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resin cure control flow sensing
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Book: Composites
Series: ASM Handbook
Volume: 21
Publisher: ASM International
Published: 01 January 2001
DOI: 10.31399/asm.hb.v21.a0003435
EISBN: 978-1-62708-195-5
... dielectric cure sensors, fiberoptics-based resin cure sensors, ultrasonics-based resin cure sensors, and dosimetry-based resin cure sensors. The article provides information on the resin cure control flow sensing, flow modeling, flow mapping, and resin flow. It addresses some practical issues in sensing...
Abstract
This article discusses the attempts made by the industry to create sensing approaches for modeling a process, part, and chemistry and kinetics. It reviews microwave curing of thick-section composites and the resin cure sensors that are used for resin cure monitoring. These include dielectric cure sensors, fiberoptics-based resin cure sensors, ultrasonics-based resin cure sensors, and dosimetry-based resin cure sensors. The article provides information on the resin cure control flow sensing, flow modeling, flow mapping, and resin flow. It addresses some practical issues in sensing resin cure and flow.
Series: ASM Handbook
Volume: 11B
Publisher: ASM International
Published: 15 May 2022
DOI: 10.31399/asm.hb.v11B.a0006916
EISBN: 978-1-62708-395-9
... the ability to easily dispense or flow before curing. Adhesives offer a great example. Think about the five-minute epoxies available at most hardware stores. The user mixes Part A (resin) and Part B (hardener), and the mixture is a relatively low-viscosity substance that is applied to the surfaces...
Abstract
This article focuses on manufacturing-related failures of injection-molded plastic parts, although the concepts apply to all plastic manufacturing processes It provides detailed examples of failures due to improper material handling, drying, mixing of additives, and molecular packing and orientation. It also presents examples of failures stemming from material degradation improper use of metal inserts, weak weld lines, insufficient curing of thermosets, and inadequate mixing and impregnation in the case of thermoset composites.
Book Chapter
Book: Casting
Series: ASM Handbook
Volume: 15
Publisher: ASM International
Published: 01 December 2008
DOI: 10.31399/asm.hb.v15.a0005354
EISBN: 978-1-62708-187-0
... in handling sand-resin mixtures for no-bake molds or cones and lists some advantages of no-bake air-set cores and molds. The article describes the process procedures, advantages, and disadvantages of gas curing and air-setting hardening of sodium silicates. It examines the members of the air-setting organic...
Abstract
No-bake sand molds are based on the curing of inorganic or organic binders with either gaseous catalysts or liquid catalysts. This article reviews the major aspects of no-bake sand bonding in terms of coremaking, molding methods, and sand processing. It discusses the points to be noted in handling sand-resin mixtures for no-bake molds or cones and lists some advantages of no-bake air-set cores and molds. The article describes the process procedures, advantages, and disadvantages of gas curing and air-setting hardening of sodium silicates. It examines the members of the air-setting organic binders, namely, furan no-bake resins, phenolic no-bake resins, and urethanes. The article provides an overview of gas-cured organic binders. It also illustrates the three commercial systems for sand reclamation: wet reclamation systems, dry reclamation systems, and thermal reclamation.
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 November 1995
DOI: 10.31399/asm.hb.emde.a0003045
EISBN: 978-1-62708-200-6
... analysis pattern orientation control quality control techniques tooling control ultrasonic inspection ultrasonic scans QUALITY ASSURANCE for composites has traditionally centered on techniques for validating the physical/mechanical properties of a cured laminate. This end-result approach has...
Abstract
Ultrasonic inspection is a nondestructive technique that is useful in both quality control and research applications for flaw detection in fiber-reinforced composite materials. This article describes ultrasonic nondestructive analysis by outlining its three basic types of scans. It reviews the important quality control techniques used during the manufacture of composite components by analyzing tooling control, material control, pattern orientation control, and in-process control.
Book: Composites
Series: ASM Handbook
Volume: 21
Publisher: ASM International
Published: 01 January 2001
DOI: 10.31399/asm.hb.v21.a0003413
EISBN: 978-1-62708-195-5
... the most popular material for high-volume automotive work. The mold design loop needs to address the flow, thermal, and structural characteristics of the tool set. Failure to address each of these issues will result in lack of control over the part impregnation, curing, and dimensional control...
Abstract
Resin transfer molding and structural reaction injection molding belong to a family, sometimes denoted as liquid composite molding. This article provides information on the characteristics and automotive and aerospace applications of liquid composite molding. It reviews techniques that use hard tooling and positive (superatmospheric) pressures to produce structures. The techniques include vacuum-assisted resin injection, vacuum infusion, resin-film infusion, and injection-compression molding. The article provides an overview of the materials that are commonly used together with some of processing characteristics that are important to processing speed and part quality. It concludes with a discussion on design guidelines for the liquid composite molding.
Series: ASM Handbook
Volume: 11B
Publisher: ASM International
Published: 15 May 2022
DOI: 10.31399/asm.hb.v11B.a0006924
EISBN: 978-1-62708-395-9
... to calculate the conversion or degree of cure from the ΔH res or from T g,res if the T g conversion relationship has been established. Rheological Methods In addition to the curing process, the flow of the uncured resin formulation is a key processing parameter. As such, rheological methods...
Abstract
This article discusses the most common thermal analysis methods for thermosetting resins. These include differential scanning calorimetry, thermomechanical analysis, thermogravimetric analysis, and dynamic mechanical analysis. The article also discusses the characterization of uncured thermosetting resins as well as the curing process. Then, the techniques to characterize the physical properties of cured thermosets and composites are presented. Several examples of stress-strain curves are shown for thermosets and thermoplastic polymers.
Book Chapter
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 November 1995
DOI: 10.31399/asm.hb.emde.a0003047
EISBN: 978-1-62708-200-6
... conditions. It then focuses on the characteristics, types, and properties of the five groups of adhesives, such as structural, hot melt, pressure sensitive, water based, ultraviolet, and electron beam cured adhesives. The article also discusses the functions and applications of adhesive modifiers, including...
Abstract
This article begins with an overview of the fundamentals of adhesive technology, including functions, limitations, adhesive joint types, and the key factors in the selection of adhesives, including application, type of joint, process limitation, mechanical requirement, and service conditions. It then focuses on the characteristics, types, and properties of the five groups of adhesives, such as structural, hot melt, pressure sensitive, water based, ultraviolet, and electron beam cured adhesives. The article also discusses the functions and applications of adhesive modifiers, including fillers, adhesion promoters, tackifiers, and tougheners. It gives a short note on functions of primers and primerless bonding. Applications of adhesives in automotive, aerospace, electronics, electrical, medical, sports, and construction sectors are also described. Finally, the article describes the steps in adhesive bonding, including storage and handling of adhesives, bonding preparation, adhesive application, tooling, and curing.
Book: Composites
Series: ASM Handbook
Volume: 21
Publisher: ASM International
Published: 01 January 2001
DOI: 10.31399/asm.hb.v21.a0003456
EISBN: 978-1-62708-195-5
... prematurely begin the curing process of resins and adhesives, thus shortening their working life. Humidity control is important as polymeric materials absorb moisture readily from the atmosphere, contaminating the material and possibly reducing the mechanical properties. Excessively low humidity...
Abstract
Maintainability is a function of the durability, damage tolerance, and repairability of a structure. This article discusses the configurations of composite structures, such as sandwich, stiffened-skin, and monolithic structures, used in commercial aircraft composites. It describes the considerations for maintainability of the composite structures during the conceptual design phase. Sources of the defects and damage, such as manufacturing defects and in-service defects, are reviewed. The article describes the nondestructive inspection methods that are used in the repair of composite structures to locate damage, characterize the extent of damage, and ensure post-repair quality. It lists suggestions that can be used as design guidelines for adhesive bonding, general composite structure, sandwich structure, material selection, and lightning-strike protection. The article also provides the basic considerations for personnel, facilities, and equipment during maintenance.
Series: ASM Handbook
Volume: 6
Publisher: ASM International
Published: 01 January 1993
DOI: 10.31399/asm.hb.v06.a0001466
EISBN: 978-1-62708-173-3
... sense to save on the cost of this operation by using cheaper fibers with the same resin. One solution for the problem of a large range in temperature within the composite part or assembly, once a cure is already in progress, is to put constant-temperature dwells in the cure cycle to give the various...
Abstract
Successful adhesive bonding of organic-matrix composites is dependent on the nature of the adherend surfaces. This article emphasizes the critical importance of proper surface preparation in both thermoset and thermoplastic composites. It provides information on surface preparation for thermoset composite adherends along with a standard technique (water-break test) for verifying the adequacy of surface preparation for metal bonding. In addition, the article provides examples of good and bad adhesive bonds and describes some important process variables that are considered and controlled in bonding process for thermoset adhesives. The article concludes with a discussion on three different approaches for bonding thermoplastic composite composite panels together.
Series: ASM Handbook
Volume: 5B
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v05b.a0006063
EISBN: 978-1-62708-172-6
... be combined with knowledge of coatings, field observations, thorough document review, and common sense. Coatings and coating products are numerous and variable and likely will continue to increase in complexity. The problems related to historic, current, and newly developed coatings will correspondingly...
Abstract
This article provides an overview of common analytical tools used as part of the process of providing practical information regarding the causes of a coating problem or failure. The common analytical tools include Fourier transform infrared spectroscopy, differential scanning calorimetry, scanning electron microscopy-energy dispersive X-ray spectroscopy, chromatography, and electrochemical impedance spectroscopy. Test cabinets and standard test environments for laboratory analysis are reviewed. The article describes non-standard simulation testing and case studies of simulated environments for coating failure analysis.
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 November 1995
DOI: 10.31399/asm.hb.emde.9781627082006
EISBN: 978-1-62708-200-6
Book Chapter
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 November 1995
DOI: 10.31399/asm.hb.emde.a0003068
EISBN: 978-1-62708-200-6
... pressure in a medium to the rate of alternating flow of between the catalyst and the resin (usually in the polym- the medium through a specified surface due to the abbesive. A material that resists adhesion. A film or erizing of resins or vulcanization of rubbers). Also sound wave. coating applied...
Series: ASM Handbook
Volume: 24
Publisher: ASM International
Published: 15 June 2020
DOI: 10.31399/asm.hb.v24.a0006578
EISBN: 978-1-62708-290-7
..., curing characteristics, green-part fabrication, property identification, process design and planning, and quality control and optimization are introduced. The article also provides information on postprocessing techniques, namely debinding and sintering, as well as on the phenomenon of shrinkage...
Abstract
This article presents a detailed account of the processes involved in vat-photopolymerization-based fabrication of ceramics, namely bioceramics, structural ceramics, piezoelectric ceramics, optical ceramics, and polymer-derived ceramics. Information and methods of material preparation, curing characteristics, green-part fabrication, property identification, process design and planning, and quality control and optimization are introduced. The article also provides information on postprocessing techniques, namely debinding and sintering, as well as on the phenomenon of shrinkage and compensation.
Series: ASM Handbook
Volume: 11B
Publisher: ASM International
Published: 15 May 2022
DOI: 10.31399/asm.hb.v11B.9781627083959
EISBN: 978-1-62708-395-9
Book: Composites
Series: ASM Handbook
Volume: 21
Publisher: ASM International
Published: 01 January 2001
DOI: 10.31399/asm.hb.v21.a0003350
EISBN: 978-1-62708-195-5
.... They are used mainly in commercial, industrial, and transportation applications, including chemically resistant piping and reactors, truck cabs and bodies, appliances, bathtubs and showers, and automobile hoods, decks, and doors. The very large number of resin formulations, curing agents, fillers, and other...
Abstract
This article begins with a brief history of composite materials and discusses its characteristics. It presents an introduction to the constituents, product forms, and fabrication processes of composite materials. The article concludes with a discussion on the applications of organic-matrix, metal-matrix, and ceramic-matrix composites.
Series: ASM Handbook
Volume: 11B
Publisher: ASM International
Published: 15 May 2022
DOI: 10.31399/asm.hb.v11B.a0006930
EISBN: 978-1-62708-395-9
... Abstract Rheology is defined as the study of the flow and deformation of matter. This article begins with an examination of flow behavior. It describes the geometries and methods employed for rheological testing of polymers in their molten state. It also discusses materials...
Abstract
Rheology is defined as the study of the flow and deformation of matter. This article begins with an examination of flow behavior. It describes the geometries and methods employed for rheological testing of polymers in their molten state. It also discusses materials that are predominantly in the solid state and the methods employed for solids testing. Examples of unidirectional and dynamic oscillatory testing are provided for different mechanical behaviors.
Series: ASM Handbook
Volume: 11B
Publisher: ASM International
Published: 15 May 2022
DOI: 10.31399/asm.hb.v11B.a0006925
EISBN: 978-1-62708-395-9
.... Engineering plastics all have, as their principal constituent, one or more synthetic polymer resins and almost universally contain additives. Additives, which have much smaller molecules than polymers, provide color, flexibility, rigidity, flame resistance, weathering resistance, and/or processibility...
Abstract
This introductory article describes the various aspects of chemical structure that are important to an understanding of polymer properties and thus their eventual effect on the end-use performance of engineering plastics. The polymers covered include hydrocarbon polymers, carbon-chain polymers, heterochain polymers, and polymers containing aromatic rings. The article also includes some general information on the classification and naming of polymers and plastics. The most important properties of polymers, namely, thermal, mechanical, chemical, electrical, and optical properties, and the most significant influences of structure on those properties are then discussed. A variety of engineering thermoplastics, including some that are regarded as high-performance thermoplastics, are covered in this article. In addition, a few examples of commodity thermoplastics and biodegradable thermoplastics are presented for comparison. Finally, the properties and applications of six common thermosets are briefly considered.
Series: ASM Handbook
Volume: 24A
Publisher: ASM International
Published: 30 June 2023
DOI: 10.31399/asm.hb.v24A.a0006968
EISBN: 978-1-62708-439-0
... of product development ( Ref 5 ). Because of these advantages, the emergence of AM technologies marks a new era for the manufacturing industry. Polymer-based AM is a critical AM branch that first appeared as stereolithography (SLA), which is based on photochemical resin curing ( Ref 1 ). Currently...
Abstract
Additive manufacturing (AM) is a revolutionary technology that fabricates parts layerwise and provides many advantages. This article discusses polymer AM processes such as material extrusion, vat photopolymerization (VPP), powder-bed fusion (PBF), binder jetting (BJ), material jetting (MJ), and sheet lamination (SL). It presents the benefits of online monitoring and process control for polymer AM. It also introduces the respective monitoring devices used, including the models and algorithms designed for polymer AM online monitoring and control.
Series: ASM Handbook
Volume: 5B
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v05b.a0006073
EISBN: 978-1-62708-172-6
... occurs primarily as a result of solvent addition to the resin when manufacturing the paint. Solvents are added in order to reduce the viscosity of a resin, thinning it for application purposes. Upon drying and curing, the solvent must volatilize from the coating into the atmosphere in a timely manner...
Abstract
This article discusses the environmental influences on protective coating films that can result in deterioration. These environmental factors can be classified into four groups: (1) energy: solar, heat; (2) permeation: moisture, solvent, chemical, and gas; (3) stress: drying and curing-internal stress, and vibration-external stress; and (4) biological influences such as microbiological, mildew, and marine fouling.
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006782
EISBN: 978-1-62708-295-2
... of the material), the increased molecular mobility results in significant changes in the properties of a cured resin system. From the DSC graph, the heat of fusion, which is determined from the melting endotherm and indicates the degree of crystallinity of the polymer, can be calculated. From the graph, the T g...
Abstract
Corrosion is the deterioration of a material by a reaction of that material with its environment. The realization that corrosion control can be profitable has been acknowledged repeatedly by industry, typically following costly business interruptions. This article describes the electrochemical nature of corrosion and provides the typical analysis of environmental- and corrosion-related failures. It presents common methods of testing of laboratory corrosion and discusses the processes involved in the prevention of environmental- and corrosion-related failures of metals and nonmetals.
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