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residual porosity
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Image
Published: 30 September 2015
Fig. 2 Effect of residual porosity, reported as relative density, on mechanical properties. A relative density of 1.0 represents the pore-free state indicated by the vertical broken line. The gray shaded region immediately to the left represents the range from 98% dense to fully dense
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Image
Published: 30 September 2015
Fig. 12 Influence of process variables on residual porosity in critical corner areas of a powder-forged gear tooth. (a) Powder-forged gear; D1 and D2 are average densities in grams per cubic centimeter. (b) Preform temperature at a forging pressure of 1000 MPa (145 ksi). (c) and (d) Forging
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Published: 01 January 2005
Fig. 13 Influence of process variables on residual porosity in critical corner areas of a powder forged gear tooth. (a) Powder forged gear; D1 and D2 are average densities in grams per cubic centimeter. (b) Preform temperature at a forging pressure of 1000 MPa (145 ksi). (c) and (d) Forging
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Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006119
EISBN: 978-1-62708-175-7
... relating to welding of PM stainless steels, specifically, the effects of density, residual porosity, and sintered chemistry on weldability. Further, the article investigates the influence the sintering atmosphere has on machinability, as well as differences created by the presence of residual porosity...
Abstract
Powder metallurgy (PM) stainless steels, as with conventional PM steels, are often used in the as-sintered condition. In addition to cost considerations, minimization of postsinter handling and secondary operations is also preferred because it reduces the potential for contamination of the parts with particulates and residues, which can result in the appearance of surface rust. This article provides information on various secondary operations, including tumbling, re-pressing, resin impregnation, annealing or heat treating, brazing, machining, and welding. It describes those aspects relating to welding of PM stainless steels, specifically, the effects of density, residual porosity, and sintered chemistry on weldability. Further, the article investigates the influence the sintering atmosphere has on machinability, as well as differences created by the presence of residual porosity.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006125
EISBN: 978-1-62708-175-7
... Abstract The residual porosity in sintered refractory metal ingots is usually eliminated by different densification processes, such as thermomechanical processes. This article focuses on thermomechanical processing of tungsten, molybdenum, and tantalum. It provides an overview of liquid-phase...
Abstract
The residual porosity in sintered refractory metal ingots is usually eliminated by different densification processes, such as thermomechanical processes. This article focuses on thermomechanical processing of tungsten, molybdenum, and tantalum. It provides an overview of liquid-phase sintering of tungsten heavy alloys and describes the infiltration of tungsten and molybdenum for attaining full density. The article concludes by providing information on hot isostatic pressing of refractory metal alloys to full density.
Image
in Titanium Powder Metallurgy Products
> Properties and Selection: Nonferrous Alloys and Special-Purpose Materials
Published: 01 January 1990
Fig. 2 Chlorine-induced porosity in a titanium BE compact. (a) Scanning electron microscopy photomicrograph of large-size residual porosity in a sectioned Ti-6Al-4V BE compact. (b) Transmission electron microscopy photomicrograph of a Ti-6Al-4V BE compact after postsintering HIP at 925 °C
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Image
Published: 01 January 2001
Fig. 12 Microstructure of a woven Nicalon/Si-C-O-N matrix composite with a SiC filler. Small amounts of residual porosity and a clear filler-free network can be seen in the matrix of the composite.
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Image
Published: 01 January 2001
Fig. 5 Microstructure of reaction-bonded SCS-6 fiber/Si 3 N 4 composite showing uniform fiber distribution and small amounts of residual porosity around the periphery of the large- diameter fibers
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in Preparation and Microstructural Analysis of High-Performance Ceramics
> Metallography and Microstructures
Published: 01 December 2004
Fig. 12 Sealing disk of alumina. The light micrograph shows typical residual porosity of 3–4%, a bimodal grain size distribution, and a glassy phase at the grain boundaries (liquid-phase sintering). Thermally etched at 1400 °C (2550 °F)
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Series: ASM Handbook
Volume: 20
Publisher: ASM International
Published: 01 January 1997
DOI: 10.31399/asm.hb.v20.a0002486
EISBN: 978-1-62708-194-8
... components. The P/F process has been successful in developing mechanical properties in P/F steel comparable to wrought steels (see Table 3 ). This process successfully overcomes the mechanical property limitations imposed by the residual porosity in conventional P/M products. Properties of powder forged...
Abstract
This article begins with a discussion on general powder metallurgy design considerations that assist in the selection of the appropriate processing method. It reviews powder processing techniques, conventional press-and-sinter methods, and full-density processes to understand the design restrictions of each powder processing method. The article provides comparison of powder processing methods based on their similarities, differences, advantages, and disadvantages. It concludes with a discussion on design issues for the components of powder processing technologies.
Series: ASM Handbook
Volume: 24A
Publisher: ASM International
Published: 30 June 2023
DOI: 10.31399/asm.hb.v24A.a0006972
EISBN: 978-1-62708-439-0
... of melt pools, leading to plastic deformation and residual stress exceeding ultimate stress. Fig. 1 Common types of defects found in parts fabricated by means of laser powder-bed fusion. (a) Lack of fusion. (b) Gas-sourced porosity. (c) Microcrack (Source: Ref 4 ). (d) Grain-boundary impurities...
Book: Composites
Series: ASM Handbook
Volume: 21
Publisher: ASM International
Published: 01 January 2001
DOI: 10.31399/asm.hb.v21.a0003421
EISBN: 978-1-62708-195-5
...-matrix composite (some residual porosity can be seen in this micrograph), while Fig. 2(b) shows the pressure and temperature schedule used during hot pressing of this composite. Fig. 1 Schematic of the slurry infiltration process followed by hot pressing Fig. 2 Unidirectional alumina...
Abstract
Ceramic-matrix composites (CMCs) have ability to withstand high temperatures and have superior damage tolerance over monolithic ceramics. This article describes important processing techniques for CMCs: cold pressing, sintering, hot pressing, reaction-bonding, directed oxidation, in situ chemical reaction techniques, sol-gel techniques, pyrolysis, polymer infiltration, self-propagating high-temperature synthesis, and electrophoretic deposition. The advantages and disadvantages of each technique are highlighted to provide a comprehensive understanding of the achievements and challenges that remain in this area.
Series: ASM Handbook
Volume: 2A
Publisher: ASM International
Published: 30 November 2018
DOI: 10.31399/asm.hb.v02a.a0006498
EISBN: 978-1-62708-207-5
... of the die casting process, including high-speed production, excellent dimensional repeatability, tight tolerances, and the ability to produce thin-walled components. Conventional die castings typically contain relatively high levels of residual porosity (both shrinkage and gas porosity), while semisolid...
Abstract
Semisolid casting is a near-net shape manufacturing process capable of producing thick- and thin-walled complex-shaped components having excellent mechanical and functional performance. This article begins with a discussion on the history of semisolid processing and the advantages claimed for semisolid casting. It describes the four notable processes used to produce semisolid castings: thixocasting, rheocasting, thixomolding, and wrought processes. Most commercial aluminum semisolid casters use either thixocasting or rheocasting. The article discusses the die design, process conditions, and simulation for semisolid casting. It concludes with a review of several components produced by each of the various semisolid casting processes.
Series: ASM Handbook
Volume: 24
Publisher: ASM International
Published: 15 June 2020
DOI: 10.31399/asm.hb.v24.a0006566
EISBN: 978-1-62708-290-7
... processes used for steel, and available powder feedstock characteristics. The article emphasizes the characteristics of the as-built microstructure, including porosity, inclusions, and residual stresses. It also reviews the material properties of AM steel parts, including hardness, tensile strength...
Abstract
This article provides a general overview of additively manufactured steels and focuses on specific challenges and opportunities associated with additive manufacturing (AM) stainless steels. It briefly reviews the classification of the different types of steels, the most common AM processes used for steel, and available powder feedstock characteristics. The article emphasizes the characteristics of the as-built microstructure, including porosity, inclusions, and residual stresses. It also reviews the material properties of AM steel parts, including hardness, tensile strength, and fatigue strength, as well as environmental properties with respect to corrosion resistance, highlighting the importance of postbuild thermal processing.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006076
EISBN: 978-1-62708-175-7
... when dimensional change control is a key consideration. Another technique is available to produce copper-infiltrated steels with final residual porosity of less than 1%. The modified process uses a powder forging-grade iron powder, and the dynamic mechanical properties of these materials...
Abstract
The two most important classes of materials that are manufactured via infiltration methods are copper- and silver-infiltrated refractory metals and refractory carbides, and copper-infiltrated steels. This article focuses on copper-infiltrated steels and discusses the basic requirements for infiltration, which is a technique that is only applicable to material systems that meet certain requirements. It addresses these requirements and describes the conventional (partial) infiltration process of powder metallurgy (PM) steel. The materials used in the process, such as matrix and infiltrant, are discussed. The article also details several criteria used to evaluate the performance of an infiltration process. It concludes with information on alloy steels and fully infiltrated steels.
Series: ASM Handbook
Volume: 24A
Publisher: ASM International
Published: 30 June 2023
DOI: 10.31399/asm.hb.v24A.a0006990
EISBN: 978-1-62708-439-0
... by the microstructure but are also affected by porosity and surface roughness. Fatigue failure in AM materials is also influenced by porosity, surface roughness, microstructure, and residual stress due to applied manufacturing processing parameters. Post-processing treatments can further influence fatigue failure in AM...
Abstract
Structure-property relationships for metal additive manufacturing (AM) using solidification-based AM processes (e.g., powder-bed fusion and directed-energy deposition) are the focus of this article. Static strength and ductility properties in AM materials are impacted heavily by the microstructure but are also affected by porosity and surface roughness. Fatigue failure in AM materials is also influenced by porosity, surface roughness, microstructure, and residual stress due to applied manufacturing processing parameters. Post-processing treatments can further influence fatigue failure in AM materials.
Series: ASM Handbook
Volume: 6
Publisher: ASM International
Published: 01 January 1993
DOI: 10.31399/asm.hb.v06.a0001463
EISBN: 978-1-62708-173-3
... of water pressure on the formation of porosity in underwater gravity welding. The article concludes with a discussion on the practical applications of underwater welding. acicular ferrite grain-boundary ferrite heat-affected zone cracking low carbon steel microstructure porosity residual stress...
Abstract
This article discusses the metallurgical aspects of underwater welds. It describes the microstructural development, which mainly includes three types of ferrite associated with low carbon steel weld metal: grain-boundary ferrite, sideplate ferrite, and acicular ferrite. The article explains the factors that affect heat-affected zone (HAZ) cracking. These include hydrogen from the weld pool, microstructures that develop in the HAZ, and stress levels that develop in the weld joint. The article describes the welding practices that can reduce residual stresses. It explains the effect of water pressure on the formation of porosity in underwater gravity welding. The article concludes with a discussion on the practical applications of underwater welding.
Book Chapter
Series: ASM Handbook
Volume: 17
Publisher: ASM International
Published: 01 August 2018
DOI: 10.31399/asm.hb.v17.a0006465
EISBN: 978-1-62708-190-0
..., such as porosity, inclusions, cracking, and residual stress, that can be avoided by using vendor recommended process parameters and approved materials. It describes the development of process-structure-property-performance modeling. The article explains the practical considerations in nondestructive evaluation...
Abstract
Additive manufacturing (AM) is the process of joining materials to make parts from three-dimensional (3D) model data, usually layer upon layer, as opposed to subtractive manufacturing and formative manufacturing methodologies. This article discusses various defects in AM components, such as porosity, inclusions, cracking, and residual stress, that can be avoided by using vendor recommended process parameters and approved materials. It describes the development of process-structure-property-performance modeling. The article explains the practical considerations in nondestructive evaluation for additively manufactured metallic parts. It also examines nondestructive testing (NDT) inspection and characterization methods for each of the manufacturing stages in their natural order. The article provides information on various inspection techniques for completed AM manufactured parts. The various electromagnetic and eddy current techniques that can be used to detect changes to nearsurface geometric anomalies or other defects are also discussed. These include ultrasonic techniques, radiographic techniques, and neutron imaging.
Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0003795
EISBN: 978-1-62708-177-1
... of a ceramic sealing disk with a typical residual porosity of 3 to 4%, a bimodal grain size distribution, and a glassy phase at the grain boundaries (liquid-phase sintering) is given in Fig. 12 . Figure 13 shows the microstructure of a spark plug with anisotropic grains, a glassy grain-boundary phase...
Abstract
Microstructural analysis reveals many important details about the qualities and capabilities of high-performance ceramics. This article explains how to prepare ceramic samples for imaging and the imaging technologies normally used. It describes sectioning, mounting, grinding, and polishing as well as ceramographic etching. It discusses common imaging approaches, including scanning electron microscopy and thin-section polarized light techniques, a type of optical microscopy. The article also addresses microstructural classification, examining detailed micrographs from samples of aluminum oxide, zirconium dioxide, aluminum nitride, silicon carbide, and piezoelectric ceramics.
Book: Fatigue and Fracture
Series: ASM Handbook
Volume: 19
Publisher: ASM International
Published: 01 January 1996
DOI: 10.31399/asm.hb.v19.a0002374
EISBN: 978-1-62708-193-1
... limit of 255 MPa (37 ksi). With expansion of P/M fabrication technology into dynamically loaded components, there arise performance limitations associated with fracture and fatigue. For static tensile properties, there is a good basis for predicting the effect of residual porosity on strength ( Ref 2...
Abstract
This article discusses the fracture and fatigue properties of powder metallurgy (P/M) materials depending on the microstructure. It describes the effects of porosity on the P/M processes relevant to fatigue and fracture resistance. The article details the factors determining fatigue and fracture resistance of P/M materials. It reviews the methods employed to improve fatigue and fracture resistance, including carbonitriding, surface strengthening and sealing treatments, shot-peening, case hardening, repressing and resintering, coining, sizing, and postsintering heat treatments. Safety factors for P/M materials are also detailed.
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