This article describes testing and characterization methods of ceramics for chemical analysis, phase analysis, microstructural analysis, macroscopic property characterization, strength and proof testing, thermophysical property testing, and nondestructive evaluation techniques. Chemical analysis is carried out by X-ray fluorescence spectrometry, atomic absorption spectrophotometry, and plasma-emission spectrophotometry. Phase analysis is done by X-ray diffraction, spectroscopic methods, thermal analysis, and quantitative analysis. Techniques used for microstructural analysis include reflected light microscopy using polarized light, scanning electron microscopy, transmission electron microscopy, energy dispersive analysis of X-rays, and wavelength dispersive analysis of X-rays. Macroscopic property characterization involves measurement of porosity, density, and surface area. The article describes testing methods such as room and high-temperature strength test methods, proof testing, fracture toughness measurement, and hardness and wear testing. It also explains methods for determining thermal expansion, thermal conductivity, heat capacity, and emissivity of ceramics and glass and measurement of these properties as a function of temperature.

This article briefly introduces the concepts of failure analysis, including root-cause analysis (RCA), and the role of failure analysis as a general engineering tool for enhancing product quality and failure prevention. It initially provides definitions of failure on several different levels, followed by a discussion on the role of failure analysis and the appreciation of quality assurance and user expectations. Systematic analysis of equipment failures reveals physical root causes that fall into one of four fundamental categories: design, manufacturing/installation, service, and material, which are discussed in the following sections along with examples. The tools available for failure analysis are then covered. Further, the article describes the categories of mode of failure: distortion or undesired deformation, fracture, corrosion, and wear. It provides information on the processes involved in RCA and the charting methods that may be useful in RCA and ends with a description of various factors associated with failure prevention.

This article aims to identify and illustrate the types of overload failures, which are categorized as failures due to insufficient material strength and underdesign, failures due to stress concentration and material defects, and failures due to material alteration. It describes the general aspects of fracture modes and mechanisms. The article briefly reviews some mechanistic aspects of ductile and brittle crack propagation, including discussion on mixed-mode cracking. Factors associated with overload failures are discussed, and, where appropriate, preventive steps for reducing the likelihood of overload fractures are included. The article focuses primarily on the contribution of embrittlement to overload failure. The embrittling phenomena are described and differentiated by their causes, effects, and remedial methods, so that failure characteristics can be directly compared during practical failure investigation. The article describes the effects of mechanical loading on a part in service and provides information on laboratory fracture examination.

This article provides information on the general characteristics, composition, uses, applications and specifications for standard grades of ductile iron. It describes the manufacturing and metallurgical process control procedures, including testing and inspection, and heat treatment. The article also talks about the effects of composition, graphite shape, and section size on the mechanical properties of ductile iron. Tables and graphs provide helpful information on the tensile properties, compressive properties, torsional properties, damping capacity, impact properties, fracture toughness, fatigue strength, and elevated-temperature properties of ductile iron.

A sliding bearing (plain bearing) is a machine element designed to transmit loads or reaction forces to a shaft that rotates relative to the bearing. This article explains the role of wear damage mechanisms in the design and selection of bearing materials, and its relationship with bearing material properties. Sliding bearings are commonly classified by terms that describe their application; they also are classified according to material construction, as single-metal, bimetal, or trimetal sliding bearings. The article further provides detailed tabular data on the designation and composition of the following types of bearing materials: tin-base alloys, lead-base alloys, copper-base alloys, and aluminum-base alloys. It also briefly discusses the following types of bearing materials: zinc-base alloys, silver-base alloys, gray cast irons, cemented carbides, and nonmetallic bearing materials.

This article is an atlas of fractographs that helps in understanding the causes and mechanisms of fracture of AISI/SAE alloy steels (4xxx steels) and in identifying and interpreting the morphology of fracture surfaces. The fractographs illustrate the brittle fracture, ductile fracture, impact fracture, fatigue fracture surface, reversed torsional fatigue fracture, transgranular cleavage fracture, rotating bending fatigue, tension-overload fracture, torsion-overload fracture, slip band crack, crack growth and crack initiation, crack nucleation, microstructure, hydrogen embrittlement, sulfide stress-corrosion failure, stress-corrosion cracking, and hitch post shaft failure of these steels. The components considered in the article include tail-rotor drive-pinion shafts, pinion gears, outboard-motor crankshafts, bull gears, diesel engine bearing cap bolts, splined shafts, aircraft horizontal tail-actuator shafts, bucket elevators, aircraft propellers, helicopter bolts, air flasks, tie rod ball studs, and spiral gears.

This article reviews the various types of mechanical testing methods, including hardness testing; tension testing; compression testing; dynamic fracture testing; fracture toughness testing; fatigue life testing; fatigue crack growth testing; and creep, stress-rupture, and stress-relaxation testing. Shear testing, torsion testing, and formability testing are also discussed. The discussion of tension testing includes information about stress-strain curves and the properties described by them.

This article examines how design and materials selection address diverse requirements, such as cost, speed, and quality requirements of the process paired with the functional requirements of conventional die casting tooling, specifically tooling for high-volume processes. It discusses considerations, including properties of the material being cast, capacity and operating parameters of the casting machines being used, and economics of post processing that are considered along with the functional requirements.

Wear is mechanically-induced surface damage that results in the progressive removal of material. Because different types of wear occur in machinery, many different types of wear tests have been developed to evaluate its effects on materials and surface treatments. This article provides an explanation on mechanisms, forms (sliding, impact, and rolling) and the causes of wear. It describes the wear measuring methods, including the mass loss method, wear width method, and scar depth method. The units used to report wear vary with type of wear and with the purpose for which the data are to be used. Listing the considerations of tribosystem analysis, the article provides information on selection of ASTM wear test methods grouped by wear type. The article concludes by tabulating the testing geometries and parameters that are commonly controlled and reported when conducting wear tests.

This article focuses on the factors that determine the extent of deformation a metal can withstand before cracking or fracture occurs. It informs that workability depends on the local conditions of stress, strain, strain rate, and temperature in combination with material factors. The article discusses the common testing techniques and process variables for workability prediction. It illustrates the simple and most widely used fracture criterion proposed by Cockcroft and Latham and provides a workability analysis using the fracture limit line. The article describes various workability tests, such as the tension test, ring compression test, plane-strain compression test, bend test, indentation test, and forgeability test. It concludes with information on the role of the finite-element modeling software used in workability analysis.

This article discusses two types of hot-tension tests, namely, the Gleeble test and conventional isothermal hot-tension test, as well as their equipment. It summarizes the data for hot ductility, strength, and hot-tension for commercial alloys. The article presents isothermal hot-tension test data, which helps to gain information on a number of material parameters and material coefficients. It details the effect of test conditions on flow behavior. The article briefly describes the detailed interpretation of data from the isothermal hot-tension test using numerical model. It also explains the cavitation mechanism and failure modes that occur during hot-tension testing.

In terms of their electrical properties, plastics can be divided into thermosetting and thermoplastic materials, some of which are conductive or semiconductive. This article provides detailed information on factors that affect the property of plastics. It discusses the major test methods used to determine the following dielectric properties of plastics: dielectric breakdown voltage, dielectric strength, dielectric constant, dissipation factor, arc tracking resistance, insulation resistance, volume, and surface resistivity or conductivity. The test specifications and conditions, recommended by several U.S. and foreign testing organizations for characterizing the electrical properties of plastic materials are listed. The article describes the influence of these properties on selection of plastics for insulation application. An outline of the electromagnetic shielding and testing methods of electromagnetic interference are also provided. Designations, electrical properties, and applications of elastomers are tabulated.

This article provides a discussion on probes for laboratory tests and resultant curves of industrial quenching processes. It describes the scope of the tests, and the calculation of heat-transfer coefficient (HTC) based on the tests. The article highlights the differences between the laboratory tests and characterization of industrial quenching processes. It reviews the importance of initial heat-flux density and first critical heat-flux density. The theoretical principle behind and the purpose of the temperature gradient method are discussed. The article provides information on the design of the probe, heat-extraction dynamics, and influence of wetting kinematics. It also includes discussions on the simplified 1-D temperature-distribution model, calculation of the HTC, and the finite-volume method for the heat-conduction equation.

This article discusses the identifying characteristics of the forms or mechanisms of corrosion that commonly attack copper metals, as well as the most effective means of combating each. It tabulates corrosion ratings of wrought copper alloys in various corrosive media. The article describes the corrosion behavior of copper alloys in specific environments. It reviews the corrosion characteristics of copper and copper alloys in various acids, alkalis, salts, organic compounds, and gases. The article provides information on the behavior of copper alloys that is susceptible to stress-corrosion cracking in various industrial and chemical environments. It concludes with a discussion on various corrosion testing methods, including aqueous corrosion testing, dynamic corrosion tests, and stress-corrosion testing.

This article discusses the equipment design, procedures, experimental considerations, and interpretation of the torsion tests used to establish workability. It describes the application of torsion testing to obtain flow-stress data and to gage fracture-controlled workability and flow-localization-controlled failure. The article discusses the torsion test used to establish the processing parameters that are required to produce the desired microstructures.

Friction and wear are important when considering the operation and efficiency of components and mechanical systems. Among the different types and mechanisms of wear, adhesive wear is very serious. Adhesion results in a high coefficient of friction as well as in serious damage to the contacting surfaces. In extreme cases, it may lead to complete prevention of sliding; as such, adhesive wear represents one of the fundamental causes of failure for most metal sliding contacts, accounting for approximately 70% of typical component failures. This article discusses the mechanism and failure modes of adhesive wear including scoring, scuffing, seizure, and galling, and describes the processes involved in classic laboratory-type and standardized tests for the evaluation of adhesive wear. It includes information on standardized galling tests, twist compression, slider-on-flat-surface, load-scanning, and scratch tests. After a discussion on gear scuffing, information on the material-dependent adhesive wear and factors preventing adhesive wear is provided.

Acoustic emission is the generation of stress waves by sudden movement in stressed materials. This article begins with a comparison of acoustic emission from most other nondestructive testing (NDT) methods, and discusses the range of applicability of acoustic emission. It describes the instrumentation principles of acoustic emission and reviews the role of acoustic emission in materials studies. The article illustrates the testing of metal-matrix composites (MMCs) using acoustic emission and the use of acoustic emission inspection in production quality control. It concludes with information on the structural test applications of acoustic emission inspection to find defects and to assess or ensure structural integrity.

This article introduces the principal methodologies and some advanced technologies that are being applied for nondestructive evaluation (NDE) of fiber-reinforced polymer-matrix composites. These include acoustic emission, ultrasonic, eddy-current, computed tomography, electromagnetic acoustic transducer, radiography, thermography, and low-frequency vibration methods. The article also provides information on NDE methods commonly used for metal-matrix composites.

Powder forging is an extension of the conventional press and sinter powder metallurgy process, which is recognized as an effective technology for producing a variety of parts to net or near-net shape. This article focuses on the material considerations, such as powder characteristics, alloy development, and inclusion assessment; and process considerations, such as process stages, tool design, and secondary operations; of ferrous alloy powder forging. The mechanical properties of powder forged materials are also reviewed. The article discusses the quality assurance tests for powder forged materials: the part dimensions and surface finish measurement, magnetic particle inspection, metallographic analysis, and nondestructive testing. It concludes with a discussion on the applications of powder forged parts with examples.

Temperature control in heat treating is of paramount importance in maintaining the quality and achieving the desired metallurgical results. This article provides a detailed account of the factors affecting temperature control in heat treating furnaces, with information on temperature control systems, including contact sensors, noncontact sensors, controllers, energy-flow regulators, measurement instruments, and set-point programmers. Common contact sensors include temperature scales, thermocouples, and resistance temperature detectors, whereas optical pyrometers and on-line radiation thermometers fall under the noncontact type. The article describes two types of instrumentation used in heat treating: field test instruments for temperature-uniformity surveys and system-accuracy tests; and controlling, monitoring, and recording instruments for digital instrumentation.