The quantitative characterization of fracture surface geometry, that is, quantitative fractography, can provide useful information regarding the microstructural features and failure mechanisms that govern material fracture. This article is devoted to the fractographic techniques that are based on fracture profilometry. This is followed by a section describing the methods based on scanning electron microscope fractography. The article also addresses procedures for three-dimensional fracture surface reconstruction. In each case, sufficient methodological details, governing equations, and practical examples are provided.

This article describes the fatigue properties of particle-reinforced metal-matrix composites (PR-MMCs) in terms of mechanisms of crack initiation, fatigue life, and fatigue crack growth. It reviews specimen preparation and microscopic procedures that are used in fatigue testing of MMCs. It also describes the evaluation of the long fatigue crack growth behavior of MMCs by using the test methods and specimens that are used for unreinforced metallic alloys. Fractography of MMCs under plane-strain conditions is also described with information on the observed features of MMC fatigue fracture surfaces and their observation methods.

The principal objective of quantitative fractography is to express the characteristics of features in the fracture surface in quantitative terms, such as the true area, length, size, spacing, orientation, and location. This article provides a detailed account of the development of more quantitative geometrical methods for characterizing nonplanar fracture surfaces. Prominent techniques for studying fracture surfaces are based on the projected images, stereoscopic viewing, and sectioning. The article provides information on various roughness and materials-related parameters for profiles and surfaces. The applications of quantitative fractography for striation spacings, precision matching, and crack path tortuosity are also discussed.

The purpose of fractography is to analyze fracture features and attempt to relate the topography of the fracture surface to the causes and/or basic mechanisms of fracture. This article reviews the historical development of fractography, from the early studies of fracture appearance dating back to the sixteenth century to the state-of-the-art work in electron fractography and quantitative fractography. It also describes the applications and limitations of scanning electron microscope and transmission electron microscope.

This article discusses the fractal characteristics of fracture surfaces as a means for describing and quantifying irregular, complex curves and surfaces of fractured materials. It describes the important relationship between the profile and surface roughness parameters that yield the surface area of irregular fracture surfaces. The article reviews the experimental procedures required to obtain profiles and measurements that are made. In addition, fractal equations that linearize all the experimental data and provide constant fractal dimensions are presented in the article. Modified fractal dimensions that result from these analyses appear to possess some generality for natural irregular nonplanar surfaces and their profiles.

Failure analysis is a process of acquiring specified information regarding the appropriateness of the design of a part, the competence with which the various steps of its manufacture have been performed, any abuse suffered by it in packing and transportation, or the severity of service under which failure has occurred. Beginning with a discussion of the various stages of failure analysis of glass and ceramic materials, this article focuses on descriptive and quantitative fracture surface analysis techniques that are used in the examination of glass and surfaces created by fracture and the interpretation of the fracture markings seen on these surfaces. Details are provided for the procedures for locating fracture origins, determining direction of crack propagation, learning the sequence of crack propagation, deducing the stress state at the time of fracture, and observing interactions between crack fronts and inclusions, etc. A separate fractography terminology is provided in this article.

This article provides a summary of the concepts discussed in the articles under the Section “Failure Analysis” in ASM Handbook, Volume 21: Composites. Most of the information in this Section is geared toward organic-matrix composites, although there is some information on failure analysis and fractography of ceramic- and metal-matrix composites.

Scanning electron microscopy (SEM) has unique capabilities for analyzing fracture surfaces. This article discusses the basic principles and practice of SEM, with an emphasis on its applications in fractography. The topics include an introduction to SEM instrumentation, imaging and analytical capabilities, specimen preparation, and the interpretation of fracture features. SEM can be subdivided into four systems, namely, illuminating/imaging, information, display, and vacuum systems. The article also describes the major criteria and techniques of SEM specimen preparation, and the general features of ductile and brittle fracture modes.

Fractography is the means and methods for characterizing a fractured specimen or component. This includes the examination of fracture-exposed surfaces and the interpretation of the fracture markings as well as the examination and interpretation of crack patterns. This article describes the former of these two parts of fractography. It presents the techniques of fractography and explains fracture markings using glass and ceramic examples. The article also discusses the fracture modes in ceramics and provides examples of fracture origins.

This article provides an overview of fractography and explains how it is used in failure analysis. It reviews the basic types of fracture processes, namely, ductile, brittle, fatigue, and creep, principally in terms of fracture appearances, such as microstructure. The article also describes the general features of fatigue fractures in terms of crack initiation and fatigue crack propagation.

This article provides an overview of the origin of metallography. It presents information on how to select a section from a specimen and prepare it for macroscopic analysis. The article describes the macroscopic analysis of steel fracture surfaces with emphasis on ductile, brittle, and fatigue fracture with illustrations. It discusses microanalysis with a focus on the method of light microscopy and includes information of scanning electron microscope in fractography. The article also explains the characteristics of solidification, transformation, deformation structures, and discontinuities that are present in a microstructure. It concludes with information on image analysis.

Engineering component and structure failures manifest through many mechanisms but are most often associated with fracture in one or more forms. This article introduces the subject of fractography and aspects of how it is used in failure analysis. The basic types of fracture processes (ductile, brittle, fatigue, and creep) are described briefly, principally in terms of fracture appearances. A description of the surface, structure, and behavior of each fracture process is also included. The article provides a framework from which a prospective analyst can begin to study the fracture of a component of interest in a failure investigation. Details on the mechanisms of deformation, brittle transgranular fracture, intergranular fracture, fatigue fracture, and environmentally affected fracture are also provided.

This article discusses the operating principles, advantages, and limitations of scanning electron microscopy, atomic force microscopy, x-ray photoelectron spectroscopy, and secondary ion mass spectroscopy that are used to analyze the surface chemistry of plastics.

This article describes the failure analysis procedures for composites and the techniques to be used in these analyses. These procedures include a review of the available in-service records, materials and processing methods, print requirements, and manufacturing records; visual analysis and nondestructive part evaluation; and verification of materials and processing methods. The article discusses the determination of fiber, matrix, and void volume fractions and verification of ply lay-up and orientation. A review of composites processing parameters; fractography and surface analysis; and mechanical testing and stress analysis is also presented.

This article presents examples of the visual fracture examination that illustrate the procedure as it applies to failure analysis and quality determination. It describes the techniques and procedures for the visual and light microscopic examination of fracture surfaces with illustrations. The article also describes microscopic and macroscopic features of the different fracture mechanisms with illustrations with emphasis on visual and light microscopy examination. The types of fractures considered include ductile fractures, tensile-test fractures, brittle fractures, fatigue fractures, and high-temperature fractures.

This article reviews the essential parts of the complex process of quantitative image analysis to assist automatic image analysis in laboratories. It describes the basic difference between the bias of classical manual stereological analysis and quantitative image analysis. The article concentrates on the basic properties of digital measurements that are the core of quantitative image analysis. It provides a brief description of the specimen and apparatus preparation as well as the image acquisition. The article explains how to evaluate stereological parameters and provides the general rules and guidelines for optimization of image processing algorithms from the viewpoint of shape quantification. It concludes with examples that demonstrate the usefulness of automatic image analysis in comparison to manual methods.

Fractography is the systematic study of fractures and fracture surfaces. It is a useful tool in failure analysis and provides a means for correlating the influence of microstructure on the fracture mode of a given material. This article discusses the preservation, preparation, and photography of fractured parts and surfaces, and describes some of the more common fractographic features revealed by light microscopy, including tensile-fracture surface marks in unnotched specimens, fatigue marks, and structural discontinuities within the metal. The article also explains how to interpret fracture information contained in optical and scanning-electron microscope fractographs.

This article outlines the beam/sample interactions and the basic instrumental design of a scanning electron microscopy (SEM), which include the electron gun, probeforming column (consisting of magnetic electron lenses, apertures, and scanning coils), electron detectors, and vacuum system. It discusses the contrasts mechanisms used for imaging and analyzing materials in the SEM. These include the topographic contrast, compositional contrast, and electron channeling pattern and orientation contrast. Special instrumentation and accessory equipment used at elevated pressures and during the X-ray microanalysis are reviewed. The article also provides information on the sample preparation procedure and the materials applications of the SEM.