This article provides information on the microstructure of powder metal alloys and the special handling requirements of porous materials. It covers selection, sectioning, mounting, grinding, and polishing, and describes procedures, such as washing, liquid removal, and impregnation, meant to preserve pore structures and keep them open for analysis. The article compares and contrasts the microstructures of nearly 50 powder metal alloys, using them to illustrate the effect of consolidation and compaction methods as well as particle size, composition, and shape. It discusses imaging equipment and techniques and provides data on etchants and etching procedures.

The corrosion processes of metals during burial are affected by environmental pollutants, other archaeological material, geography, microorganisms in the soil, vegetation, land use, soil chemistry, soil physical properties, and the presence or absence of water and air. This article discusses the key environmental variables that affect the corrosion of buried metal artifacts. These include water (including dissolved salts and gases), sulfate-reducing bacteria, pH (acidity), and potential (oxidizing or reducing capacity). The article contains tables that list some corrosion products identified on archaeological tin and pewter, lead, iron alloys, silver alloys, and copper alloys. It also discusses the corrosion problems after excavation and the techniques followed by archaeological department for conserving metal artifacts.

This article describes the paint systems generally used to protect steel structures, steel sheet, and bridges from corrosion, and how they deter corrosion. It provides a discussion on the basic design criteria of steel structures for corrosion protection. The article also explains the differences between prepaint and postpaint, and the steps involved in prepaint processing of steel. It presents the selection guideline for paint system evaluation. The advantages of corrosion protection are also discussed.

Nonplanar microstructures form most frequently during the solidification of alloys, and play a crucial role in governing the properties of the solidified material. This article emphasizes the basic ideas, characteristic lengths, and the processing conditions required to control the columnar and equiaxed microstructures. The formation of cellular and dendritic structures in one- and two-phase structures is presented with emphasis on the effect of processing conditions and composition on the selection of microstructure and microstructure scales.

Contour roll forming is a continuous process for forming metal from sheet, strip, or coiled stock into desired shapes of uniform cross section by feeding the stock through a series of roll stations equipped with contoured rolls. This article discusses the materials, roll-forming machines, tooling, and auxiliary equipment used in contour roll forming and its process variables. Tooling used in roll forming includes forming rolls and dies for punching and cutting off the material. The article discusses the additional tooling required in tube mills to weld, size, and straighten the tubes as they are produced on the machine. It describes the roll design for tube rolling and reviews the seam welding operations of pipe and tubing. The article discusses cross-sectional tolerances, the reshaping of round tubing, and factors that affect the quality, accuracy, and surface finish.

This article provides a comprehensive discussion on die casting alloy types and casting processes used in high-pressure die casting. It presents the advantages and disadvantages of high-pressure die casting and describes the product design for the process. The article concludes with information on the metal injection process of high-pressure die casting.

Fracture surfaces are fragile and subject to mechanical and environmental damage that can destroy microstructural features. This article discusses the importance of care and handling of fractures and the factors that need to be considered during the preliminary visual examination. It describes the procedures for sectioning a fracture and opening secondary cracks as well as the effect of nondestructive inspection on subsequent evaluation. The article provides information on the most common techniques for cleaning fracture surfaces. These techniques are dry air blast cleaning, replica stripping, organic-solvent cleaning, water-base detergent cleaning, cathodic cleaning, and chemical-etch cleaning.

Stretch forming is the forming of sheet, bars, and rolled or extruded sections over a die or form block of the required shape while the workpiece is held in tension. This article discusses the applicability, advantages, and machines and accessories of stretch forming. It provides a detailed discussion on four methods of stretch forming, namely, stretch draw forming, stretch wrapping, compression forming, and radial draw forming.

This article focuses on the general methods and approaches from the perspective of a reconstruction analyst and includes discussions relevant to materials failure analysts at the incident scene. The elements of accident reconstruction are described. These have conceptual similarity with the principles for failure analysis of material incidents that are less complex than a large-scale accident. The article provides a brief review of some general concepts on the use of modeling which can be a very powerful tool for information pertaining to the reconstruction of an accident where the model can be a physical, mathematical, or logical representation of a physical system or process.

This article focuses on the specific aspects of nitinol that are of interest to medical device designers. It describes the physical metallurgy, physical properties, and tensile properties of the nitinol. The article discusses the factors influencing superelastic shape memory effects, fatigue, and corrosion in medical device design. It reviews the biocompatibility of nitinol based on corrosion behavior. The article explains the general principles, potential pitfalls, and key properties for manufacturing, heat treatment, and processing of nitinol.

This article primarily considers the problem of sampling bulk materials, including minerals, metals, environmentally important substances, and industrial raw materials and waste products. It provides useful information on sample types, sampling plan, optimizing sampling resources, practical aspects of sampling, and how to ensure the quality of sampling.

Thermal spray coatings (TSCs) are surface coatings engineered to provide wear-, erosion-, abrasion-, and corrosion-resistant coatings for original equipment manufacture and for the repair and upgrading of in-service equipment. This article presents an overview of five thermal spray processes and the specific flame and arc spray processes used to preserve large steel components and structures. It describes the TSC selection guide and an industrial process procedure guide for applying aluminum and zinc TSCs onto steel.

This article focuses on the three basic groups of flexible-die forming methods: rubber pad, fluid cell, and fluid forming. It provides information on the Guerin process, the Verson-Wheelon process, the trapped-rubber process, the Marform process, the Hydroform process, the SAAB process, and the Demarest process. The article provides a discussion on the procedures of these processes, as well as the presses and tools used. It describes the methods of hydraulic forming of thin metal parts, namely, hydraulic forming with diaphragm, hydraulic forming with gasket and pressure control, and hydrobuckling.

Radial forging is a hot- or cold-forming process that uses two or more radially moving anvils or dies to produce solid or tubular components with constant or varying cross sections along their lengths. This article focuses on the workpiece configuration, workpiece materials, machines, dies, advantages, and limitations of radial forging. It concludes with a discussion on the applications of radial forging.

This article discusses the mechanics, surface preparation and principles of metal forming operations such as drawing, bending (draw bending, compression bending, roll bending, and stretch bending), spinning, and straightening of bars, tubes, wires, rods and structural shapes. The article also discusses the machines and tools, including dies and mandrels, and lubricants used for these metal forming operations.

This article outlines the basic steps to be followed and the range of techniques available for failure analysis, namely, background data assembling, visual examination, microfractography, chemical analysis, metallographic examination, electron microscopy, electron microprobe analysis, X-ray techniques, and simulations. It also describes the steps for analyzing the data, preparing the report, preservation of evidence, and follow-up on recommendations.

This article discusses the classification, characteristics and temper designations of wrought aluminum alloys. Wrought aluminum products are available as flat-rolled products such as sheets, plates, and foils; rods, bars, and wires; tubular products such as tubes and pipes; extruded shapes; forgings; and impacts. The article provides information on product economics, design and selection, including product dimension and dimension tolerances, and design and use of wrought product capabilities. Finally, it tabulates the specifications and standards for aluminum mill products.

This article discusses the solidification of a matrix alloy in cast metal matrix composites (MMCs). It begins with a discussion on the mixing techniques in reinforcement incorporation and wettability of reinforcement. It describes the solidification processes, such as stir mixing and melt infiltration, used in the synthesis of MMCs. The article also considers the fundamentals of the process and presents a computational modeling of particle/solidification front interactions in metal-ceramic systems. The article concludes with information on nanocomposites.