Rough grinding and polishing of specimens are required to prepare fiber-reinforced composite samples for optical analysis. This article discusses the consumables, process variables, and the equipment that influence the sample preparation procedure. It describes the hand and automated grinding methods. The article summarizes the rough and final polishing steps for both hand and automated techniques. Common artifacts that may be created during grinding and polishing steps of composite samples are reviewed. These include scratches, fiber pull-out, matrix smears, streaks, erosion of different phases, and fiber and sample edge rounding and relief.

Metal is removed from the workpiece by the mechanical action of irregularly shaped abrasive grains in all grinding operations. This article discusses three primary components of grinding wheels, namely, abrasive (the cutting tool), bond (the tool holder), and porosity or air for chip clearance and/or the introduction of coolant. It describes the compositions and applications of coated abrasives and types of grinding fluids, such as petroleum-base and mineral-base cutting oils, water-soluble oils, synthetic fluids, semisynthetic fluids, and water plus additives. The article concludes with information on different types of grinding processes, namely, rough grinding, precision grinding, surface grinding, cylindrical grinding, centerless grinding, internal grinding, and tool grinding.

Microscopy is a valuable tool in materials investigations related to problem solving, failure analysis, advanced materials development, and quality control. This article describes the sample preparation techniques of composite materials. These techniques include mounting, rough grinding, and polishing. The preparation techniques of ultrathin sections are also summarized. The article explains the illumination methods used by reflected light microscopy to view a specimen. These consist of epi-bright-field illumination, epi-dark-field illumination, epi-polarized light, and epi-fluorescence. The article also provides information on transmitted light microscopy.

In all grinding operations, care must be used in the selection of wheels and abrasive belts to meet finish and tolerance requirements without damaging the workpiece. This article discusses the major aspects of the grinding wheel, including production methods, selection considerations, standard marking systems, abrasives, and bonding types. It compares bonded wheel grinding with abrasive belt grinding. The article reviews the types of grinding fluids and discusses their importance in grinding operations. It describes the specific grinding processes and provides recommendations for grinding and grinding wheels.

Abrasive finishing is a method where a large number of multipoint or random cutting edges are coupled with abrasive grains as a bond or matrix material for effective removal of material at smaller chip sizes. This article provides a broad overview of the various categories of abrasive products and materials, abrasive finishing processes, and the mechanisms of delivering the abrasives to the grinding or machining zone. Abrasive finishing processes, such as grinding, honing, superfinishing, microgrinding, polishing, buffing, and lapping, are discussed. The article presents a brief discussion on abrasive jet machining and ultrasonic machining. It concludes with a discussion on the four categories of factors that affect the abrasive finishing or machining: machine tool, work material, wheel selection, and operational.

This article focuses on the sample preparation methods for titanium honeycomb composites, boron fiber composites, and titanium/polymeric composite hybrids. These include mounting, sectioning, grinding, and polishing. The article also provides information on the sample preparation of unstaged and staged prepreg materials for optical analysis.