Search Results for specimen handling

This article describes some of the common elemental composition analysis methods and explains the concept of referee and economy test methods in failure analysis. It discusses different types of microchemical analyses, including backscattered electron imaging, energy-dispersive spectrometry, and wavelength-dispersive spectrometry. The article concludes with information on specimen handling.

Many metal failures involve fracture, and fractography is an essential activity in many, if not most, failure analysis (FA) investigations. This article introduces and illustrates the role of fractography in an FA investigation. Basic guidelines are briefly presented for investigating a failure and how fractography helps the FA investigator determine evidence. Examples are given throughout this article on how the examination of fracture surfaces discerns various sources of crack initiation and mechanisms of crack growth. The procedures for analyzing fractures also include several steps and techniques that involve photographic documentation, proper specimen handling, and visual or microscopic examination. The article also briefly describes the use of metallography in fracture analysis along with case studies as illustrative examples of various fracture mechanisms and modes.

This article discusses the importance of the care and handling of fracture specimens and what to look for during the preliminary field or laboratory observation and collection, the preservation of specimens, and the cleaning and preparation of fracture specimens for additional analyses. The preservation of nonmetallic specimens, medical devices, oversized components, light alloys, nondestructively tested components, and materials that are part of legal proceedings is addressed.

Mounting of the specimen is often desirable or necessary for handling and metallographic polishing after the specimen is cut into an appropriate size. This article illustrates the different mechanical clamps used in mounting small specimens. It provides useful information on compression molded mounts, which are molded with thermoplastic and thermosetting resins. The article reviews several resins and their key factors, which help in the selection of the most appropriate mounting method and resin. It also discusses the characteristics of plastic mounting materials. The article provides information on the molds and resins used for castable mounts, vacuum treatment of mounts, special mount arrangements, and mount marking and storage.

This article describes the methods and equipments involved in the preparation of specimens for examination by light optical microscopy, scanning electron microscopy, electron microprobe analysis for microindentation hardness testing, and for quantification of microstructural parameters, either manually or by the use of image analyzers. Preparation of metallographic specimens generally requires five major operations: sectioning, mounting, grinding, chemical polishing, and etching. The article provides information on the principles of technique selection in mechanical polishing, and describes the procedures, advantages, and disadvantages of electrolytic and chemical polishing. It also provides a detailed account of procedures, precautions, and composition for preparation and handling of etchants.

Fracture surfaces are fragile and subject to mechanical and environmental damage that can destroy microstructural features. This article discusses the importance of care and handling of fractures and the factors that need to be considered during the preliminary visual examination. It describes the procedures for sectioning a fracture and opening secondary cracks as well as the effect of nondestructive inspection on subsequent evaluation. The article provides information on the most common techniques for cleaning fracture surfaces. These techniques are dry air blast cleaning, replica stripping, organic-solvent cleaning, water-base detergent cleaning, cathodic cleaning, and chemical-etch cleaning.

This article is an atlas of fractographs that helps in understanding the causes and mechanisms of fracture of low-carbon steels and in identifying and interpreting the morphology of fracture surfaces. The fractographs illustrate the following: the intergranular fracture, bending impact fracture, brittle fracture, tensile-test fracture, transgranular fracture, cleavage fracture, delayed fracture, corrosion fatigue, inclusion morphology, fatigue crack propagation, and in-service fatigue fracture of various automotive components. These components include tie rod adjusting sleeves, automotive bolts, hydraulic jack shafts, crank handle collars, boiler tubes, drive shafts, bicycle pedal axles, lift-truck hydraulic-piston rods, and steel springs.

This article provides information on the liquid lithium systems that are exposed to liquid metal. It discusses the forms in which liquid-metal corrosion is manifested. The influence of several key factors on the corrosion of metals and alloys by liquid-metal systems or liquid-vapor metal coolants is described. Some information on safety precautions for handling liquid metals, operating circulating systems, dealing with fire and spillage, and cleaning contaminated components, are also provided.

This article describes the four major conditions that can cause beryllium to corrode in air. These include beryllium carbide particles exposed at the surface; surface contaminated with halide, sulfate, or nitrate ions; surface contaminated with other electrolyte fluids; and atmosphere that contains halide, sulfate, or nitrate ions. The article provides information on the behavior of beryllium under the combined effects of high-purity water environment, stress and chemical environment, and high-temperature environment. The compositions of the structural grades for intentionally controlled elements and major impurities are tabulated. The article discusses the in-process problems and procedures that are common but avoidable when processing beryllium and aluminum-beryllium composites. It also describes the types of coatings used on beryllium and aluminum-beryllium. These include chemical conversion coatings, anodized coatings, plated coatings, organic coatings, and plasma-sprayed coatings.

This article briefly reviews the analysis methods for spalling of striking tools with emphasis on field tests conducted by A.H. Burn and on the laboratory tests of H.O. McIntire and G.K. Manning and of J.W. Lodge. It focuses on the metallography and fractography of spalling. The macrostructure and microstructure of spall cavities are described, along with some aspects of the numerous specifications for striking/struck tools. The article also describes the availability of spall-resistant metals and the safety aspects of striking/struck tools in railway applications.

Fracture toughness is an empirical material property that is determined by one or more of a number of standard fracture toughness test methods. This article describes the fracture toughness test methods in a chronological outline, beginning with the methods that use the linear-elastic parameter. After this, the methods that use the nonlinear parameters are discussed. The article reviews some of the work in progress to update the standard test methods, namely, common fracture toughness test method and transition fracture toughness test method. Finally, an overview of fracture toughness testing for ceramic and polymer materials is provided.

Metallographic contrasting methods include various electrochemical, optical, and physical etching techniques, which in turn are enhanced by the formation of a thin transparent film on the specimen surface. This article primarily discusses etching in conjunction with light microscopy and describes several methods for film formation, namely, heat tinting, color etching, anodizing, potentiostatic etching, vapor deposition, and film deposition by sputtering. It provides information on the general procedures and precautions for etchants and reagents used in metallographic microetching, macroetching, electropolishing, chemical polishing, and other similar operations.

This article discusses the various heat treating processes, namely, solid-solution hardening, solution treating, solution aging and dispersion hardening, for low-melting-point alloys such as lead alloys, tin-rich alloys, and zinc alloys. Heat treating of tin-rich alloys has been practiced for bearing alloys, pewterware, and organ pipe alloys. The article reviews the principles underlying these applications.

This article illustrates how objective experiments and comparisons can be used to develop surface preparation procedures for metallographic examination of structural features of metals. These procedures are classified as machining, grinding and abrasion, or polishing. The article describes the abrasion artifacts in austenitic steels, zinc, ferritic steels, and pearlitic steels, and other effects of abrasion damages, including flatness of abraded surfaces and embedding of abrasive. Different polishing damages, such as degradation of etching contrast and scratch traces, are reviewed. The article explains the final-polishing processes such as skid polishing, vibratory polishing methods, etch-attack and electromechanical polishing, and polishing with special abrasives. An overview of special polishing techniques for unusual materials such as very hard and very soft materials is provided. The article concludes with a discussion on semiautomatic preparation procedures, providing information on procedures based on the use of diamond abrasives charged in a carrier paste and in a suspension.

This article focuses on the corrosion-wear synergism in aqueous slurry and grinding environments. It describes the effects of environmental factors on corrosive wear and provides information on the impact and three-body abrasive-corrosive wear. The article also discusses the various means for combating corrosive wear, namely, materials selection, surface treatments, and handling-environment modifications.

This article describes the safety precautions required for using laboratory equipment. It reviews the various personal protective equipment specified on the Material Safety Data Sheets (MSDS) for laboratory chemicals and products. The article provides information on the storage and handling of etchants, solvents, acids, bases, and other chemicals. It describes the safety precautions and procedures for handling concentrated and dilute hydrofluoric acid. The article concludes with a discussion on the precautions to be followed in the event of spills and cleanup.

Fractography is the systematic study of fractures and fracture surfaces. It is a useful tool in failure analysis and provides a means for correlating the influence of microstructure on the fracture mode of a given material. This article discusses the preservation, preparation, and photography of fractured parts and surfaces, and describes some of the more common fractographic features revealed by light microscopy, including tensile-fracture surface marks in unnotched specimens, fatigue marks, and structural discontinuities within the metal. The article also explains how to interpret fracture information contained in optical and scanning-electron microscope fractographs.

Hadfield's austenitic manganese steel exhibits high toughness and ductility with high work-hardening capacity and, usually, good wear resistance. Beginning with an overview of the as-cast properties and composition of these class of steels, this article discusses the heat treatment methods used to improve their wear resistance, and the changes in the mechanical properties after heat treatment. Manganese steels are unequaled in their ability to work harden, exceeding even the metastable austenitic stainless steels in this feature.

Low-temperature carburization hardens the surface of austenitic stainless steels through the diffusion of interstitial carbon without the formation of carbides. This article provides an overview on austenitic stainless steels and low-temperature carburization. It reviews the competing technologies and commercial application of low-temperature carburization. The article discusses several processing parameters, including activation of the surface, proper surface preparation, selection and condition of the alloy to be carburized, treatment temperature, and carburizing atmosphere for successful low-temperature carburization of austenitic stainless steels and other chromium-containing alloys. It describes the performance properties of the low-temperature carburized layer: fatigue resistance, wear resistance, erosion resistance, and corrosion resistance.