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Image
Scanning electron microscope image revealing a region of a fractured powder...
Available to PurchasePublished: 01 June 2024
Fig. 6 Scanning electron microscope image revealing a region of a fractured powder metal component. Dimpled rupture at interparticle sinter bonds is much less prevalent than that observed in Fig. 5 . The dearth of ruptured sinter bonds in this area corresponds to the location of a green crack
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Image
Scanning electron microscope image revealing numerous pools of dimpled rupt...
Available to PurchasePublished: 01 June 2024
Fig. 5 Scanning electron microscope image revealing numerous pools of dimpled rupture, indicated by arrows. These areas represent overload at sinter bonds between metal powder particles. Original magnification: 1000×
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Image
Microstructures of (a) resin-bonded and (b) sintered brake friction materia...
Available to PurchasePublished: 31 December 2017
Image
Published: 30 September 2015
Book Chapter
Joining Powder Metallurgy Steel Components
Available to PurchaseBook: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006108
EISBN: 978-1-62708-175-7
... site The joining processes most often successful on lower-density parts are diffusion welding, sinter bonding, adhesive joining, and brazing. Parts at intermediate density levels (6.6 to 6.9 g/cm 3 ) can be joined using a wide assortment of processes. However, those that minimize the volume...
Abstract
This article characterizes the physical differences between powder metallurgy (PM) and wrought or cast materials, as they apply to joining. It discusses acceptable joining procedures and techniques, including welding and brazing and solid-state methods. Information on the weldability of various PM materials is presented. The article also describes the effects of porosity on several important properties that affect the welding characteristics.
Book Chapter
Diffusion Bonding
Available to PurchaseSeries: ASM Handbook
Volume: 6A
Publisher: ASM International
Published: 31 October 2011
DOI: 10.31399/asm.hb.v06a.a0005612
EISBN: 978-1-62708-174-0
... on this process in which ceramic powder compacts are simultaneously sintered and bonded are also discussed. ceramic powder compacts ceramic-ceramic joints ceramic-metal joints diffusion bonding dissimilar metals liquid-phase process nonferrous alloys sinter-bond process solid-phase process steels...
Abstract
This article describes the solid-phase and liquid-phase processes involved in diffusion bonding of metals. It provides a detailed discussion on the diffusion bonding of steels and their alloys, nonferrous alloys, and dissimilar metals. Ceramic-ceramic diffusion welding and a variation on this process in which ceramic powder compacts are simultaneously sintered and bonded are also discussed.
Book Chapter
Sintering of Stainless Steels
Available to PurchaseBook: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006118
EISBN: 978-1-62708-175-7
... interparticle bonding, and (c) preventing reoxidation and nitride formation during cooling from sintering temperature. PM stainless steels got their start with “conventional” sintering, i.e. sintering in continuous mesh belt furnaces that utilize high-temperature-grade stainless steel mesh belts, stainless...
Abstract
This article describes the sintering behavior of austenitic, ferritic, and martensitic stainless steels. It presents different sintering schedules that are selected by Metal Powder Industries Federation (MPIF). The article provides information on the equipment and atmospheres used for sintering and the steps involved in the process. It discusses the factors that influence the dimensional changes in sintering, namely, powder-related, compaction-related, and sintering-related factors.
Book Chapter
Densification and Sintering of Ceramics
Available to PurchaseSeries: ASM Desk Editions
Publisher: ASM International
Published: 01 November 1995
DOI: 10.31399/asm.hb.emde.a0003054
EISBN: 978-1-62708-200-6
... Abstract Sintering provides the interparticle bonding that generates the attractive forces needed to hold together the otherwise loose ceramic powder mass. It also improves hardness, strength, transparency, toughness, electrical conductivity, thermal expansion, magnetic saturation, corrosion...
Abstract
Sintering provides the interparticle bonding that generates the attractive forces needed to hold together the otherwise loose ceramic powder mass. It also improves hardness, strength, transparency, toughness, electrical conductivity, thermal expansion, magnetic saturation, corrosion resistance, and other properties. This article discusses the fundamentals of sintering and its effects on pore structures and particle density. It addresses some of the more common sintering methods, including solid-state, liquid-phase, and gas pressure sintering, and presents alternative processes such as reaction sintering and self-propagating, high-temperature synthesis. It also describes several pressure densification methods, including hot isostatic pressing, gas pressure sintering, molten particle deposition, and sol-gel processing. The article concludes with a section on grain growth that discusses the underlying mechanisms and kinetics and the relationship between grain growth and densification.
Book
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.9781627081757
EISBN: 978-1-62708-175-7
Book Chapter
Ceramic-Matrix Composites
Available to PurchaseSeries: ASM Desk Editions
Publisher: ASM International
Published: 01 November 1995
DOI: 10.31399/asm.hb.emde.a0003063
EISBN: 978-1-62708-200-6
..., discontinuously reinforced composites and continuous-fiber-reinforced composites. Processing methods include cold pressing, sintering, hot pressing, reaction bonding, melt infiltration, directed metal oxidation, sol-gel and polymer pyrolysis, self-propagating high-temperature synthesis and joining. A table...
Abstract
Ceramic-matrix composites (CMCs) are being developed for a number of high-temperature and high-performance applications in industrial, aerospace, and energy conservation sectors. This article focuses on processing, fabrication, testing, and characterization methods of CMCs, namely, discontinuously reinforced composites and continuous-fiber-reinforced composites. Processing methods include cold pressing, sintering, hot pressing, reaction bonding, melt infiltration, directed metal oxidation, sol-gel and polymer pyrolysis, self-propagating high-temperature synthesis and joining. A table summarizes the properties of various ceramic reinforcements and industrial applications of these composites.
Image
Effect of sintering time on iron powder and graphite mix (pressed to 6.1 g/...
Available to Purchase
in Metallography and Microstructures of Powder Metallurgy Alloys
> Metallography and Microstructures
Published: 01 December 2004
Fig. 34 Effect of sintering time on iron powder and graphite mix (pressed to 6.1 g/cm 3 ) with a sintering temperature of 1120 °C (2050 °F). (a) Sintered for 5 min, which resulted in all-pearlite structure (combined content at 0.70%) and some bonding of particles. (b) Sintered for 120 min
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Variation in fracture surface with sintering time for iron powder pressed t...
Available to Purchase
in Metallography and Microstructures of Powder Metallurgy Alloys
> Metallography and Microstructures
Published: 01 December 2004
Fig. 23 Variation in fracture surface with sintering time for iron powder pressed to 6.6 g/cm 3 and sintered in hot zone at 1120 °C (2050 °F) with dissociated ammonia for (a) 3 min and (b) 10 min. Image (a) from 3 min sinter shows where a bond has broken (arrows D). Arrows S outline
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Effect of sintering (in dissociated ammonia for 30 min) at different temper...
Available to Purchase
in Metallography and Microstructures of Powder Metallurgy Alloys
> Metallography and Microstructures
Published: 01 December 2004
°C (1950 °F) forms many bonds between particles, but with numerous particles boundaries and angular pores. (c) Sintering temperature at 1120 °C (2050 °F) results in more numerous and extensive bonds with some grain growth and spheroidization of pores. (d) Sintering at 1175 °C (2150 °F) results
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Book Chapter
Superabrasives and Ultrahard Tool Materials
Available to PurchaseSeries: ASM Handbook
Volume: 2
Publisher: ASM International
Published: 01 January 1990
DOI: 10.31399/asm.hb.v02.a0001106
EISBN: 978-1-62708-162-7
... . The focus of this article is further restricted to synthesized diamond and CBN. The latter does not occur in nature, and the former commands 90% of the industrial diamond market. These materials will be treated in terms of the forms in common use: diamond or CBN grains (looser or bonded) and sintered...
Abstract
Synthetic diamond and cubic boron nitride are among a class of superhard materials from the boron-carbon-nitrogen-silicon family of elements. This article focuses on the two materials, the forms in which they are produced, and their respective properties. Synthetic diamond and cubic boron nitride compounds are available in the form of grit and sintered polycrystalline blanks of various size, shape, and composition. The article explains how superabrasive grains made from these materials can be used in lapping, polishing, and grinding applications, and how diamond and boron nitride blanks can be mounted to suitable substrates to form ultrahard cutting edges and tools.
Book Chapter
Secondary Operations and Quality Control for Refractory Metal Powders
Available to PurchaseBook: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006133
EISBN: 978-1-62708-175-7
... of graphite by high-temperature brazing A special extension of furnace brazing can be employed when it becomes necessary to join massive sintered WHA bodies together to form a shape impossible to sinter as a self-supporting, monolithic form. In this technique, termed sinter bonding , previously...
Abstract
Refractory metals are typically processed from powders into ingots that are subsequently swaged into round bars or rolled into plates. Secondary operations are required to fabricate more complex refractory metal components. This article discusses two such secondary operations, namely, machining and joining processes for tungsten, tungsten heavy alloys, molybdenum, tantalum, niobium, and rhenium components. It describes the various types of metal joining processes, including mechanical fastening, brazing, and welding.
Book Chapter
Pressing and Sintering of Copper Powders
Available to PurchaseBook: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006105
EISBN: 978-1-62708-175-7
... thickness. Sintering of Copper Powders The sintering process is often described as a complex high-temperature process that consolidates and strengthens loose or compacted particles into a more dense and coherent body. During sintering, powder particles form coherent bonds and densify by pore...
Abstract
Development of the properties of copper powder metallurgy parts is affected by pressing and sintering processes used in the production of components, such as contacts, carbon brushes, and friction materials. This article briefly describes the powder properties of copper and discusses the roles of lubricant and compaction dies in pressing of copper powders. It explains the structural defects that originate during the compaction process of PM parts. The article also provides information on sintering, re-pressing, and re-sintering of copper PM parts.
Book Chapter
High-Temperature Sintering of Ferrous Powder Metallurgy Components
Available to PurchaseBook: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006110
EISBN: 978-1-62708-175-7
... cycle. The breakdown of oxides and the removal of adsorbed gases cleanse the metal particle surfaces and promote the diffusion process. Particle bonding: The formation of solid bridges or necks between powder particles is the critical result of the early stages of sintering. These particle bonds...
Abstract
High-temperature sintering of ferrous components continues to be important in the powder metallurgy (PM) industry. Improvements in both production rates and properties are possible as sintering temperatures increase above 1120 deg C. This article provides an overview of the different various stages of the sintering process and the physical, chemical, and metallurgical phenomena occur within the mass of metal powder particles. It discusses the four advantages of high-temperature sintering of various ferrous PM materials: improved mechanical properties, improved physical properties, development of liquid phase, and ability to sinter active elements in alloy steels. The article also provides information on three sources of process control requirements, namely, the powder blend, green density, and sintering conditions.
Image
Progress of sintering in a loose stack of copper powder spheres, secondary ...
Available to PurchasePublished: 01 December 2004
Fig. 19 Progress of sintering in a loose stack of copper powder spheres, secondary electron images. (a) Light bonding at 600 °C (1110 °F) during heating to sintering temperature. (b) After sintering for 1 h at 1050 °C (1920 °F). Clearly visible is the formation of necks between touching
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Series: ASM Handbook
Volume: 2
Publisher: ASM International
Published: 01 January 1990
DOI: 10.31399/asm.hb.v02.a0001105
EISBN: 978-1-62708-162-7
..., pressing, slip casting, and sintering. It also discusses fundamental concepts such as chemical bonding, chemical composition, microstructure, and the development of physical and mechanical properties. boride cermets, carbide cermets, carbonitride cermets, cermets, cutting tools, oxide cermets...
Abstract
Ceramic-metal composites, or cermets, combine the heat and wear resistance of ceramics with the formability of metals, filling an application niche that includes cutting tools, brake pads, heat shields, and turbine components. This article examines a wide range of cermets, including oxide cermets, carbide and carbonitride cermets, boride cermets, and other refractory types. It describes the powder metallurgy process by which cermets are produced, examining each step from powder preparation to post treatment. It discusses forming and compacting, injection molding, extrusion, rolling, pressing, slip casting, and sintering. It also discusses fundamental concepts such as chemical bonding, chemical composition, microstructure, and the development of physical and mechanical properties.
Book Chapter
Processing of Ceramic-Matrix Composites
Available to PurchaseBook: Composites
Series: ASM Handbook Archive
Volume: 21
Publisher: ASM International
Published: 01 January 2001
DOI: 10.31399/asm.hb.v21.a0003421
EISBN: 978-1-62708-195-5
... Abstract Ceramic-matrix composites (CMCs) have ability to withstand high temperatures and have superior damage tolerance over monolithic ceramics. This article describes important processing techniques for CMCs: cold pressing, sintering, hot pressing, reaction-bonding, directed oxidation...
Abstract
Ceramic-matrix composites (CMCs) have ability to withstand high temperatures and have superior damage tolerance over monolithic ceramics. This article describes important processing techniques for CMCs: cold pressing, sintering, hot pressing, reaction-bonding, directed oxidation, in situ chemical reaction techniques, sol-gel techniques, pyrolysis, polymer infiltration, self-propagating high-temperature synthesis, and electrophoretic deposition. The advantages and disadvantages of each technique are highlighted to provide a comprehensive understanding of the achievements and challenges that remain in this area.
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