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Book Chapter
Analysis of Designed Experiments
Available to PurchaseSeries: ASM Handbook
Volume: 8
Publisher: ASM International
Published: 01 January 2000
DOI: 10.31399/asm.hb.v08.a0009215
EISBN: 978-1-62708-176-4
... Abstract This article describes methods that are oriented toward the analysis of planned cooperative experiments that involve multiple factors, blocks, and/or treatment levels. The experiments include factorial, fractional factorial, randomized block, and incomplete block experiments...
Abstract
This article describes methods that are oriented toward the analysis of planned cooperative experiments that involve multiple factors, blocks, and/or treatment levels. The experiments include factorial, fractional factorial, randomized block, and incomplete block experiments.
Series: ASM Handbook
Volume: 8
Publisher: ASM International
Published: 01 January 2000
DOI: 10.31399/asm.hb.v08.a0009214
EISBN: 978-1-62708-176-4
... the experimenter varies the parameters, or factors, under study and then observes the effects of this action. These include factorial experiments, blocked factorial experiments, and fractional factorial experiments. The article describes the estimation of experimental errors and provides information on randomized...
Abstract
Planning of experiments does not consist merely of identifying a few key parameters and then selecting a specific plan. Selection of the proper experimental plan depends on the purpose of the experiment, physical restrictions on the taking of measurements, and other restrictions imposed by time, economic considerations, and materials and personnel availability. This article presents recommendations that should be followed in outlining the methods of conducting and analyzing an experiment to ensure successful results. It discusses restricted type of experiments, in which the experimenter varies the parameters, or factors, under study and then observes the effects of this action. These include factorial experiments, blocked factorial experiments, and fractional factorial experiments. The article describes the estimation of experimental errors and provides information on randomized designs and block designs. It also presents the methods for determining optimum conditions or levels.
Book Chapter
Designing, Planning, and Preparing Corrosion Tests
Available to PurchaseSeries: ASM Handbook
Volume: 13A
Publisher: ASM International
Published: 01 January 2003
DOI: 10.31399/asm.hb.v13a.a0003640
EISBN: 978-1-62708-182-5
... of the experimenter's problem. In planning an experiment, it is necessary to limit any bias that may be introduced by the experimental units or experimental conditions. Strategies such as randomization and blocking can be used to minimize the effect of nuisance or noise elements. In some production processes, units...
Abstract
When planning a corrosion-testing program, it is advisable to select the testing conditions carefully in order to produce ranking parameters with minimal influence from testing conditions while rich in engineering significance. This article provides a discussion on test objectives, metal composition and metallurgical conditions, test specimen preparation, and corrosion damage assessment. It describes a strategy for planning the design of controlled and uncontrolled factorial experiments. The article contains a table that lists the elements of an iterative process for the experimental design. It illustrates the experimental designs applied to corrosion testing.
Book Chapter
Fatigue Crack Growth under Variable-Amplitude Loading
Available to PurchaseBook: Fatigue and Fracture
Series: ASM Handbook
Volume: 19
Publisher: ASM International
Published: 01 January 1996
DOI: 10.31399/asm.hb.v19.a0002356
EISBN: 978-1-62708-193-1
... of amplitudes Size of period of blocks Distribution function of amplitudes Complex tests Random load tests Spectral density function (narrow band or broad band) Crest factor (clipping ratio) Irregularity factor Service simulation tests Variable of service load history to be simulated OL...
Abstract
This article summarizes fatigue phenomena in metallic materials. It discusses fatigue under variable-amplitude (VA) loading, with emphasis on crack growth. The article presents the prediction models of crack initiation and crack growth under VA loading. It concludes with a discussion on the conditions associated with engineering applications of VA loading.
Series: ASM Handbook
Volume: 8
Publisher: ASM International
Published: 01 January 2000
DOI: 10.31399/asm.hb.v08.a0009212
EISBN: 978-1-62708-176-4
... specific types of experimental designs, ranging from very simple two-level factorial designs to more complex experimental designs involving multiple levels, randomized blocks and partial factorial procedures. The third article, “Analysis of Designed Experiments,” addresses some of the basic...
Abstract
This article discusses statistical concepts that form the basis of most of the following articles on specific areas of applied statistics and data analysis. It reviews some of the basic concepts that must be understood to successfully apply the statistical procedures, including probability, random variables, degrees of freedom, confidence limits and intervals, and reliability. Descriptive statistics, measures of central tendency, confidence limits and intervals, and degrees of freedom are also discussed.
Series: ASM Handbook Archive
Volume: 10
Publisher: ASM International
Published: 01 January 1986
DOI: 10.31399/asm.hb.v10.a0001763
EISBN: 978-1-62708-178-8
..., the observation of a single maximum or a set of maxima is not sufficient to prove periodicity because they can occur for other reasons. Fig. 4 Types of scattering curves. (a) Widely separated homogeneous spheres. (b) Phase separated blend, block copolymer, a metallic alloy, or a glass. (c) A random...
Abstract
This article presents the experimental and theoretical aspects of small-angle scattering, and discusses specific applications used in the characterization of metals, glasses, polymers, and ceramics. The basic methods of collimating x-rays, the cause of smearing from a line source, desmearing parameters, and the types of scattering curves are illustrated.
Book Chapter
Uncertainty Management in Materials Design and Analysis
Available to PurchaseSeries: ASM Handbook
Volume: 22B
Publisher: ASM International
Published: 01 November 2010
DOI: 10.31399/asm.hb.v22b.a0005534
EISBN: 978-1-62708-197-9
... robust ( Ref 19 , 20 ), distribution robust ( Ref 21 , 22 ), or both ( Ref 13 ). Note that this is a different use of the term robust than robust design of the entire system. In blocking, the experiment is designed so that the experiments are run in small groups or blocks so that the error within...
Abstract
This article presents an approach to manage the uncertainty present in materials design. It describes inductive and deductive approaches to deal with uncertainty. The article focuses on providing an understanding of the opportunities for managing uncertainty and the decisions that influence the accuracy of the results. A design of experiments (DOE) represents a sequence of experiments to be performed, expressed in terms of factors set at specified levels. The article discusses the two types of DOEs: the full factorial design and the fractional factorial design. It explains the factors to be considered when selecting a procedure for propagating uncertainty. The article lists the categories of the popular types of uncertainty propagation methods, including simulation-based methods, local expansion methods, and numerical integration-based methods.
Series: ASM Handbook
Volume: 22A
Publisher: ASM International
Published: 01 December 2009
DOI: 10.31399/asm.hb.v22a.a0005407
EISBN: 978-1-62708-196-2
... of simple synchronous processing elements that are inspired by the biological central nervous systems in living organisms. It comes to a conclusion, given the relevant information, or stimuli, and experience. The basic unit, or building block, in the ANN is the neuron, also referred to as the node. Neurons...
Abstract
Neural-network (NN) modeling is most suitable for simulations of correlations that are hard to describe or cannot be accurately predicted by physical models. This article describes the principles and procedures of NN modeling. It discusses the use of NN modeling in general organization of software and graphical user interfaces. The article also provides information on the ways to improve and upgrade the NN models.
Book Chapter
Analysis Methods for Probabilistic Life Assessment
Available to PurchaseSeries: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003514
EISBN: 978-1-62708-180-1
... when an experiment is repeated and different values are observed. In general, a random sample can be defined as X ˜ = ( X 1 , X 2 , … , X n ), where X i is the i th observation and n is the sample size. The engineer needs to make decisions in face of this uncertainty. Thus...
Abstract
This article describes the historical background, uncertainties in structural parameters, classifications, and application areas of probabilistic analysis. It provides a discussion on the basic definition of random variables, some common distribution functions used in engineering, selection of a probability distribution, the failure model definition, and a definition of the probability of failure. The article also explains the solution techniques for special cases and general solution techniques, such as first-second-order reliability methods, the advanced mean value method, the response surface method, and Monte Carlo sampling. A brief introduction to importance sampling, time-variant reliability, system reliability, and risk analysis and target reliabilities is also provided. The article examines the various application problems for which probabilistic analysis is an essential element. Examples of the use of probabilistic analysis are presented. The article concludes with an overview of some of the commercially available software programs for performing probabilistic analysis.
Series: ASM Handbook
Volume: 20
Publisher: ASM International
Published: 01 January 1997
DOI: 10.31399/asm.hb.v20.a0002427
EISBN: 978-1-62708-194-8
... combines and recombines his past experience, possibly with some distortion, in such a way that he arrives at new patterns, new configurations, and arrangements that better solve some need of mankind.” ( Ref 3 ) “Creativity is a process of becoming sensitive to problems, deficiencies, gaps in knowledge...
Abstract
This article presents the definitions of creativity and creative thinking. It discusses the various stages in creative problem solving process. The stages include understanding the product problem, transforming the product, and breaking the product into subfunctional groups. The article provides a description of concept generating tools that are often arbitrarily described as individual or group tools. It concludes with a discussion on the application of creative concept generation in product design.
Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006682
EISBN: 978-1-62708-213-6
... at repetitive counting. Many years ago, George Moore ( Ref 5 ) and members of ASTM International Committee E-4 on Metallography conducted a simple counting experiment. Approximately 400 people were asked to count the number of times the letter “e” appeared in a paragraph without physically marking or striking...
Abstract
This article reviews many commonly used stereological counting measurements and the relationships based on these parameters. The discussion covers the processes involved in sampling and specimen preparation. Quantitative microstructural measurements are described including volume fraction, number per unit area, intersections and intercepts per unit length, grain size, and inclusion content.
Book: Composites
Series: ASM Handbook
Volume: 21
Publisher: ASM International
Published: 01 January 2001
DOI: 10.31399/asm.hb.v21.a0003414
EISBN: 978-1-62708-195-5
.... To keep the process rational as they moved from spray-up to vacuum infusion, they used a thin glass fiber shell instead of a bag as the male mold. The female mold is similar to a spray-up mold that has a modified flange construction. The lay-up consists of a heavy combination fabric (a random mat material...
Abstract
Vacuum infusion is a resin injection technique derived from resin transfer molding. This article discusses the characteristics of the technique and its applications. It presents the theory and background of the technique and provides an illustration of how parts are made. The article provides information on the equipment and material used for vacuum infusion. It describes the mechanical properties of components and summarizes the influence of production on the properties. The article concludes with a discussion on design guidelines.
Series: ASM Handbook
Volume: 23
Publisher: ASM International
Published: 01 June 2012
DOI: 10.31399/asm.hb.v23.a0005676
EISBN: 978-1-62708-198-6
... on the sequence and number of monomer units in the backbone (e.g., statistical, random, or alternating). Common medical copolymers include thermoplastic elastomers such as thermoplastic polyurethane and polyether-block-amide. The chemical nature of the monomers in a polymer will affect its interaction within...
Abstract
Polymers offer a wide range of choices for medical applications because of their versatility in properties and processing. This article provides an overview of polymeric materials and the characteristics that make them a unique class of materials. It describes the ways to classify polymers, including the polymerization method, how the material deforms, or molecular origin or stability. The article contains tables that list common medical polymers used in medical devices. It explains the medical polymer selection criteria and regulatory aspects of materials selection failure analysis and prevention. Failure analysis and prevention processes to determine the root cause of failures that arise at different stages of the product life cycle are reviewed. The article describes the mechanisms of plastic product failure analysis. It discusses the trends in the use of medical polymers, such as high-performance polymers for implants, tissue engineering, and bioresorbable polymers.
Book Chapter
Probability of Detection
Available to PurchaseSeries: ASM Handbook
Volume: 17
Publisher: ASM International
Published: 01 August 2018
DOI: 10.31399/asm.hb.v17.a0006463
EISBN: 978-1-62708-190-0
... of size a in the trial. A standard or guideline on how to perform an experiment to estimate a POD curve was not available immediately. Within the American Society for Nondestructive Testing (ASNT), an effort was initiated by W.H. Lewis to develop a recommended practice document. Although the final...
Abstract
Probability of detection (POD) assesses the performance of a non-destructive evaluation (NDE)-based inspection, which is a method used to determine the capability of an inspection as a function of defect type and defect size. This article provides an overview of the concept of POD, why it is needed, the history behind the development of POD, how POD assessments are performed, and how modeling and simulation can be integrated into the execution of a POD assessment. It describes the methods by which POD is determined. This includes detail on the experimental process to acquire the needed data, the mathematical methods to obtain a POD curve, and techniques to assess uncertainty in the POD curve as it is obtained from a limited data set. The concept of model-assisted POD (MAPOD) is introduced, with additional details and representative examples of MAPOD.
Series: ASM Handbook
Volume: 22A
Publisher: ASM International
Published: 01 December 2009
DOI: 10.31399/asm.hb.v22a.a0005432
EISBN: 978-1-62708-196-2
... in the same flock, but their movements are somehow connected. Similarly, grain “X” does not know that grain “Y” is recrystallizing some tens or hundreds of micrometers away in a block of metal, but their behavior can be connected through the kinetics of recrystallization. It is this localization of the rules...
Abstract
This article examines how cellular automaton (CA) can be applied to the simulation of static and dynamic recrystallization. It describes the steps involved in the CA simulation of recrystallization. These include defining the CA framework, generating the initial microstructure, distributing nuclei of recrystallized grains, growing the recrystallized grains, and updating the dislocation density. The article concludes with information on the developments in CA simulations.
Series: ASM Handbook
Volume: 8
Publisher: ASM International
Published: 01 January 2000
DOI: 10.31399/asm.hb.v08.a0009219
EISBN: 978-1-62708-176-4
... validity. Reference 1 provides several examples of randomized test programs, including a completely randomized design, a randomized complete block design, and elementary split plot designs. Identifying Control Modes and Test Types In planning fatigue experiments, it is important to keep in mind...
Abstract
This article reviews the planning of fatigue experiments, including the structure of a test plan, randomization, and nuisance variables. The statistical characterization of the S/N (stress/life) or e/N (strain/life) response of a single material tested under a single condition is discussed. The techniques for defining a mean fatigue curve and evaluating scatter or variability about that mean are explained. The article presents the standard techniques for statistical characterization of the fatigue strength or fatigue limit of a single material by use of the Probit method, the up-and-down (staircase) method, and two-point procedures. Stress-level selection methods are also presented. The article discusses the comparison of the fatigue behavior of two or more materials for data generated at a single stress or strain level. Treatments to compare data generated over a range of stress or strain levels are included. The article also summarizes the consolidation of fatigue data generated at different conditions.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003516
EISBN: 978-1-62708-180-1
... such as the Palmgren-Miner Rule did not recognize complex stress sequencing. Fig. 8 Different types of block spectra. (a) Low-high. (b) High-low. (c) Low-high-low Unfortunately, the use of the block spectrum did not accurately reflect the fleet experience, and it should be noted that the fleet experience...
Abstract
This article discusses the fundamental variables involved in fatigue-life assessment, which describe the effects and interaction of material behavior, geometry, and stress history on the life of a component. It compares the safe-life approach with the damage-tolerance approach, which employs the stress-life method of fatigue life assessment. The article examines the behavior of three different metallic materials used in the design and manufacture of structural components: steel, aluminum, and titanium. It also reviews the effects of retardation and spectrum load on component life. The article concludes with case studies of fatigue life assessment from the aerospace industry.
Book Chapter
Formation of Microstructures, Grain Textures, and Defects during Solidification
Available to PurchaseSeries: ASM Handbook
Volume: 22B
Publisher: ASM International
Published: 01 November 2010
DOI: 10.31399/asm.hb.v22b.a0005518
EISBN: 978-1-62708-197-9
... Grain Solidification” in this Volume, where they are referred to as direct models of the grain structure. They provide a detailed description of the grain structure and, in particular, textures in cast parts, including statistical aspects due to random nucleation events. Unlike direct models...
Abstract
This article reviews the various aspects of the simulation of solidification microstructures and grain textures. It describes the grain structures and morphology of dendrites or eutectics that compose the internal structure of the grains. A particular emphasis has been put on the simulation of defects related to grain textures and microstructures. The article provides information on the application of the most important simulation approaches and the status of numerical simulation.
Book: Composites
Series: ASM Handbook
Volume: 21
Publisher: ASM International
Published: 01 January 2001
DOI: 10.31399/asm.hb.v21.a0003402
EISBN: 978-1-62708-195-5
... of the physical process or the system. Manufacturing of composites has relied on intuition based on experience and trial and error methods when designing, developing, and producing new products. However, this approach has proven to be expensive in time and money when developing new prototype geometries. The risks...
Abstract
This article provides information on the classification of various composites manufacturing processes based on similar transport processes. The composites manufacturing processes can be grouped into three categories: short-fiber suspension methods, squeeze flow methods, and porous media methods. The article presents an overview of the modeling philosophy and approach that is useful in describing composite manufacturing processes.
Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006637
EISBN: 978-1-62708-213-6
... standard samples, RBS analyses often serve as standards for other techniques that are much more sensitive but require calibration. Detailed information on RBS is available in Ref 1 to 3 . Rutherford’s first scattering experiment established the analytical utility of the ion beam. Scattering...
Abstract
This article provides a detailed account of the basic concepts of Rutherford backscattering spectrometry (RBS). It begins with a description of the principles of RBS, as well as the effect of channeling in conjunction with backscattering measurements and the effect of energy loss under this condition. This is followed by a section on equipment used in RBS analysis. Channel-energy conversion, energy-depth conversion, and separation of the dechanneling background are then discussed as the main steps of RBS data analysis. The article also discusses the applications of RBS—including composition of bulk samples, thin-film composition and layer thickness, impurity profiles, damage depth profile, and surface peak—as well as the various codes developed to simulate it.
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