Quenchant agitation can be obtained by circulating quenchant in a quench tank through pumps and impellers. The selection of the agitation method depends on the tank design, type and volume of the quenchant, part design, and the severity of quench required. This article describes flow measurement methods, temperature control, materials handling, and filtration processes during the agitation process. The maintenance of quenching installations is also discussed.

This article provides information on the various stages of quenching, sources of distortion, and factors that affect the creation of thermal gradients. It reviews the various determinations of heat-transfer coefficients by the thermal conductivity and diffusivity method, analytical and empirical methods, application of cooling curves, computational fluid dynamics, and the inverse conduction calculation and measurement of parts. Suitable examples are also provided.

Molten salt, including nitrite/nitrate salts, is the quenching medium most commonly used in austempering and marquenching of ferrous materials. This article describes the use of molten salts in the quenching of ferrous materials. It provides information on the processing and operation of salt quenching including considerations of time, temperature, environment, and safety, as well as critical characteristics such as the composition of the quenchant, agitation, and water additions.

The fundamental objective of quenching is to preserve, as nearly as possible, a metastable solid solution formed at the solution heat treating temperature, by rapidly cooling to some lower temperature, usually near room temperature. This article provides an overview of the factors used to determine a suitable cooling rate and the appropriate quenching process to develop a suitable cooling rate. It discusses the three distinct stages of quenching: vapor stage, boiling stage, and convection stage. The article reviews the factors that affect the rate of cooling in production operations. It discusses the quenchants that are used in quenching aluminum alloys, namely, hot or cold water and polyalkylene glycol. The article also describes the racking practices for controlling distortion and the level of residual stresses induced during the quench.

Quenching refers to the rapid cooling of metal from the solution treating temperature, typically between 465 and 565 deg C (870 and 1050 deg F) for aluminum alloys. This article provides an overview on the appropriate quenching process and factors used to determine suitable cooling rate. It describes the quench sensitivity and severity of alloys, quench mechanisms and the different types of quenchants used in immersion, spray, and fog quenching. The article provides a detailed description of the quench-factor analysis that mainly includes residual stress and distortion, which can be controlled by proper racking. It concludes with information on agitation and the quench tank system used in the quenching of aluminum alloys.

Quenching severity is agitation-dependent and therefore, magnitude and turbulence of fluid flow around a part in the quench zone are critically important relative to the uniformity of heat transfer throughout the quenching process. This article provides an overview of the measurement principles for different types of flow devices used in production quench tanks, namely, vane sensors, fluid-quench sensors, caterpillar quench-evaluation sensors, and thermal probes. Various methods of flow measurement in commercial quench tanks may be acceptable for adequate control to ensure a high-quality production process.

Intensive quenching (IQ) is an alternative method of hardening steel parts, providing extremely high cooling rates within the martensite-phase formation temperature range. This article begins with the description on the general correlation between steel mechanical properties and cooling rate during IQ. It presents a review of batch intensive quenching (IQ-2) methods and single-part intensive quenching (IQ-3) methods as well as practical applications of these methods. The article provides useful information on the effect of heat flow on cooling in these methods, and discusses the improvements achieved in part microstructure, mechanical properties, and stress conditions of steel, after intensive quenching. It also describes the reasons for part distortion in IQ, and reviews the types of quench systems used in IQ-2 and IQ-3 processes.

This article provides an overview of common quenching media, the factors involved in the mechanism of quenching, and process variables, namely, surface condition, mass and section size of the workpiece, and flow rate of the quenching liquid. It describes the methods of quenchant characterization using hardening-power and cooling-power tests. The article discusses the fundamentals involved in heat-transfer coefficient and heat flux of quenching processes. This discussion is followed by various actual examples of applications of these methods using simplified equations. Quenchant evaluation, classification, selection, and maintenance are reviewed in detail. The article addresses the various reasons for quench oil variability and complications due to aging and contamination.

Induction heating has many different applications, such as melting, heating stock for forging, and heat treating. This article begins with a discussion on the types of power supplies, namely, solid-state power supplies and oscillator tubes. It provides information on system elements, including cooling systems, power supplies, heat stations, work handling fixtures, induction or work coils, and quench systems. The article discusses the influence of system elements on induction heat treating system design. It also deals with the general theory, types, and applications of induction coils.

Induction heating for hardening of steels has advantages from the standpoint of quenching because parts are individually processed in a controlled manner. This article provides information on the effect of agitation, temperature, hardening, residual stresses, and quenching media, on quenching. It also describes various quenching methods for steel induction heat treating, namely, spray quenching, immersion quenching, self or mass quenching, and forced air quenching. The article also reviews quench system design and quenchants and their maintenance.

This article describes various quenchants, namely, water and inorganic salt solutions, polymers (polyvinyl alcohol, polyalkylene glycol, polyethyl oxazoline, polyvinyl pyrrolidone and sodium polyacrylates), quench oils, and molten salts, which are used for heat treatment of ferrous alloys. It also provides information on the steps for controlling quenching performance for polymer quenchants and oils with an emphasis on measuring quenchant performance, safety measures, and oxidation.

The fluidized bed provides a means for exchanging heat between a metal part, the solid particles, and the fluidizing gas and which is viable for quenching. This article briefly considers the design aspects of the gas distributor, plenum, container, immersed cooling tubes and surface air spray cooling system in the quenching fluidized bed. It describes the fundamental factors affecting quenching power of the fluidized beds, namely, particle size, particle material, fluidizing gas composition, fluidizing gas flow rate, bed temperature and pressure, and the arrangement of quenched parts with respect to one another and to the bed. The article discusses the advantages, disadvantages, various applications and processes, including conventional batch quenching, two-step batch quenching, and continuous quenching of fluidized bed quenching, in detail.

Hardness testing equipment is important as all results from the induction equipment are graded by the hardness testing equipment. This article includes maintenance tips and points to consider regarding hardness test equipment, power supplies, controls, programmable logic controllers, computer systems, water cooling systems, fixtures and machines, air-operated or pneumatic devices, coils, and quench systems. It also presents simple rules that need to be applied while moving the equipment from one location to another.

This article provides information on the boundary conditions that must be applied to model the heat-transfer coefficient (HTC) in a component being cooled. It describes the historical perspective of various experiments to determine the HTCs. Computational fluid dynamics codes have also been used to predict the HTCs around a part. The article provides information on the various modeling studies used to predict cooling rates in a component. The prediction of residual stresses by validation and optimization of residual stress models is also discussed. Several techniques, such as models neglecting and incorporating material transformation effects, used to predict residual stresses are reviewed. The article also explains the various aspects of models used to prevent cracking during heating and quenching.

This article provides a detailed discussion on the types of furnace atmospheres required for heat treating. These include generated exothermic-based atmospheres, generated endothermic-based atmospheres, generated exothermic-endothermic-based atmospheres, generated dissociated-ammonia-based atmospheres, industrial gas nitrogen-base atmospheres, argon atmospheres, and hydrogen atmospheres. Atmospheres for backfilling, partial pressure operation, and quenching in vacuum are also discussed. Furnace atmospheres constitute four major groups of safety hazards in heat treating: fire, explosion, toxicity, and asphyxiation. The article reviews the fundamentals of principal gases and vapors. It describes how the evaluation of the atmospheric requirements of heat treating furnaces is influenced by factors such as cost of operation and capital investment.

Furnaces are one of the most versatile types of industrial appliances that span many different areas of use. This article discusses the classification of various furnaces used in heat treating based on the mode of operation (batch-type furnaces and continuous-type furnaces), application, heating method, mode of heat transfer, type of materials handling system, and mode of waste heat recovery (recuperation and regeneration). It provides information on uniform temperature distribution, the general requirements and selection criteria for insulation materials, as well as the basic safety requirements of these furnaces.

Vacuum heat treating consists of thermally treating metals and alloys in cylindrical steel chambers that have been pumped down to less than normal atmospheric pressure. This article provides a detailed account of the operations and designs of vacuum furnaces, discussing their pressure levels, resistance heating elements, quenching systems, work load support, pumping systems, and temperature control systems. It describes the classification of instruments used for measuring and recording pressure inside a vacuum processing chamber. Common devices include hydrostatic measuring devices and devices for measuring thermal and electrical conductivity. The article also describes the applications of the vacuum heat treating process, namely, vacuum nitriding and vacuum carburizing. Finally, it reviews the heat treating process of tool steels, stainless steels, Inconel 718, and titanium and its alloys.

This article describes the advantages of martempering and the use of oil and salt as quenchants in the martempering process. It also discusses safety precautions to be followed by an operator and reviews the steels that are suitable for martempering. The article provides information on the importance of controlling process variables in martempering, including austenitizing temperature, temperature of the martempering bath, time in the bath, salt contamination, water additions to salt, agitation, and the rate of cooling from the martempering bath. It also describes specific situations in which distortion problems have been encountered during martempering. The article contains tables that indicate typical applications of martempering in salt and oil by listing commonly treated steel parts and giving details of martempering procedures and hardness requirements. The article also lists equipment requirements for oil and salt martempering of steel.

This article describes the uses of the liquid carburizing process carried out in low and high temperature cyanide-containing baths, and details the noncyanide liquid carburizing process which can be accomplished in a bath containing a special grade of carbon. It presents a simple formula for estimating total case depth, and illustrates the influence of carburizing temperature, duration of carburizing, quenching temperature, and quenching medium with the aid of typical hardness gradients. The article provides information on controlling of cyaniding time and temperature, bath composition, and case depth, and presents examples that relate dimensional change to several shapes that vary in complexity. It also provides information on the quenchant removal and salt removal processes, lists the applications of liquid carburizing in cyanide baths, and discusses the process and importance of cyanide waste disposal in detail.