Rough grinding and polishing of specimens are required to prepare fiber-reinforced composite samples for optical analysis. This article discusses the consumables, process variables, and the equipment that influence the sample preparation procedure. It describes the hand and automated grinding methods. The article summarizes the rough and final polishing steps for both hand and automated techniques. Common artifacts that may be created during grinding and polishing steps of composite samples are reviewed. These include scratches, fiber pull-out, matrix smears, streaks, erosion of different phases, and fiber and sample edge rounding and relief.

Metal is removed from the workpiece by the mechanical action of irregularly shaped abrasive grains in all grinding operations. This article discusses three primary components of grinding wheels, namely, abrasive (the cutting tool), bond (the tool holder), and porosity or air for chip clearance and/or the introduction of coolant. It describes the compositions and applications of coated abrasives and types of grinding fluids, such as petroleum-base and mineral-base cutting oils, water-soluble oils, synthetic fluids, semisynthetic fluids, and water plus additives. The article concludes with information on different types of grinding processes, namely, rough grinding, precision grinding, surface grinding, cylindrical grinding, centerless grinding, internal grinding, and tool grinding.

Microscopy is a valuable tool in materials investigations related to problem solving, failure analysis, advanced materials development, and quality control. This article describes the sample preparation techniques of composite materials. These techniques include mounting, rough grinding, and polishing. The preparation techniques of ultrathin sections are also summarized. The article explains the illumination methods used by reflected light microscopy to view a specimen. These consist of epi-bright-field illumination, epi-dark-field illumination, epi-polarized light, and epi-fluorescence. The article also provides information on transmitted light microscopy.

Both surface finish and surface integrity must be defined, measured, and maintained within specified limits in the processing of any product. Surface texture is defined in terms of roughness, waviness, lay, and flaws. This article illustrates some of the designations of surface roughness and the symbols for defining lay and its direction. In addition, it describes the applications of surface integrity, typical surface integrity problems created in metal removal operations, and principal causes of surface alterations produced by machining processes. The article tabulates the effect of some machining methods on fatigue strength, and low-stress grinding procedures for steels, nickel-base high-temperature alloys, and titanium alloys.

This article reviews how process variations influence the characteristics of thermal spray coatings. It describes various specimen preparation techniques, which allow accurate microstructural analysis. These techniques include sectioning, cleaning, mounting, planar grinding, fine grinding, rough polishing, and etching. The article provides information on the problems associated with specimen preparation. It concludes with a discussion on the various methods of analysis for thermal spray coatings.

Abrasive finishing is a method where a large number of multipoint or random cutting edges are coupled with abrasive grains as a bond or matrix material for effective removal of material at smaller chip sizes. This article provides a broad overview of the various categories of abrasive products and materials, abrasive finishing processes, and the mechanisms of delivering the abrasives to the grinding or machining zone. Abrasive finishing processes, such as grinding, honing, superfinishing, microgrinding, polishing, buffing, and lapping, are discussed. The article presents a brief discussion on abrasive jet machining and ultrasonic machining. It concludes with a discussion on the four categories of factors that affect the abrasive finishing or machining: machine tool, work material, wheel selection, and operational.

In all grinding operations, care must be used in the selection of wheels and abrasive belts to meet finish and tolerance requirements without damaging the workpiece. This article discusses the major aspects of the grinding wheel, including production methods, selection considerations, standard marking systems, abrasives, and bonding types. It compares bonded wheel grinding with abrasive belt grinding. The article reviews the types of grinding fluids and discusses their importance in grinding operations. It describes the specific grinding processes and provides recommendations for grinding and grinding wheels.

This article focuses on the sample preparation methods for titanium honeycomb composites, boron fiber composites, and titanium/polymeric composite hybrids. These include mounting, sectioning, grinding, and polishing. The article also provides information on the sample preparation of unstaged and staged prepreg materials for optical analysis.

This article describes the various aspects relating to the selection and preparation of ultrathin-section specimens of fiber-reinforced polymeric composites for examination by transmitted light microscopy. It provides information on the contrast-enhancement methods used by transmitted-light microscopy and optimization of microscope conditions. Examples of composite ultrathin sections analyzed using transmitted-light microscopy contrast methods are also presented.

Mechanical finishes usually can be applied to aluminum using the same equipment used for other metals. This article describes the two types of grinding used in mechanical finishing: abrasive belt grinding and abrasive wheel grinding. It reviews the binders and fluid carriers used in buffing, and discusses satin finishing and barrel finishing. It also describes lapping and honing techniques that are of special interest in treating aluminum parts that have received hard anodic coatings. Honing recommendations for aluminum alloys are presented in a table.

Nickel-base alloys can be machined by techniques that are used for iron-base alloys. This article discusses the effects of distortion and microstructure on the machinability of nickel alloys. It tabulates the classification of nickel alloys based on machining characteristics. The article describes the machining operations performed on nickel alloys, such as turning, planing and shaping, broaching, reaming, drilling, tapping and threading, milling, sawing, and grinding. It provides information on the cutting fluids used in the machining of nickel alloys. The article also analyzes nontraditional machining methods that are suitable for shaping high-temperature, high-strength nickel alloys. These include electrochemical machining, electron beam machining, and laser beam machining.