion. It explains the mechanisms involved in the introduction of fusion gas, separation and detection of fusion gas by thermal-conductive and infrared detection methods. Additionally, the article explains the methods used for analyzing trace amounts of nitrogen, oxygen, and hydrogen in the carrier mediums, providing examples that aid in solving several problems.
Series: ASM Handbook
Volume: 6
Publisher: ASM International
Published: 01 January 1993
DOI: 10.31399/asm.hb.v06.a0001398
EISBN: 978-1-62708-173-3
... in terms of thermal mass, emissivity, contamination, presence of internal thermal barriers, and heat-sinking efficiency, an infrared (IR) detector was added to create an “intelligent” laser soldering system. This system enables the precise control of heat input to the joint, because the IR “eye...
Abstract
Laser soldering uses a well-focused, highly controlled beam to deliver energy to a desired location for a precisely measured length of time. This article focuses on two types of laser soldering operations, namely, blind laser soldering and intelligent laser soldering. It discusses the function of the blind laser soldering and provides a brief description on key attributes of the blind laser soldering, including repeatability, speed, quality, safety, and flexibility. The article explores the function of the intelligent laser soldering and concludes with a section on key attributes of the intelligent laser soldering. The key attributes of the intelligent laser soldering include repeatability, speed, quality, safety, cost, and flexibility.
Image
Published: 01 January 1994
Fig. 8 Schematic diagram of laser-flash method for thermal diffusivity measurement. T m , maximum temperature measured by the liquid nitrogen-cooled infrared detector
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Series: ASM Handbook
Volume: 4B
Publisher: ASM International
Published: 30 September 2014
DOI: 10.31399/asm.hb.v04b.a0005925
EISBN: 978-1-62708-166-5
... control systems, including contact sensors, noncontact sensors, controllers, energy-flow regulators, measurement instruments, and set-point programmers. Common contact sensors include temperature scales, thermocouples, and resistance temperature detectors, whereas optical pyrometers and on-line radiation...
Abstract
Temperature control in heat treating is of paramount importance in maintaining the quality and achieving the desired metallurgical results. This article provides a detailed account of the factors affecting temperature control in heat treating furnaces, with information on temperature control systems, including contact sensors, noncontact sensors, controllers, energy-flow regulators, measurement instruments, and set-point programmers. Common contact sensors include temperature scales, thermocouples, and resistance temperature detectors, whereas optical pyrometers and on-line radiation thermometers fall under the noncontact type. The article describes two types of instrumentation used in heat treating: field test instruments for temperature-uniformity surveys and system-accuracy tests; and controlling, monitoring, and recording instruments for digital instrumentation.
Series: ASM Handbook Archive
Volume: 10
Publisher: ASM International
Published: 01 January 1986
DOI: 10.31399/asm.hb.v10.a0001748
EISBN: 978-1-62708-178-8
... may range as high as 10 or 11 MeV, necessitating use of a detector having reasonably good efficiency at such energies. In PGAA at a reactor the counting arrangement can be such that the sample is placed in the reactor thermal column, with the emitted γ-rays being observed through a collimator...
Abstract
Neutron activation analysis (NAA) is a highly sensitive and accurate method of assaying bulk materials for trace levels of many elements. This article provides a detailed account on several types of NAA, namely, nondestructive and radiochemical thermal neutron activation, delayed neutron counting, epithermal and 14-MeV fast neutron activation, and prompt gamma activation analysis. It also includes application examples, explaining where and how each method is used and the types of elements on which they are effective.
Image
Published: 01 December 2004
the cathode ray tube beam is deflected proportionally to the detector signal) allows control of the depth of thermal etching. 4000×. (d) Decay of nickel fibers in a silver matrix of an electrical conduction material produced by the drawing of bundled, coated rods. During annealing at 900 °C (1650 °F) for 5 h
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Image
Published: 01 January 1986
) furnace; 11, dust filter; 12, heated rare earth copper oxide; 13, Mg(ClO 4 ) 2 desiccant; 14, silica gel column; 15, thermal conductive detector/readout; 16, flow rotameter
More
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 December 1998
DOI: 10.31399/asm.hb.mhde2.a0003250
EISBN: 978-1-62708-199-3
... a series of traps, absorbers, and converters to separate them and remove interfering elements. They are then quantified using detectors based on either thermal conductivity or absorption of infrared light. In the case of inert gas fusion for oxygen, nitrogen, or hydrogen, the sample is heated by either...
Abstract
The overall chemical composition of metals and alloys is most commonly determined by X-ray fluorescence (XRF) and optical emission spectroscopy (OES), and combustion and inert gas fusion analysis. This article provides information on the capabilities, uses, detection threshold and precision methods, and sample requirements. The amount of material that needs to be sampled, operating principles, and limitations of the stated methods are also discussed.
Series: ASM Handbook Archive
Volume: 10
Publisher: ASM International
Published: 01 January 1986
DOI: 10.31399/asm.hb.v10.a0001749
EISBN: 978-1-62708-178-8
... and beta-particle emission, positron emission, and gamma and x-ray emission. It compares and contrasts measurement techniques based on various detectors, namely, charged-particle detectors, photon detectors, counting and recording instruments, and radioactive decay spectrometers. It also addresses sample...
Abstract
Radioanalysis is an analytical technique that uses energy emitted by radioactive isotopes to measure the concentration of related elements in test samples. This article begins with a discussion on the principles of radioactive decay and various forms of emission, including alpha and beta-particle emission, positron emission, and gamma and x-ray emission. It compares and contrasts measurement techniques based on various detectors, namely, charged-particle detectors, photon detectors, counting and recording instruments, and radioactive decay spectrometers. It also addresses sample preparation, equipment and process safety, and the handling of radioactive gasses and materials. The article concludes with application examples involving the analysis of rare-earth elements and nuclear fuels.
Book: Fractography
Series: ASM Handbook
Volume: 12
Publisher: ASM International
Published: 01 June 2024
DOI: 10.31399/asm.hb.v12.a0006876
EISBN: 978-1-62708-387-4
... analyses) to approximately 10,000×. This magnification range is well within the capabilities of traditional tungsten thermal-emission SEMs, so tungsten thermal-emission SEMs are commonly used in fractography studies. Instruments with alternative emission sources (LaB 6 , Schottky field-emission, or cold...
Abstract
This article presumes the reader has a basic understanding of the operation and principles of scanning electron microscopy (SEM). The emphasis of this article is specifically on the application of SEM to the study of metallic and nonmetallic fracture surfaces, where the typical objectives of SEM examination of a fracture surface may include the following: identification of characteristic fracture features to aid in identifying fracture mechanism(s); characterization of material anomalies that may have influenced the fracture; qualitative or semiquantitative chemical analysis of component material(s); and qualitative or semiquantitative analysis of deposits or corrosion products on or near fracture surfaces.
Series: ASM Handbook
Volume: 18
Publisher: ASM International
Published: 31 December 2017
DOI: 10.31399/asm.hb.v18.a0006432
EISBN: 978-1-62708-192-4
... or inductive sensors, mainly use a change in length or distance as an indicator for wear. Such measurements give a good feedback about changes occurring in wear behavior, but exact quantification is limited by thermal, plastic, or elastic elongations, as well as by the presence of a lubricant or particles...
Abstract
Radionuclide methods for wear measurement are used to measure wear continuously throughout a tribological experiment at a resolution of nanometers or micrograms per hour. This article presents an overview of radionuclide methods for wear measurement. It discusses complementary wear measurement methods to introduce the advantages of using radioactive isotopes (RI) for wear or corrosion measurements in comparison to other methods. The article provides information on radiation safety regulations and approaches to minimize external radiation exposure. It describes neutron activation, thin layer or surface layer activation, and ultrathin layer or recoil activation that are used to create radioactive isotopes in the samples to be tested. The article reviews the two common types of wear measurement setup configurations: the direct method and the indirect method. It concludes with a discussion on the practical application of wear measurement using radioactive isotopes.
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