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Brian S. Hayes, Luther M. Gammon
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resin impregnation
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Book Chapter
Secondary Operations for Powder Metallurgy Stainless Steels
Available to PurchaseBook: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006119
EISBN: 978-1-62708-175-7
... of the parts with particulates and residues, which can result in the appearance of surface rust. This article provides information on various secondary operations, including tumbling, re-pressing, resin impregnation, annealing or heat treating, brazing, machining, and welding. It describes those aspects...
Abstract
Powder metallurgy (PM) stainless steels, as with conventional PM steels, are often used in the as-sintered condition. In addition to cost considerations, minimization of postsinter handling and secondary operations is also preferred because it reduces the potential for contamination of the parts with particulates and residues, which can result in the appearance of surface rust. This article provides information on various secondary operations, including tumbling, re-pressing, resin impregnation, annealing or heat treating, brazing, machining, and welding. It describes those aspects relating to welding of PM stainless steels, specifically, the effects of density, residual porosity, and sintered chemistry on weldability. Further, the article investigates the influence the sintering atmosphere has on machinability, as well as differences created by the presence of residual porosity.
Image
Mounted titanium honeycomb specimen. Note the cuts introduced into the tita...
Available to Purchase
in Special Sample Preparation and Polishing for Fiber-Reinforced Composites[1]
> Metallography and Microstructures
Published: 01 December 2004
Fig. 1 Mounted titanium honeycomb specimen. Note the cuts introduced into the titanium honeycomb to facilitate resin impregnation.
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Book Chapter
Special Sample Preparation and Polishing for Fiber-Reinforced Composites
Available to PurchaseSeries: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0009074
EISBN: 978-1-62708-177-1
... damage to the sample. To make these types of specimens ready for grinding and final polishing, it is necessary that the honeycomb is impregnated with a mounting resin. This is accomplished using a thin abrasive blade and making cuts through the honeycomb core, but not far enough to separate the sample...
Abstract
This article focuses on the sample preparation methods for titanium honeycomb composites, boron fiber composites, and titanium/polymeric composite hybrids. These include mounting, sectioning, grinding, and polishing. The article also provides information on the sample preparation of unstaged and staged prepreg materials for optical analysis.
Book Chapter
Effects of Composition, Processing, and Structure on Properties of Composites
Available to PurchaseSeries: ASM Handbook
Volume: 20
Publisher: ASM International
Published: 01 January 1997
DOI: 10.31399/asm.hb.v20.a0002465
EISBN: 978-1-62708-194-8
... Wet fiber, winding, prepreg tape Undirectional continuous fiber tape Yes Yes Yes Multidirectional parallel to mandrel Low Low Braiding Wet resin impregnation after winding Continuous fiber Yes Yes Yes Parallel to braid mold surface, multidirectional fibers Medium/high Medium...
Abstract
This article describes the interaction of composition, manufacturing process, and composite properties of composites. The manufacturing process includes resin-matrix, metal-matrix, and carbon/carbon matrix processing. The article discusses various mechanical properties of composites. It explores how variations in the composition, manufacturing, shop process instructions, and loading/environmental conditions can affect the use of a composite product in a performance/service life operation.
Book: Composites
Series: ASM Handbook
Volume: 21
Publisher: ASM International
Published: 01 January 2001
DOI: 10.31399/asm.hb.v21.a0003416
EISBN: 978-1-62708-195-5
... driven by reductions in cost of the fibers (and the resultant prepreg), the need for minimal or no cleanup (long a problem for wet filament-winding), the reduced environmental impact, and faster wind speeds (no resin sling for hoops, no aeration of resin in impregnation bath). Increased strength...
Abstract
Filament winding is a process for fabricating a composite structure in which continuous reinforcements, either previously impregnated with a matrix material or impregnated during winding, is placed over a rotating form or mandrel in a prescribed way to meet certain stress conditions. This article describes the advancements in filament winding and lists the advantages and disadvantages of filament winding. It discusses the effects of fiber tension in filament winding and the selection of fibers, resins, and materials for filament winding. The article emphasizes the three basic filament-winding patterns, such as helical, polar, and hoop. It presents information on the applications of filament winding, including rocket motors, natural gas vehicle (NGV) tanks, and sporting goods. The article presents recommendations for the basic design guidelines for filament-winding design/manufacturing process and concludes with a discussion on fabrication recommendations.
Book: Composites
Series: ASM Handbook
Volume: 21
Publisher: ASM International
Published: 01 January 2001
DOI: 10.31399/asm.hb.v21.a0003368
EISBN: 978-1-62708-195-5
... a discussion on the background, categories, characteristics, product forms, properties, cost benefits, and processing techniques of thermoplastic resins. Strategies that have been advanced to deal with impregnation difficulties are also discussed. thermoplastic resins continuous fiber reinforced...
Abstract
This article provides information on the thermoplastic resins used as matrix materials for continuous fiber reinforced composites. It focuses on the materials that are suitable for fabrication of structural laminates and used for aerospace applications. The article provides a discussion on the background, categories, characteristics, product forms, properties, cost benefits, and processing techniques of thermoplastic resins. Strategies that have been advanced to deal with impregnation difficulties are also discussed.
Book: Composites
Series: ASM Handbook
Volume: 21
Publisher: ASM International
Published: 01 January 2001
DOI: 10.31399/asm.hb.v21.a0003441
EISBN: 978-1-62708-195-5
... of continuous filament carbon and graphite yarns, strands, rovings, and tows by the tensile loading to failure of the resin-impregnated fiber forms. This technique loses accuracy as the filament count increases. Strain and Young's modulus are measured by extensometer. The purpose of using impregnating resin...
Abstract
This article describes the most significant tests to characterize the properties of constituent materials. It discusses the chemical, physical, and mechanical tests for determining the properties of reinforcement fibers and fabrics. The article provides information on some of the basic materials used for thermoset and thermoplastic resin matrices. It reviews the identification of the individual characteristics of thermoset and thermoplastic resin along with the test methods normally used for their determination. The article contains a table that lists properties and tests for uncured and cured thermoset-matrix resins and prepregs.
Image
Cross section of a polished composite showing areas of the microcracks part...
Available to Purchase
in Rough Grinding and Polishing of Fiber-Reinforced Composite Samples[1]
> Metallography and Microstructures
Published: 01 December 2004
Fig. 1 Cross section of a polished composite showing areas of the microcracks partially filled with epoxy mounting resin. Incomplete impregnation of the mounting resin can cause edge rounding and also fill the unprotected edges with grinding and polishing debris. Unimpregnated areas
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Book Chapter
Resin Transfer Molding and Structural Reaction Injection Molding
Available to PurchaseSeries: ASM Desk Editions
Publisher: ASM International
Published: 01 November 1995
DOI: 10.31399/asm.hb.emde.a0003020
EISBN: 978-1-62708-200-6
... quality, process economics, equipment, and tooling. Process Description Resin Transfer Molding Resin transfer molding is a closed-mold, low-pressure process in which a preplaced, dry reinforcement preform is impregnated with a liquid resin in an injection or transfer process ( Fig. 1...
Abstract
Resin transfer molding (RTM) and structural reaction injection molding (SRIM) are two similar processes that are well suited to the manufacture of large, complex, and high-performance structures. This article discusses the similarities and differences of RTM and SRIM processes and the unique design considerations with respect to the physical properties, geometry, surface quality, process economics, equipment, and tooling of a component that should be considered in choosing RTM or SRIM over other competing processes for fabricating reinforced components.
Image
Polished composite where Rhodamine B was added to the mounting resin and a ...
Available to Purchase
in Viewing Composite Specimens Using Reflected Light Microscopy[1]
> Metallography and Microstructures
Published: 01 December 2004
Fig. 13 Polished composite where Rhodamine B was added to the mounting resin and a laser penetration dye (Magnaflux Zyglo) was added after polishing. The microcracks impregnated by the Rhodamine-B-dyed mounting resin appear red, and the microcracks impregnated by the (Magnaflux Zyglo
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Book Chapter
Resin Transfer Molding and Structural Reaction Injection Molding
Available to PurchaseBook: Composites
Series: ASM Handbook
Volume: 21
Publisher: ASM International
Published: 01 January 2001
DOI: 10.31399/asm.hb.v21.a0003413
EISBN: 978-1-62708-195-5
... the vacuum bag and a relatively stiff mold. This cavity is then evacuated, which compacts the reinforcement and removes the residual air. Resin is then introduced to the cavity (usually via a peripheral gallery) and impregnates the reinforcement as it advances toward the central suction point(s). Since...
Abstract
Resin transfer molding and structural reaction injection molding belong to a family, sometimes denoted as liquid composite molding. This article provides information on the characteristics and automotive and aerospace applications of liquid composite molding. It reviews techniques that use hard tooling and positive (superatmospheric) pressures to produce structures. The techniques include vacuum-assisted resin injection, vacuum infusion, resin-film infusion, and injection-compression molding. The article provides an overview of the materials that are commonly used together with some of processing characteristics that are important to processing speed and part quality. It concludes with a discussion on design guidelines for the liquid composite molding.
Book: Composites
Series: ASM Handbook
Volume: 21
Publisher: ASM International
Published: 01 January 2001
DOI: 10.31399/asm.hb.v21.a0003431
EISBN: 978-1-62708-195-5
... of a nonconforming condition. The quality of the composite material was based on validating the physical and mechanical properties of that structure after cure. A greater focus now is being placed on understanding the critical resin impregnation process during the fabrication stage. This effort supports the concept...
Abstract
This article presents the importance of progressing from post-manufacturing inspection/verification to in-process inspection/verification methods. It lists the various quality assurance factors considered for typical composite laminate lay-up process. The article provides information on composite cure tooling that is fabricated from steel, aluminum, or high-temperature composite materials. The quality assurance for commercial applications is reviewed. The article concludes with a discussion on data fusion systems designed to provide nondestructive analysis data from fabrication and assembly processes for each individual composite part.
Image
Composite material that was subjected to a laboratory-induced lightning str...
Available to Purchase
in Sample Preparation and Mounting for Fiber-Reinforced Composites[1]
> Metallography and Microstructures
Published: 01 December 2004
Fig. 11 Composite material that was subjected to a laboratory-induced lightning strike. The section shown is 1 mm (0.04 in.) away from the center of the strike. This sample was first impregnated with Rhodamine-B-dyed epoxy casting resin and then, after sectioning, mounted with Coumarin 35
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Book: Composites
Series: ASM Handbook
Volume: 21
Publisher: ASM International
Published: 01 January 2001
DOI: 10.31399/asm.hb.v21.a0003411
EISBN: 978-1-62708-195-5
... impregnated with thermoset resin, supplied in roll form on a backing paper carrier material, on 255 mm (10 in.) inside-diameter cores, and with edges of impregnated fibers flush with backing paper. Backing Paper and Resin Impregnation Rolls of composite material for hand lay-up and automated tape lay...
Abstract
Automated tape laying is a mature process used in both commercial and military aircraft applications. This article provides a brief history of the process and describes the use of commercially available flat and contour tape-laying equipment. It discusses the advantages and disadvantages of the tape laying. The article describes the various components of a ten-axis gantry-type tape laying machine and the tape laying process. It provides a discussion on typical material types and forms for tape laying and provides information on design guidelines for tape laying.
Book Chapter
Pultrusion
Available to PurchaseSeries: ASM Desk Editions
Publisher: ASM International
Published: 01 November 1995
DOI: 10.31399/asm.hb.emde.a0003038
EISBN: 978-1-62708-200-6
... in the pultrusion process, the three that precede machine operation are a reinforcement handling system (referred to as creels), a resin impregnation station, and the material forming area. The machine consists of component equipment that heats, consolidates, continuously pulls, and cuts the profiles to a desired...
Abstract
Pultrusion is an automated process for manufacturing composite materials into continuous, constant cross-sectional profiles. The article provides an overview of the pultrusion process and the wide range of materials that can be used to provide a broad spectrum of composite properties. It discusses the mechanical, physical and material properties of pultruded products, and the orientation options available to utilize the properties advantageously. The article also provides guidelines for designing pultruded products.
Book Chapter
Toughening Methods for Thermoset-Matrix Composites
Available to PurchaseSeries: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0009080
EISBN: 978-1-62708-177-1
... is double-pass impregnation, which involves first impregnating a homogeneous resin (no particles) into the inner fiber bed area, followed by selectively coating a particle-modified resin on the prepreg surface ( Ref 22 ). Another technique for the development of prepreg having d surfaces is single-pass...
Abstract
This article describes the dispersed-phase toughening of thermoset matrices by the development of multiphase-structure thermosetting matrices using rubber and/or thermoplastic materials. It discusses two main methods for manufacturing prepregs, namely, single-pass impregnation and double-pass impregnation. The article illustrates reflected-light optical microscopy techniques to evaluate the morphology of thermoplastic materials for determining the material quality and correlating key microstructural features with material performance.
Book: Composites
Series: ASM Handbook
Volume: 21
Publisher: ASM International
Published: 01 January 2001
DOI: 10.31399/asm.hb.v21.a0003417
EISBN: 978-1-62708-195-5
... machine are the reinforcement handling system (referred to as roving and mat creels), the resin impregnation station, and the material forming (or preforming) area. The pultrusion machine consists of component equipment that heats the input materials, cures the reactive resin, pulls the product through...
Abstract
Pultrusion is a cost-effective automated process for manufacturing continuous, constant cross-section composite profiles. This article describes the process characteristics and advantages of pultrusion. It provides information on the applications of pultrusion and discusses the processing equipment and tooling, the material composition, and the process control essential for a basic understanding of the pultrusion process.
Book Chapter
Fabrics and Preforms
Available to PurchaseBook: Composites
Series: ASM Handbook
Volume: 21
Publisher: ASM International
Published: 01 January 2001
DOI: 10.31399/asm.hb.v21.a0003360
EISBN: 978-1-62708-195-5
..., the preform is placed in a metal die, deformed into the required shape, and impregnated with a suitable resinous material to ensure geometric stability during the remainder of the densification process, as shown in Fig. 7 . It may or may not be necessary to slit the preform before deformation; although...
Abstract
This article describes the types of fabrics and preforms used in the manufacture of advanced composites and related selection, design, manufacturing, and performance considerations. The types of fabrics and preforms include unidirectional and two-directional fabrics; multidirectionally reinforced fabrics; hybrid fabrics; woven fabric prepregs; unidirectional and multidirectional tape prepregs; and the prepreg tow. The article discusses three major categories of tape manufacturing processes, namely, the hand lay-up, machine-cut patterns that are laid up by hand, and the automatic machine lay-up. It provides a description of the two classes of prepregs. These include those that are suitable for high-performance applications and suitable for lower-performance molding compounds.
Book Chapter
Glossary of Terms: Composites
Available to PurchaseBook: Composites
Series: ASM Handbook
Volume: 21
Publisher: ASM International
Published: 01 January 2001
DOI: 10.31399/asm.hb.v21.a0003487
EISBN: 978-1-62708-195-5
... to bearing area. The diameter of the hole times the the surface of a plastic, with boundaries that 1270 mm (50 in.) wide. It may or may not be thickness of the material. The cross-section may be more or less sharply de ned, some- impregnated with resin and is usually fur- area of the bearing load member...
Abstract
This article presents a comprehensive collection of the definition of terms related to metallurgy.
Book Chapter
Filament Winding
Available to PurchaseSeries: ASM Desk Editions
Publisher: ASM International
Published: 01 November 1995
DOI: 10.31399/asm.hb.emde.a0003039
EISBN: 978-1-62708-200-6
... design factors filament winding resin systems surface considerations winding machine FILAMENT WINDING is a process that allows the precise lay-down of continuous reinforcement in predescribed patterns at a high rate of speed. In this process, continuous resin-impregnated reinforcements...
Abstract
Filament winding is a process that allows the precise lay-down of continuous reinforcement in predescribed patterns at a high rate of speed. This article discusses the filament winding process and includes a comparison to other compacting and curing processes. The article describes design factors, and techniques to produce aerodynamic surfaces, improve surface smoothness, and avoid slipping and bridging of filament. The article discusses tooling and the equipment used in the filament winding process, namely, mandrel design, winding machines, tensioners, and ovens.
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