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sulfamic acid
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Series: ASM Handbook
Volume: 13C
Publisher: ASM International
Published: 01 January 2006
DOI: 10.31399/asm.hb.v13c.a0004143
EISBN: 978-1-62708-184-9
... material incompatibilities in a table. The article summarizes the uses of chemical cleaning solutions, including hydrochloric acid, phosphoric acid, and sulfamic acid, as well as the additives used to neutralize their impact on corrosion. It discusses the chemical cleaning procedures, including selection...
Abstract
This article describes the eight chemical cleaning methods, namely, circulation, fill and soak, cascade, foam, vapor-phase organic, steam-injected, on-line chemical, and mechanical cleaning. It presents information on deposit types, solvents used to remove them, and construction material incompatibilities in a table. The article summarizes the uses of chemical cleaning solutions, including hydrochloric acid, phosphoric acid, and sulfamic acid, as well as the additives used to neutralize their impact on corrosion. It discusses the chemical cleaning procedures, including selection of cleaning method and solvent, documentation of cleaning, and corrosion monitoring in chemical cleaning.
Image
Published: 01 December 2004
Fig. 36 Twinned austenitic grain structure of solution-annealed, wrought Hadfield manganese steel (Fe-1.12%C-12.7%Mn-0.31%Si) tint etched with Beraha's sulfamic acid reagent (No. 3) (100 mL water, 3 g potassium metabisulfite, and 2 g sulfamic acid) and viewed with polarized light plus
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Image
Published: 01 February 2024
Fig. 39 Carburized gear teeth made with 8620 alloy steel (Fe-0.2%C-0.8%Mn-0.25%Si-0.55%Ni-0.5%Cr-0.2%Mo) with a gradation of carbon and microstructure revealed by tint etching with Beraha’s sulfamic acid reagent (100 mL water, 3 g potassium metabisulfite, 2 g sulfamic acid, and 0.7 g ammonium
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Image
Published: 31 August 2017
in the type B specimen in Fig. 15 , because this specimen contained more carbon. (a) As-cast. 2% nital etch. Original magnification: 100×. (b) As-cast. 2% nital etch. Original magnification: 500×. (c) As-cast. Beraha’s sulfamic acid etch No. 1. Original magnification: 100×. (d) As-cast. Beraha’s sulfamic
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Book: Surface Engineering
Series: ASM Handbook
Volume: 5
Publisher: ASM International
Published: 01 January 1994
DOI: 10.31399/asm.hb.v05.a0001251
EISBN: 978-1-62708-170-2
... Abstract Lead has been deposited from a variety of electrolytes, including fluoborates, fluosilicates, sulfamates, and methane sulfonic acid baths. This article provides a discussion on these electrolytic baths and includes information on the process sequence, equipment requirements...
Abstract
Lead has been deposited from a variety of electrolytes, including fluoborates, fluosilicates, sulfamates, and methane sulfonic acid baths. This article provides a discussion on these electrolytic baths and includes information on the process sequence, equipment requirements, and applications of lead plating.
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in Metallography and Microstructures of Stainless Steels and Maraging Steels[1]
> Metallography and Microstructures
Published: 01 December 2004
Fig. 46 Grain-boundary carbides in annealed 420 stainless steel tint etched with Beraha's sulfamic acid etch (No. 4)
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Image
Published: 01 December 2004
Fig. 37 Twinned austenitic grain structure of wrought, annealed Fe-39%Ni tint etched with Beraha's sulfamic acid solution (No. 3) and viewed with polarized light plus sensitive tint. The magnification bar is 100 μm long.
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Image
Published: 01 December 2004
Fig. 35 Microstructure of the core of a carburized, heat treated 4118 alloy steel (Fe-0.2%C-0.8%Mn-0.5%Cr-0.12%Mo) tint etched with Beraha's sulfamic acid reagent (No. 1) and viewed with polarized light plus sensitive tint, revealing a lath martensite structure. The magnification bar is 20 μm
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Image
Published: 01 December 2004
Fig. 18 Grain-boundary carbide networks in type 420 martensitic stainless steel (Fe-0.35%C-0.4%Mn-13%Cr) with two different etchants. (a) Vilella's reagent. (b) Beraha's sulfamic acid tint etch. Heat treatment: 1038 °C (1900 °F). Air quench: 177 °C (350 °F) temper. 500×
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Image
Published: 01 December 2004
Fig. 38 Microstructure at the surface of a decarburized, hardened specimen of type 420 martensitic stainless steel (Fe-0.35%C-13%Cr) tint etched with Beraha's sulfamic acid reagent (No. 4) and viewed with polarized light plus sensitive tint. Note the free ferrite (arrows) at the surface
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Image
Published: 31 August 2017
. Original magnification: 500×. (d) Beraha’s sulfamic acid etch No. 1. Original magnification: 200×
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in Metallography and Microstructures of Stainless Steels and Maraging Steels[1]
> Metallography and Microstructures
Published: 01 December 2004
Image
Published: 01 February 2024
Fig. 11 Ledeburite in a white cast iron (Fe-4.0%C-0.3%Si-0.16%Mn-0.91%Cr). Etched with Beraha’s sulfamic acid reagent (100 mL water, 3 g K 2 S 2 O 5 , and 2 g NH 2 SO 3 H). Taken in polarized light with sensitive tint. Original magnification: 500×. Courtesy of George F. Vander Voort, Vander
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Image
Published: 31 August 2017
magnification: 50×. (b) 2% nital etched. Original magnification: 100×. (c) 2% nital etched. Original magnification: 500×. (d) Beraha’s sulfamic acid etch No. 1. Original magnification: 500×
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in Metallography and Microstructures of Stainless Steels and Maraging Steels[1]
> Metallography and Microstructures
Published: 01 December 2004
retained austenite with a few martensite plates (b) to nearly all retained austenite (c). Note that the carbide content also decreases and the grain size increases. Revealed using Beraha's sulfamic acid No. 4 tint etch
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Book: Surface Engineering
Series: ASM Handbook
Volume: 5
Publisher: ASM International
Published: 01 January 1994
DOI: 10.31399/asm.hb.v05.a0001249
EISBN: 978-1-62708-170-2
... relation. Indium sulfamate plating bath Table 4 Indium sulfamate plating bath Constituent or parameter Value or condition Indium sulfamate 105.36 g/L (14 oz/gal) Sodium sulfamate 150 g/L (20 oz/gal) Sulfamic acid 26.4 g/L (3.5 oz/gal) Sodium chloride 45.84 g/L (6 oz/gal...
Abstract
This article focuses on the electrodeposition of indium and its alloys, such as indium-antimony, indium-gallium, and indium-bismuth, in nonaqueous indium plating baths. It also provides information on the stripping of indium plate from plated components and presents an overview of the specifications, standards, and hazards of indium plating.
Image
Published: 01 December 2004
etched with Beraha's sulfamic acid etch (No. 1) (aqueous 3% K 2 S 2 O 5 + 1% H 2 NSO 3 H) and viewed with polarized light plus sensitive tint. The normal structure is ferrite and pearlite, but bainite (arrows) is observed in the segregated regions. The segregated regions are easier to detect
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Book: Surface Engineering
Series: ASM Handbook
Volume: 5
Publisher: ASM International
Published: 01 January 1994
DOI: 10.31399/asm.hb.v05.a0001254
EISBN: 978-1-62708-170-2
... in Table 1 . Ruthenium electroplating solutions Table 1 Ruthenium electroplating solutions Constituent or condition Amount or value General-purpose solution Ruthenium (as sulfamate or nitrosyl sulfamate), g/L (oz/gal) 5.3 (0.7) Sulfamic acid, g/L (oz/gal) 8 (1.1) Anodes...
Abstract
The electroplating of platinum-group metals (PGMs) from aqueous electrolytes for engineering applications is limited principally to palladium and, to a lesser extent, to platinum, rhodium, and thin layers of ruthenium. This article provides a discussion on the plating operations of these PGMs along with the types of anodes used in the process.
Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0003752
EISBN: 978-1-62708-177-1
.... The magnification bar is 100 μm long. Beraha's etchants, based on sulfamic acid, a weak organic acid, have not been used much, although they are quite useful, reliable, and easy to employ ( Ref 63 ). The sulfamic-acid-based reagents ( Table 3 ) are applicable to iron, low-carbon...
Abstract
This article is a compilation of color etchants that have been developed for a limited number of metals and alloys. It describes the optical methods for producing color, such as polarized light and differential interference contrast, with illustrations. The article discusses film formation and interference techniques such as anodizing, chemical etching, and tint etching. It provides a description of reagents that deposit sulfide films and molybdate films. The article concludes with a discussion on the thermal and vapor deposition methods to produce color.
Book Chapter
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 December 1998
DOI: 10.31399/asm.hb.mhde2.a0003215
EISBN: 978-1-62708-199-3
...) Nickel sulfate, NiSO 4 ·6H 2 O 225–400 … 300 Nickel sulfamate, Ni(SO 3 NH 2 ) 2 … 300–450 … Nickel chloride, NiCl 2 ·6H 2 O 30–60 0–30 35 Boric acid, H 3 BO 3 30–45 30–45 45 Operating conditions Temperature, °C 44–66 32–60 54 Agitation Air or mechanical Air...
Abstract
Copper can be electrodeposited from numerous electrolytes. Cyanide and pyrophosphate alkalines, along with sulfate and fluoborate acid baths, are the primary electrolytes used in copper plating. This article provides information on the chemical composition, plating baths, and operating conditions of electrodeposition processes for chromium plating, nickel plating, iron plating, cadmium plating, zinc plating, indium plating, lead plating, tin plating, silver plating, gold plating, brass plating, bronze plating, tin-lead plating, zinc-iron plating, and zinc-nickel plating. The article also discusses selective plating, electroforming, and other processes and where they are typically used.
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