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spectrographic analysis
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Series: ASM Handbook
Volume: 4A
Publisher: ASM International
Published: 01 August 2013
DOI: 10.31399/asm.hb.v04a.a0005798
EISBN: 978-1-62708-165-8
... provides information on the microscopic method used to detect smaller variations in carbon content, and reviews consecutive cuts analysis and spectrographic analysis that are used to accurately evaluate the carbon concentration profile of carburized parts. It describes procedures of and precautions...
Abstract
This article presents the different hardness test methods used to measure the effectiveness of surface carbon control in carburized parts of steel. Common test methods include Rockwell hardness measurements, superficial Rockwell 15N testing, and microhardness testing. The article provides information on the microscopic method used to detect smaller variations in carbon content, and reviews consecutive cuts analysis and spectrographic analysis that are used to accurately evaluate the carbon concentration profile of carburized parts. It describes procedures of and precautions to be undertaken during shim stock analysis, which is used to measure the atmosphere carbon potential. The article includes a discussion on the electromagnetic nondestructive tests that are used to evaluate the case depth of case-hardened parts.
Series: ASM Handbook
Volume: 4A
Publisher: ASM International
Published: 01 August 2013
DOI: 10.31399/asm.hb.v04a.a0005795
EISBN: 978-1-62708-165-8
... methods of measuring case depth in steels, including chemical methods such as the combustion analysis and spectrographic analysis, microhardness test method, macroscopic and microscopic visual methods, and nondestructive methods. It contains a table that provides approximate equivalent hardness numbers...
Abstract
Case depth is the normal distance from the surface of the steel to the start of the core. Measurement of case depth is highly sensitive to the type of case hardening, original steel composition, quenching condition, and even to the testing method. This article describes the various methods of measuring case depth in steels, including chemical methods such as the combustion analysis and spectrographic analysis, microhardness test method, macroscopic and microscopic visual methods, and nondestructive methods. It contains a table that provides approximate equivalent hardness numbers for steel.
Book Chapter
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 December 1998
DOI: 10.31399/asm.hb.mhde2.a0003199
EISBN: 978-1-62708-199-3
... of guidelines for safety procedures that are common to all industrial heat treating furnace installations. carbon potential measurement electromagnetic testing furnace atmosphere control devices furnace safety procedures heat treating processed steel parts spectrographic analysis temperature...
Abstract
Control of temperature and furnace atmospheres has become increasingly critical to successful heat treating. Temperature instrumentation and control systems used in heat treating include temperature sensors, controllers, final control elements, measurement instruments, and set-point programmers. This article describes these items and discusses the classifications and control of furnace atmospheres. The article also describes the surface carbon control devices available for the wide variety of furnace atmospheres and evaluation of carbon control. Finally, the article provides a set of guidelines for safety procedures that are common to all industrial heat treating furnace installations.
Series: ASM Handbook
Volume: 1A
Publisher: ASM International
Published: 31 August 2017
DOI: 10.31399/asm.hb.v01a.a0006318
EISBN: 978-1-62708-179-5
... elements in cast irons. Although spectrometers used for elemental analysis of minor elements continue to be improved, the detection limit and the quantitative working range for elemental analysis must be considered when reporting and acting on spectrographic trace element levels in cast irons. Also...
Abstract
During the melting and solidification of cast irons, certain trace (minor) elements may unintentionally accumulate to an extent that they have a detrimental effect on the microstructure of castings. This article discusses the residual elements, trace elements, and tramp elements in cast irons. Elements that influence the matrix structure of cast irons are commonly classified as ferrite-promoting elements or pearlite-promoting elements. The article describes the effects of minor elements on microstructure and properties of cast irons. It discusses the use of a combination of tools to control the effects of minor elements on the structure and properties of cast irons. The article concludes with information on allowable levels of trace and tramp elements in cast irons.
Series: ASM Handbook Archive
Volume: 10
Publisher: ASM International
Published: 01 January 1986
DOI: 10.31399/asm.hb.v10.a0001739
EISBN: 978-1-62708-178-8
... Wet chemical analysis excludes all spectrographic techniques that measure the emission of electromagnetic energy from the sample. Similarly excluded from this article are all other fundamentally instrumental analytical techniques, although extensive chemical pretreatment may be required for their use...
Abstract
This article provides information on basic chemical equilibria, wet analytical chemistry, and the appropriateness of classical wet methods. It focuses on nonoxidizing acids and oxidizing acids. The article includes information on the qualitative methods used to identify materials by wet chemical reaction. Gravimetry, in which a chemical species is weighed; titrimetry, which involves volume measurement of a liquid reactant; and a host of separation techniques, which require diverse forms of laboratory manipulation, are discussed. The article briefly describes the partitioning of oxidation states as well as those applications in surface studies and rapid material identification in which chemical techniques have proved useful.
Book: Casting
Series: ASM Handbook
Volume: 15
Publisher: ASM International
Published: 01 December 2008
DOI: 10.31399/asm.hb.v15.a0005340
EISBN: 978-1-62708-187-0
... techniques is provided below. Chemical Analysis Elemental composition of an impurity is determined either wet or via spectrographic analysis in unfiltered and filtered samples ( Ref 1 ). An efficiency parameter (η) is then used to describe the filter performance ( Ref 1 ): (Eq 1) η = 100...
Abstract
Several qualitative, semiquantitative, and quantitative tests are available to estimate and control metal cleanliness, particularly inclusion concentration of aluminum alloys. This article provides a description of a few of the metal cleanliness assessment techniques, such as chemical analysis, pressure filter tests, electric resistivity tests, reduced-pressure test, and ultrasonic technique. Detection methods based on the certain principles and the types of impurities in chemical analysis are discussed.
Series: ASM Handbook
Volume: 2
Publisher: ASM International
Published: 01 January 1990
DOI: 10.31399/asm.hb.v02.a0001090
EISBN: 978-1-62708-162-7
...-bearing impurities; therefore, maximum limits of 10 to 20 ppm are usually placed on HCl, OH, CH 2 , and CH 3 contents. Analytical and Test Methods The analysis of ores for germanium is usually done with an emission spectrograph but can be done in the field with the phenylfluorone method ( Ref 41...
Abstract
Germanium is a semiconducting metalloid element found in Group IV A. Germanium is used in the field of electronics, infrared optics, and in the fields of gamma ray spectroscopy, catalysis, and fiber optics. This article discusses the sources, manufacturing, and processing of germanium, and focuses on the chemical properties of various germanium compounds, including germanium halides, germanates, germanides, germanes, inorganic, and organogermanium compounds. It also tabulates the physical, thermal, electronic, and optical properties of germanium, and explains the economical aspects and specifications of germanium. The article describes the analytical and test methods of germanium, including gravimetric method, titrimetric method, and spectral method. It provides a short note on toxicology, and concludes with the uses of germanium in different fields.
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 November 1995
DOI: 10.31399/asm.hb.emde.a0006515
EISBN: 978-1-62708-200-6
... quantitative spectrographic analysis mV millivolt r radius vector in a plane normal to the axis MV megavolt PEK polyetherketone MVT moisture vapor transmission PES, PESV polyether sulfone r particle radius; radius of curvature; rate of MW molecular weight PET polyethylene terephthalate n growth exponent PETG...
Book: Composites
Series: ASM Handbook
Volume: 21
Publisher: ASM International
Published: 01 January 2001
DOI: 10.31399/asm.hb.v21.a0003437
EISBN: 978-1-62708-195-5
... be chemically analyzed by appropriate methods. Composites containing silicon carbide cannot be analyzed by spectrographic methods due to the silicon signal coming from the reinforcement. The most reliable method is the ICP method. Since the ICP method involves dissolving the sample, a volume fraction analysis...
Abstract
This article describes the characterization techniques, mechanical tests, and nondestructive evaluation methods that are commonly used for metal-matrix composites. It also tabulates typical methods of particle size and size distribution measurement, as well as mechanical test specifications for aluminum-matrix composites.
Series: ASM Handbook Archive
Volume: 10
Publisher: ASM International
Published: 01 January 1986
DOI: 10.31399/asm.hb.v10.a0001747
EISBN: 978-1-62708-178-8
... studies, which indicated a high aluminum oxide (Al 2 O 3 ) content. Oxygen analysis by inert gas fusion indicated the total oxygen content to be correct, and a spectrographic analysis showed the aluminum content to be correct. A solid specimen of the material was prepared and analyzed by a controlled...
Abstract
Inert gas fusion is a method of determining the quantitative content of gases in ferrous and nonferrous materials where gases, such as hydrogen, nitrogen, and oxygen, are physically and chemically adsorbed by the materials and later removed and swept by from the fusion area by an inert carrier gas. This article describes the operating principles and sample selection of inert gas fusion. It explains the mechanisms involved in the introduction of fusion gas, separation and detection of fusion gas by thermal-conductive and infrared detection methods. Additionally, the article explains the methods used for analyzing trace amounts of nitrogen, oxygen, and hydrogen in the carrier mediums, providing examples that aid in solving several problems.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0001822
EISBN: 978-1-62708-180-1
... Railroads) with evidence of copper penetration. The axle from the Macon, Dublin & Savannah Railroad had gross cracking with visible copper-colored material in the cracks. Spectrographic analysis of samples from both axles containing copper penetration revealed that the major constituents were copper...
Abstract
This article provides a background of friction-bearing failures due to overheating. The failures of locomotive axles caused by overheated traction-motor support bearings are discussed. The article also describes liquid-metal embrittlement (LME) in steel. It examines the results of various axle studies, with illustrations and concludes with information on the simulation of the LME mechanism.
Book Chapter
Series: ASM Handbook Archive
Volume: 10
Publisher: ASM International
Published: 01 January 1986
DOI: 10.31399/asm.hb.v10.a0005692
EISBN: 978-1-62708-178-8
... the time interval between the is used in spectrographic analysis to cal- portant information about atomic arrange- absorption and re-emission of light is very culate the relative intensity of a radiant ments and bonding. Either synchrotron short. Contrast with phosphorescence. source from the density...
Series: ASM Handbook
Volume: 1A
Publisher: ASM International
Published: 31 August 2017
DOI: 10.31399/asm.hb.v01a.a0006299
EISBN: 978-1-62708-179-5
... (also called cooling curve analysis) can provide more complete insight into the dynamic changes occurring upon melting and melt treatment of cast iron than other methods, such as fractured test samples (e.g., the wedge test) and spectrographic chemical analysis. Initially, TA was used for the rapid...
Abstract
Thermal analysis is used to analyze solidification processes by recording the temperature as a function of time during cooling or heating of a metal or alloy to or from a temperature above its melting point. This article describes the use of cooling curves for analyzing a solidification process, such as the solidification temperature, structure analysis, fraction of phases and heat of fusion with focus on solidification of cast iron, and the use of cooling curves to control and adjust the casting conditions. It discusses deviations from equilibrium that occur due to kinetic effects during solidification. The article also illustrates the evaluation of fraction of solid formed during the precipitation of austenite from heat balance.
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 December 1998
DOI: 10.31399/asm.hb.mhde2.a0003228
EISBN: 978-1-62708-199-3
... their identifying marks, some means of sorting mixed lots is necessary. The best method of identifying such items is by quantitative chemical analysis. However, chemical or spectrographic analyses require extensive, time-consuming procedures and expensive equipment that may not be fully utilized. Also, a complete...
Abstract
This article reviews nondestructive testing (NDT) and inspection techniques, namely liquid penetrant, magnetic particle, ultrasonics, X-ray, eddy current, visual and radiography that are commonly used to detect and evaluate flaws or leaks in an engineering system. This article compares the merits and limitations of these techniques and describes the various uses of NDT, including leak detection, metrology, structure or microstructure characterization, stress-strain response determination, and rapid identification of metals and alloys.
Book Chapter
Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006748
EISBN: 978-1-62708-213-6
... in which data signals originate. tron microscope (SEM) usually directed at in spectrographic analysis to calculate the the same point where the sample can be relative intensity of a radiant source from expansivity. The thermal strain of a material, located. Also known as cross-beam or dual- the density...
Series: ASM Handbook
Volume: 4B
Publisher: ASM International
Published: 30 September 2014
DOI: 10.31399/asm.hb.v04b.a0005935
EISBN: 978-1-62708-166-5
... the acoustic signal (spectrograph) obtained during quenching in different media. Point 1 for pure water; point 2 for 5% solution. Other curves for 10 and 15% solutions (two types each, type A and B). (a) 150 Hz frequency. (b) 16,000 Hz frequency The analysis of the acoustic spectrum obtained during...
Abstract
This article focuses on the heat removal stages involved in quenching, and on the experimental setup used for measuring temperature and detecting sound signals with the help of illustrations and curves. The quenching process generates acoustic signals, which are the consequences of the phase transformation of steel and of the boiling process at the interface during the cooling process. The sound-pressure signal is captured by the hydrophone through sound-emission measurements that occur during steel quenching in different quenching media. The analysis of the results offers an interesting approach to evaluation and, more importantly, to monitoring, controlling, and optimizing the entire quenching process.
Series: ASM Handbook
Volume: 8
Publisher: ASM International
Published: 01 January 2000
DOI: 10.31399/asm.hb.v08.a0009214
EISBN: 978-1-62708-176-4
... in one block. For example, suppose that a block is one day, but that the time required for each test is so long that all experimental treatments cannot be run in one day. The limitation might also be due to a lack of space, such as in spectrographic analysis in which a block may be one photographic plate...
Abstract
Planning of experiments does not consist merely of identifying a few key parameters and then selecting a specific plan. Selection of the proper experimental plan depends on the purpose of the experiment, physical restrictions on the taking of measurements, and other restrictions imposed by time, economic considerations, and materials and personnel availability. This article presents recommendations that should be followed in outlining the methods of conducting and analyzing an experiment to ensure successful results. It discusses restricted type of experiments, in which the experimenter varies the parameters, or factors, under study and then observes the effects of this action. These include factorial experiments, blocked factorial experiments, and fractional factorial experiments. The article describes the estimation of experimental errors and provides information on randomized designs and block designs. It also presents the methods for determining optimum conditions or levels.
Series: ASM Handbook Archive
Volume: 10
Publisher: ASM International
Published: 01 January 1986
DOI: 10.31399/asm.hb.v10.a0001728
EISBN: 978-1-62708-178-8
... Abstract This article discusses the general principles, optical systems, and emission sources of optical emission spectroscopy for elemental analysis. Changes in the energy of the valence or outer shell electrons result in the atomic lines used in emission spectroscopy. Each possible...
Abstract
This article discusses the general principles, optical systems, and emission sources of optical emission spectroscopy for elemental analysis. Changes in the energy of the valence or outer shell electrons result in the atomic lines used in emission spectroscopy. Each possible combination of electron configurations produces a spectroscopic term that describes the state of the atom. Atomic emission is analytically useful only to the extent that the emission from one atomic species can be measured and its intensity recorded independent of emission from other sources. Emission sources are often designed to minimize molecular emission. Each of the four types of emission sources; arcs, high-voltage sparks, glow discharges, and flames; has a set of physical characteristics with accompanying analytical assets and liabilities. The article also discusses the applications of each type of emission source.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003573
EISBN: 978-1-62708-180-1
... and is commonly computed by classical design or limit analysis. This article discusses the common aspects of failure by distortion with suitable examples. Analysis of a distortion failure often must be thorough and rigorous to determine the root cause of failure and to specify proper corrective action...
Abstract
Distortion failure occurs when a structure or component is deformed so that it can no longer support the load it was intended to carry. Every structure has a load limit beyond which it is considered unsafe or unreliable. Estimation of load limits is an important aspect of design and is commonly computed by classical design or limit analysis. This article discusses the common aspects of failure by distortion with suitable examples. Analysis of a distortion failure often must be thorough and rigorous to determine the root cause of failure and to specify proper corrective action. The article summarizes the general process of distortion failure analysis. It also discusses three types of distortion failures that provide useful insights into the problems of analyzing unusual mechanisms of distortion. These include elastic distortion, ratcheting, and inelastic cyclic buckling.
Book Chapter
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006797
EISBN: 978-1-62708-295-2
... Abstract Distortion often is observed in the analysis of other types of failures, and consideration of the distortion can be an important part of the analysis. This article first considers that true distortion occurs when it was unexpected and in which the distortion is associated...
Abstract
Distortion often is observed in the analysis of other types of failures, and consideration of the distortion can be an important part of the analysis. This article first considers that true distortion occurs when it was unexpected and in which the distortion is associated with a functional failure. Then, a more general consideration of distortion in failure analysis is introduced. Several common aspects of failure by distortion are discussed and suitable examples of distortion failures are presented for illustration. The article provides information on methods to compute load limits, errors in the specification of the material, and faulty process and their corrective measures to meet specifications. It discusses the general process of material failure analysis and special types of distortion and deformation failure.
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